A method for conveying a reaction tube unit including a vertical reaction tube and a gas supply pipe provided at a distance from an inner wall of the vertical reaction tube along a longitudinal direction thereof, the method includes: arranging a buffer inside the reaction tube between the inner wall and the gas supply pipe to alleviate a collision; placing the reaction tube unit attached with the buffer on a carriage via a vibration isolator; and conveying the reaction tube unit by moving the carriage.

Disclosed is an experimental device for studying the sediment yield behavior and the radial deformation of porous media during the exploitation of natural gas hydrates, comprising a high-pressure reactor, a hydrate sample chamber, a simulated wellbore, a deformation measurement unit, an ambient temperature control unit, an outlet control unit, an inlet control unit and a data processing unit. Further disclosed is a method using the above-mentioned experimental device to carry out experiments. The experimental device and method according to the present invention can conveniently measure the deformation of the porous media during the decomposition of the hydrates and simulate the sediment producing situation in the wellbore, can simulate the sediment yield problem during the exploitation of natural gas hydrates as well as the gas-liquid-solid flowing problem in the wellbore during the exploitation of natural gas hydrates, and can accurately obtain the gas-solid-liquid three-phase yields in real time during the decomposition of natural gas hydrates. Being simple to operate and easy to control, and suitable for various sizes and shapes of reactors, it can provide basic experimental data and a theoretical basis for the technologies of hydrate exploitation.

A gas analysis system and method using a spectrometer, such as a Fourier transform infrared spectrometer, utilizes a reactor, such as a catalytic reactor, for providing interference spectra. The gas is pressurized and chilled to remove water prior to the spectrometer.

The invention discloses a disposable reaction device, a tracer synthesizer and a method for producing a tracer. The disposable reaction device comprises: (1) a disposable reagent bottle, which is used for loading the substances required for reaction, including radioisotopes, solvents, reagents, and reactants; the load can be filled directly or through a disposable liquid pipeline into the disposable reactor; (2) disposable reactors, which are used to contain radioisotopes and at least one reagent for reaction, and can be sealed with pierceable materials; (3) disposable liquid pipelines, including evaporation elements, filling elements, retraction elements, and mass transfer pipelines. The beneficial advantages brought by the present invention are: First, there is no need to wait for 10 half-lives of radioactive decay before proceeding to the next tracer production. Secondly, the disposable reaction device enables the synthesis of the same or different tracers to be repeated in a short time.

Embodiments described herein relate generally to continuous flow photoreactors with easily replaceable and adjustable components. The photoreactor includes a reactor flow system, a lighting system, and a temperature control system. The reactor flow system includes a reactor inlet port, a reactor outlet port, and a length of reactor tubing fluidically coupled to the reactor inlet port and reactor outlet port. The lighting system includes a light emitting apparatus (e.g., a plurality of LEDs) configured to emit light in a defined wavelength range toward the length of reactor tubing. The temperature control system includes an inlet port, an outlet port, and a length of temperature control tubing fluidically coupled to the inlet port and the outlet port. In some embodiments, the temperature control system can be configured to circulate a fluid to cool the lighting system.

According to some aspects, described herein is an automated droplet-based reactor that utilizes oscillatory motion of a droplet in a tubular reactor under inert atmosphere. In some cases, such a reactor may address current shortcomings of continuous multi-phase flow platforms.

A reactor comprises a reactor vessel defining a confined reactor volume, a support assembly extending about a periphery of the confined reactor volume, a basket positioned within the reactor vessel and supported by the support assembly, the basket having an interior surface and an exterior surface, a downflow zone being defined between the exterior surface of the basket and an interior surface of the confined reactor volume, an inlet screen positioned adjacent to one end of the interior surface and an outlet screen positioned adjacent to an opposite end of the interior surface, an upflow zone defined between the inlet screen and outlet screen, the inlet screen and the outlet screen containing a quantity of particulate catalyst, and a circulating device positioned above said upflow zone and configured to continuously circulate fluid upwardly though said upflow zone and downwardly through said downflow zone, the support assembly and the basket configured to promote the formation of a fluid vortex within a portion of the downflow zone.

An active pharmaceutical ingredients (API) or related substance (RS) can be tested for stability by placing the API or RS in an instrument containing a pressure-controllable atmosphere, controlling the pressure of the atmosphere in the instrument for a predetermined time, and evaluating the API or RS for stability. Testing can be carried out also at predetermined temperature(s) and/or under the influence of gaseous trigger(s) and so forth. For instance, an API sample can be placed in a bomb test instrument/reactor, oxygen as a gaseous trigger can be introduced to contact the API sample under constant and/or ramped temperature(s) and elevated pressure(s) for predetermined time(s), and the API sample can be evaluated for stability. An insert carousel may hold a sample of API(s) and/or RS(s) and/or aliquot(s) of sample(s) of API(s) and/or RS(s) for insertion into the bomb test instrument/reactor.

The automated synthesis of clinically relevant amounts of 16-.sup.18F-fluoro-5-dihydrotestosterone (.sup.18F-FDHT) using a commercially available radiosynthesizer. Synthesis was performed in 90 minutes with a decay-corrected radiochemical yield of 295%. The specific activity was 4.6 Ci/mol (170 GBq/mol) at end of formulation with a starting activity of 1.0 Ci (37 GBq). The formulated .sup.18F-FDHT yielded sufficient activity for multiple patient doses and passed all quality control tests required for routine clinical use.

Systems and methods for synthesizing chemical products, including active pharmaceutical ingredients, are provided. Certain of the systems and methods described herein are capable of manufacturing multiple chemical products without the need to fluidically connect or disconnect unit operations when switching from one making chemical product to making another chemical product.