B01J2219/00033

Method and system for manufacturing ester-based composition

The present disclosure relates to a method for continuously manufacturing an ester-based composition and a manufacturing system therefor, the method improving a manufacturing yield by optimizing process variables of each reactor of a reaction unit in which a plurality of reactors are connected in series.

Liquid process assembly
11590470 · 2023-02-28 · ·

A liquid process assembly, the assembly including a length of pipework, and a reversible pump for selectively reciprocally moving liquid through the pipework.

Integrated processes for producing bis(fluorosulfonyl) imide

A process for producing bis(fluorosulfonyl) imide includes providing a solution comprising fluorosulfonic acid and urea, the solution maintained at a solution temperature from about 0° C. to about 70° C.; reacting the solution in the presence of a reaction medium at a reaction temperature from 80° C. to about 170° C. to produce a product stream including bis(fluorosulfonyl) imide, ammonium fluorosulfate and the reaction medium; separating the ammonium fluorosulfate from the product stream to produce an intermediate product stream; and separating the intermediate product stream into a concentrated product stream and a first recycle stream, the concentrated product stream including a higher concentration of bis(fluorosulfonyl) imide than the first recycle stream.

Apparatus and method for supercritical water oxidation

A supercritical water oxidation vortex reactor has a reactor shell configured to contain a pressurized and heated material including water, a burner assembly configured to create a supercritical core region in the material in the reactor shell, the supercritical core region including water above its critical point, an injector assembly configured to inject into the enclosed volume a subcritical wash stream including water below its critical point and an aspirator arranged in the enclosed volume and configured to remove a processed flow including purified water from an upper portion of the supercritical core region. The supercritical water oxidation vortex reactor is configured with an upward helical flow to transfer precipitated ionic compounds out of the supercritical core region, through a transcritical intermediate region, and into the subcritical wash stream where they re-dissolve.

CONTINUOUS SOLID-STATE POLYMERIZATION PROCESS AND REACTOR COLUMN FOR USE THEREIN
20230054441 · 2023-02-23 ·

The invention relates to a continuous solid-state polymerization process for preparing a polyamide derived from diamine and dicarboxylic acid, wherein the salt is polymerized in a reactor column comprising successive multifunctional zones comprising heating sections and gas-outlet sections, and a residence zone comprising at least one gas-inlet section, wherein the heating sections comprise static heat exchangers. The invention also relates to the reactor column and use thereof in a continuous solid-state polymerization process.

Process for producing trifluoroiodomethane (CF3I) from trifluoroacetic anhydride (TFAA)

The present disclosure relates to a method for producing trifluoroiodomethane (CF.sub.3I) from iodine (I.sub.2) and trifluoroacetic anhydride (TFAA) under photochemical conditions using ultraviolet (UV) light.

PROCESS FOR POLYMERIZING MOLECULAR-WEIGHT CONTROLLED POLYMER

According to an embodiment of the present invention, provided is a process for polymerizing molecular weight—adjustable polymer, comprising: a reactant supply step of supplying a gaseous monomer, a surfactant, and an initiator; a polymerization reaction step of performing a polymerization reaction in which the monomer, the surfactant, and the initiator participate; and a product discharging step of discharging the polymer compound produced by the polymerization reaction, wherein the flow rate of the supplied initiator is inversely proportional to the molecular weight of the polymer compound, and the molecular weight of the polymer compound produced by the polymerization reaction is adjusted by controlling the flow rate of the initiator.

Integrated waste conversion system and method

An entirely water-based, energy self-sufficient, integrated in-line waste management system is provided for comprehensive conversion of all organic fractions of municipal and wider community waste to fuels suitable for use in transportation, with all solid residues converted to high nutrition compost. The system is based on a combination of pre-treatment, involving alkaline hydrolysis and saponification; three-way separation of the pre-treated waste into different streams that are each directed to suitable further processing including fuel production; which includes biodiesel generation in a continuous-flow catalytic esterification unit, and anaerobic digestion to produce methane or other small molecule biofuel. Remaining solids are converted to compost in a quasi-continuous process.

CONTINUOUS, CARBOHYDRATE TO ETHYLENE GLYCOL PROCESSES

By this invention processes are provided for the conversion of carbohydrate to ethylene glycol by retro-aldol catalysis and sequential hydrogenation using control methods having at least one of acetol (hydroxyacetone) and a tracer as inputs.

PROCESS FOR PRECIPITATING A MIXED CARBONATE OR MIXED (OXY)HYDROXIDE
20220340445 · 2022-10-27 ·

Process for precipitating a mixed carbonate or mixed (oxy)hydroxide comprising nickel from an aqueous solution comprising a nickel salt, wherein such process is carried out in a vessel comprising (A) a vessel body, (B) one or more elements selected from draft tubes and guide vanes, (C) at least one stirrer whose pressure zone is in or between element(s) (B), and wherein the process comprises the step of simultaneously adding said solution comprising a nickel salt in or between element(s) (B) and a solution of alkali metal carbonate or hydroxide in or between or outside element(s) (B).