Patent classifications
B01J20/28009
Preparation of Magnetic Core-Shell Particles
The invention relates to a process for preparing core-shell particles comprising the steps of (i) providing a dispersion of primary magnetic particles having a mean diameter lower than 200 nm in a solvent; (ii) adding one or more (semi-)metal (oxyhydr)oxide(s) and/or one or more precursor(s) of a (semi-)metal (oxyhydr)oxide to said dispersion; (iii) optionally adding a hydrolysis agent for said one or more precursor(s); (iv) injecting the dispersion in a spray dryer; whereby a (semi-)metal (oxyhydr)oxide shell is formed on the magnetic particles during spray drying. The invention also relates to particles obtainable by said process, to a formulation of said particles in a solvent and to the use of said particles or said formulation for RNA or DNA extraction.
Magnetic soil remediation agent for soil heavy metal pollution, preparation method and use thereof
A magnetic soil remediation agent for soil heavy metal pollution and a preparation method and application thereof are provided. The magnetic soil remediation agent is prepared by using remediation agent framework material and magnetic core material as raw materials, and heavy metal collector as modifier; said framework material is silicon dioxide activated by strong alkali; said magnetic core material comprises magnetic materials Fe.sub.3O.sub.4 and γ-Fe.sub.2O.sub.3; said modifier comprises ethylenediaminetetraacetic acid (EDTA), nitrilotriacetic acid trisodium salt (NTA), (S,S)-ethylenediamine-N,N-disuccinic acid trisodium salt (EDDS) and mercaptoethylamine. The remediation agent of the present invention can effectively passivate the heavy metals in the soil, reduce their available contents, and inhibit the absorption of heavy metals by plants.
Method and reactor for separating and removing heavy metals from wastewater using sulfhydryl-modified nano-magnetized activated carbon
A method and reactor are disclosed for separating and removing heavy metals from wastewater using a sulfhydryl-modified nano-magnetized activated carbon. The method includes the steps of preparing a sulfhydryl-modified nano-magnetized activated carbon first; introducing heavy-metal-containing wastewater into a reactor which is equipped with a stirrer and keeping stirring, and then adding the sulfhydryl-modified nano-magnetized activated carbon, continuously stirring for a reaction; after reacting for a period, precipitating under a magnetic field generated by a magnet separator, discharging the resulting supernate, and then discharging the precipitated sludge.
Hydrocarbon adsorbent
To provide a hydrocarbon adsorbent having high hydrocarbon adsorbing properties even after exposed to a high temperature/high humidity reducing atmosphere. A hydrocarbon adsorbent, which includes a FAU type zeolite having a lattice constant of at least 24.29 Å and containing copper. Such a hydrocarbon adsorbent may be used for a method for adsorbing hydrocarbons to be exposed to a high temperature/high humidity environment, and may be used particularly for a method for adsorbing hydrocarbons in an exhaust gas of an internal combustion engine, such as an automobile exhaust gas.
Hybrid material for chromatographic separations comprising a superficially porous core and a surrounding material
The present invention provides novel chromatographic materials, e.g., for chromatographic separations, processes for their preparation and separations devices containing the chromatographic materials. The preparation of the inorganic/organic hybrid materials of the invention wherein a surrounding material is condensed on a superficially porous hybrid core material will allow for families of different hybrid packing materials to be prepared from a single core hybrid material. Differences in hydrophobicity, ion-exchange capacity, chemical stability, surface charge or silanol activity of the surrounding material may be used for unique chromatographic separations of small molecules, carbohydrates, antibodies, whole proteins, peptides, and/or DNA.
MAGNETIC TITANIUM-BASED LITHIUM ADSORBENT AND PREPARATION METHOD THEREOF
In order to resolve the problem that a magnetic lithium adsorbent in the related art is difficult to be used for lithium extraction from strong-alkaline and carbonate-type brines, a magnetic titanium-based lithium adsorbent is provided, which includes a magnetic composite and a lithium adsorption layer. The lithium adsorption layer is disposed at an outer surface of the magnetic composite. The magnetic composite includes a magnetic material and a titanium oxide. The lithium adsorption layer includes a lithium titanium oxide.
Core-shell structure polymer magnetic nanospheres with high Cr (VI) adsorption capacity, preparation method and application
A method for preparing a core-shell structure polymer magnetic nanosphere with a high Cr (VI) adsorption capacity includes: adding Fe3O4 powder into a mixed solution of water and ethanol, dispersing Fe3O4 powder in the solution evenly by ultrasound, sequentially adding resorcinol and formaldehyde into the suspension to adjust a pH, stirring and reacting to obtain Fe3O4@RF evenly dispersed in a chitosan solution, dropwise adding the prepared suspension into a mixed solution of paraffin and span 80, stirring for a period of time, adding a glutaraldehyde aqueous solution, stirring and reacting to obtain a magnetic chitosan nanosphere. The magnetic chitosan nanosphere prepared may be applied to adsorbing Cr (VI) in a water solution. Not only the magnetic chitosan nanospheres prepared has a high adsorption capacity for Cr (VI), but also can be quickly separated by an external magnetic field after adsorption.
Radionuclide adsorbent, method of preparing the same and method of removing radionuclide using the same
The present invention relates to a radionuclide adsorbent, which includes a hollow space (specifically, an area which is entirely empty or in which transition metal oxide particles are present); and a transition metal-ferrocyanide shell (specifically, a transition metal-ferrocyanide shell having a structure in which a plurality of two-dimensional nano flakes overlap or a transition metal-ferrocyanide shell having a structure in which a plurality of three-dimensional nano polyhedrons agglomerate) formed on the space surface, a preparation method thereof, and a method of removing a radionuclide using the same.
MICROVESICLE ISOLATION METHOD AND MICROVESICLE ISOLATION
Disclosed is a microvesicles isolation method to isolate microvesicles contained in the biological sample from the sample, the method comprising: (a) adding an adsorbent sphere to the biological sample containing the microvesicles therein; (b) keeping the adsorbent sphere in the biological sample to form an adsorbent sphere conjugate composed of the adsorbent sphere and the microvesicles captured thereon; (c) isolating the adsorbent sphere conjugate from the biological sample; (d) washing the isolated adsorbent sphere conjugate using a first reagent; and (e) eluting the microvesicles from the washed adsorbent sphere conjugate using a second reagent, wherein the adsorbent sphere includes a support, and one or more polyvalent cations disposed on a surface of the support.
Magnetic Soil Remediation Agent for Soil Heavy Metal Pollution, Preparation Method and Use Thereof
A magnetic soil remediation agent for soil heavy metal pollution and a preparation method and application thereof are provided. The magnetic soil remediation agent is prepared by using remediation agent framework material and magnetic core material as raw materials, and heavy metal collector as modifier; said framework material is silicon dioxide activated by strong alkali; said magnetic core material comprises magnetic materials Fe.sub.3O.sub.4 and γ-Fe.sub.2O.sub.3; said modifier comprises ethylenediaminetetraacetic acid (EDTA, nitrilotriacetic acid trisodium salt (NTA, (S,S)-ethylenediamine-N,N-disuccinic acid trisodium salt (EDDS) and mercaptoethylamine. The remediation agent of the present invention can effectively passivate the heavy metals in the soil, reduce their available contents, and inhibit the absorption of heavy metals by plants.