A method of improving the operation of polysilicon fluidized bed reactors is disclosed. The present disclosure is directed to the optimization of axial temperature gradients in gas-solid fluidized bed systems. Varying the width of the particle size distribution in the reactor alters the temperature gradient within the reactor, thereby providing a means of a better control of internal temperature profiles and hence better reactor performance.

Disclosed is a hydrothermal synthesis device for continuously preparing an inorganic slurry using a hydrothermal method. The hydrothermal synthesis device includes a mixer to mix at least one precursor solution for preparing an inorganic material, injected via at least one supply tube, to prepare an intermediate slurry, a connection tube provided at a side of the mixer, continuously discharging the prepared intermediate slurry to a reactor, and having a hydrophobic coating on an inner surface of a portion thereof adjacent to the reactor, and the reactor performing hydrothermal reaction of the intermediate slurry supplied from the connection tube by receiving a liquid stream heated to supercritical or subcritical conditions using a heat exchanger and connected to the connection tube into which the intermediate slurry prepared from the mixer is introduced and to at least one injection tube into which the heated liquid stream is injected.

In accordance with one embodiment, a processing device includes a heated internal wall and a rotating rod positioned within an interior space formed by the heated internal wall. The rotating rod may be hollow and act as an internal heat exchanger. The processing device also includes a plurality of baffles spaced apart from one another along the rotating rod and extending away from the rotating rod towards the heated internal wall. The processing device also includes at least one wiper or roller coupled to an edge of at least one of the plurality of baffles or porous, packed basket, coupled to the rotating rod and that contacts the heated internal wall while rotating together with the rotating rod. In another embodiment, a processing device may be used to adsorb reactive gases into a liquid phase while heat is exchanged.

An apparatus (10) for preparation of acetylene and synthesis gas by partial oxidation of hydrocarbons with oxygen is proposed, comprising a reactor (12). The reactor (12) has a burner block (14) with a firing space for acetylene preparation, a secondary space (18) formed within the burner block (14), and an annular space (20) surrounding the secondary space (18). The burner block (14) has holes (22) for supply of a stream of a mixture of hydrocarbons and oxygen to the firing space and holes (24) for supply of a stream of auxiliary oxygen to the firing space. The holes (24) for supply of a stream of auxiliary oxygen to the firing space are connected to the secondary space (18). The secondary space (18) is connected to the annular space (20). There is a further proposal of a process for preparing acetylene and synthesis gas by partial oxidation of hydrocarbons with oxygen.

The present disclosure provides an apparatus for preparing oligomer including: a reactor; a gas-liquid separator; a solvent transfer line; a second transfer line; a first spray nozzle unit; and a second spray nozzle unit. The apparatus is capable of improving stability of the entire process by including a first spray nozzle unit and a second spray nozzle unit in a reactor and thus preventing by-products containing polymer substances such as C20+ from being entrained with a desired product during a reaction.

The present disclosure provides a reactor cleaning apparatus including: a fixing part having a partial region inserted into a hole formed in an upper portion of a reactor to be coupled to the reactor and fixing a pipe; the pipe inserted into a hole formed in the fixing part, protruding downward from the fixing part, and having a length adjustable in a vertical direction; a spray nozzle provided at a lower end of the pipe; and a screener provided on a lower side surface of the pipe, and a reactor cleaning method using the same.

The present invention provides a weir quench, an apparatus utilizing the weir quench and processes incorporating the same. The weir quench incorporates an inlet having an inner diameter (Di) and an upper chamber having an inner diameter (Duc), wherein the inlet inner diameter (Di) is at least 90% of the upper chamber inner diameter (Duc). The apparatus constitutes a reactor having an outlet with an inner diameter fluidly coupled with the weir quench inlet, wherein the ratio of the reactor oulet inner diameter (Dr) to the weir quench inlet diameter (Di) is greater than one. The weir quench, and apparatus are advantageously utilized in processes utilizing a limiting reagent.

Methods and systems for using temperature measurements taken from a compact insulated skin thermowell to optimize a pyrolysis reaction are provided. In the present systems and methods, the upstream temperature and the upstream pressure of a pyrolysis reactor is measured through an adiabatic restriction in the inlet manifold of a parallel tube assembly to provide an absolute upstream temperature and an upstream pressure. The downstream temperature of the pyrolysis reactor is also measured following an adiabatic restriction to provide an absolute downstream temperature. The downstream pressure is then determined by multiplying the absolute upstream pressure with the quotient of the downstream temperature divided by the upstream temperature as taken to the power of k/k−1, where k is the ratio of fluid specific heat at constant pressure (Cp) to fluid specific heat at constant volume (Cv).

A catalytic reactor comprises a particle separator the reactor internals by means which makes the fluid flow stream perform a radial outwards and upwards S-curve flow path, which enables the particles to be extracted and settle in a collection section with low flow activity and turbulence.

Techniques are provided for seal flush systems. A system may include a reactor circulation pump configured to circulate a slurry through a polymerization reactor. The slurry may include an olefin monomer, a catalyst, and a diluent. The system may also include a catalyst-inhibiting additive system configured to supply a catalyst-inhibiting additive to a seal of the reactor circulation pump and a seal flush system configured to generate a seal flush mixture and supply the seal flush mixture to the seal of the reactor circulation pump.