B01J2219/00029

Lewis base-mediated recovery of fibers from fiber reinforced polymers

Disclosed are methods and apparatus for recovering fibers from fiber reinforced polymers wherein the fiber reinforced polymer is contacted with a Lewis base for a time sufficient to allow at least partial depolymerization of the polymer.

Production of cyclic imides suitable for oxidation catalysis

Disclosed are novel processes for the production of cyclic imide compounds such as N-hydroxyphthalimide (NHPI). The processes may be particularly well-suited for commercial-scale production of cyclic imides such as NHPI. Such cyclic imide compounds are suitable for use as oxidation catalysts, and specifically may be used to oxidize cyclohexylbenzene to cyclohexyl-1-phenyl-1-hydroperoxide. Such an oxidation may be particularly useful in a process for the production of phenol and/or cyclohexanone from benzene via a process comprising hydroalkylation of benzene to cyclohexylbenzene, oxidation of the cyclohexylbenzene to cyclohexyl-1-phenyl-1-hydroperoxide, and cleavage of the cyclohexyl-1-phenyl-1-hydroperoxide to phenol and cyclohexanone. The cyclic imide production process may advantageously include water washing and reactant recovery steps to maximize purity and yield.

Pipe connection structure and processing apparatus
11774017 · 2023-10-03 · ·

A pipe connection structure provided in a processing apparatus, includes a first pipe having a first flange portion formed at one end thereof, a second pipe having a second flange portion formed at one end thereof and connected to the first flange portion, and a pipe clamp configured to connect and fasten the first flange portion and the second flange portion at a plurality of positions including a position where a pipe axis of the first pipe and a pipe axis of the second pipe do not coincide with each other.

Method for preparing cathode active material precursor for secondary battery, and preparation apparatus using same

A method for preparing a cathode active material precursor for a secondary battery, including: moving a co-precipitation filtrate generated after a co-precipitation reaction to a co-precipitation filtrate storage tank; removing a metal hydroxide by passing the co-precipitation filtrate through a filter; reacting the co-precipitation filtrate from which the metal hydroxide is removed with sulfuric acid or nitric acid to produce an ammonium sulfate or an ammonium nitrate while removing ammonia from the co-precipitation filtrate from which the metal hydroxide is removed; cooling and crystallizing the co-precipitation filtrate from which the metal hydroxide and ammonia are removed to precipitate a sodium sulfate; filtering the precipitated sodium sulfate to separate the precipitated sodium sulfate from the co-precipitation filtrate from which the metal hydroxide and ammonia are removed; drying the sodium sulfate separated from the co-precipitation filtrate and moving the co-precipitation filtrate separated from the sodium sulfate to a circulation concentration tank; and heating the co-precipitation filtrate stored in the circulation concentration tank to a predetermined temperature for recycling and performing N.sub.2 purging or bubbling, is provided.

Batch processing apparatus

Current chemical batch processing technology is based on batch reactors, which typically consist of a vessel, in which reactants are processed. The batch reactor comprises a reactor vessel having at least one first thermal transfer element; a removable top cover for sealing the reactor vessel; a baffle component having at least one second thermal transfer element; and an agitator component, wherein each of the at least one first thermal transfer element and the at least one second thermal transfer element is independently controllable, and wherein the batch reactor comprises a thermal transfer surface-to-volume ratio of at least 6:1. This increases the thermal transfer potential and the thermal energy transfer efficiency of the batch reactor, thereby to increase production speed and throughput.

Process for the multi-reactor synthesis of zeolite crystals having a controlled particle size
11377361 · 2022-07-05 · ·

The present invention relates to a process for preparing zeolite crystals having a multimodal particle size distribution, and the sizes of which are between 0.02 μm and 20 μm, said process comprising feeding at least two reactors each with a synthesis gel capable of forming zeolite crystals, carrying out a crystallization reaction, in parallel, in each of the at least two reactors, and mixing the reaction media of the at least two reactors, after the start of at least one of the crystallization reactions.

Method for manufacturing terephthalate-based composition comprising applying pressure
11407706 · 2022-08-09 · ·

Provided is a method for manufacturing a terephthalate-based composition, the method comprising: a step (S1) of flowing in a dialkyl terephthalate in which alkyl has 7 to 10 carbon atoms and a primary alcohol with a low boiling point having 4 or 5 carbon atoms into a reactor and performing transesterification of the dialkyl terephthalate and the primary alcohol with a low boiling point; and a step (S2) of extracting in a reduced pressure an unreacted material and a by-product from the reactor after finishing the transesterification, wherein the step S1 comprises a pressure-applying step in which the pressure of the reactor is 1.5 to 2.5 bar.

PIPE CONNECTION STRUCTURE AND PROCESSING APPARATUS
20220299137 · 2022-09-22 ·

A pipe connection structure provided in a processing apparatus, includes a first pipe having a first flange portion formed at one end thereof, a second pipe having a second flange portion formed at one end thereof and connected to the first flange portion, and a pipe clamp configured to connect and fasten the first flange portion and the second flange portion at a plurality of positions including a position where a pipe axis of the first pipe and a pipe axis of the second pipe do not coincide with each other.

CHEMICAL CONVERTER FOR PRODUCTION OF HYDROGEN GAS

An apparatus for producing hydrogen gas is provided. The apparatus includes a first hopper having a reaction chemical. The reaction chemical includes sodium borohydride (NaBH.sub.4) and a chemical component. The chemical component may be magnesium chloride (MgCl.sub.2). The apparatus also includes a reaction chamber. The reaction chamber has an input for receiving the reaction chemical from the first hopper and an output for removal of hydrogen gas. The apparatus also includes a second hopper for containing spent solid chemical mixture removed or extracted from the reaction chamber.

HYDROGEN GENERATOR
20220105488 · 2022-04-07 ·

A hydrogen generator includes a reaction vessel, a water supply, a temperature adjustor, and a controller. The reaction vessel houses a hydrogen generating material having hydrogen generating ability. The hydrogen generating material includes a two-dimensional hydrogen boride sheet having a two-dimensional network and containing multiple negatively charged boron atoms. The controller is configured to execute a hydrogen generating mode to generate hydrogen from the hydrogen generating material and a regenerating mode to recover the hydrogen generating ability of the hydrogen generating material. The controller controls the temperature adjustor to heat the hydrogen generating material at a first predetermined temperature during the hydrogen generating mode. The controller controls the temperature adjustor to adjust the temperature of the hydrogen generating material to a second predetermined temperature and controls the water supply to supply water during the regenerating mode.