A glass lined reaction tank for chemical and pharmaceutical industries and a manufacturing method thereof. One-step molding technical standards for manufacturing iron blanks of the glass lined reaction tanks are deeply developed, an overall structure of a flanged big flange of a tank body and a tank cover matching with the tank body are innovated, and nominal pressure of the big flange and the sealing performance of a tank mouth are perfectly improved. By using a new structurally-combined precise controlled internal heating type electric furnace and an intelligent temperature program control/adjustment/recording instrument, heating temperature of an overall glass lining layer on an inner wall of the tank body is more accurately controlled to be the same, and a synchronous, integral and controlled sintering core technique is realized.

A method for heating or cooling a carbon containing reducing gas having a carbon monoxide content of at least 0.5 vol %, wherein the gas is heated to a temperature of at least 400 C. or wherein the gas is cooled from a temperature exceeding 400 C., wherein the gas is passed along a surface of a heating or cooling unit having a heat conductive metal or metal alloy body and a protective layer, which protective layer provides said surface, and which protective layer is made from a coating composition including colloidal amorphous silicate and crystalline oxide particles.

The present invention relates, in general, to the purification of boron trichloride (BCl.sub.3). More particularly, the invention relates to a process for minimizing silicon tetrachloride (SiCl.sub.4) formation in BCl.sub.3 production and/or the removal of SiCl.sub.4 in BCl.sub.3 product stream by preventing/minimizing the silicon source in the reaction chambers. In addition, a hydride material may be used to convert any SiCl.sub.4 present to SiH.sub.4 which is easier to remove. Lastly freeze separation would replace fractional distillation to remove SiCl.sub.4 from BCl.sub.3 that has been partially purified to remove light boilers.

The invention discloses a glass lined metal micro-reactor with enhanced heat transfer efficiency in continuous flow operation. More particularly, the invention discloses a glass lined micro-reactor that can be reassembled. The invention provides a novel glass lined metal micro-reactor with micro fluidic channels that provide a better mixing, better heat exchange, and better temperature control. The micro fluidic channels machined in the glass lined metal reactor/mixer may be straight, curved, lamellar, flower shaped, or spiral such that the cross sectional area of the micro fluidic channel is configured to suit the cross sectional area of the micro-reactor.

The present disclosure relates to a method and an apparatus for manufacturing a core-shell catalyst, and more particularly, to a method and an apparatus for manufacturing a core-shell catalyst, in which a particle in the form of a core-shell in which the metal nanoparticle is coated with platinum is manufactured by substituting copper and platinum through a method of manufacturing a metal nanoparticle by emitting a laser beam to a metal ingot, and providing a particular electric potential value, and as a result, it is possible to continuously produce nanoscale uniform core-shell catalysts in large quantities.

A glass lined reaction tank for chemical and pharmaceutical industries and a manufacturing method thereof. One-step molding technical standards for manufacturing iron blanks of the glass lined reaction tanks are deeply developed, an overall structure of a flanged big flange of a tank body and a tank cover matching with the tank body are innovated, and nominal pressure of the big flange and the sealing performance of a tank mouth are perfectly improved. By using a new structurally-combined precise controlled internal heating type electric furnace and an intelligent temperature program control/adjustment/recording instrument, heating temperature of an overall glass lining layer on an inner wall of the tank body is more accurately controlled to be the same, and a synchronous, integral and controlled sintering core technique is realized.

The present invention relates to a fluidized bed reactor, comprising a reaction tube, a distributor and a heating device, the reaction tube and the distributor at the bottom of the reaction tube composing a closed space, the distributor comprising a gas inlet and a product outlet, and the reaction tube comprising a tail gas outlet and a seed inlet at the top or upper part respectively, characterized in that the reaction tube comprises a reaction inner tube and a reaction outer tube, and the heating device is an induction heating device placed within a hollow cavity formed between the external wall of the reaction inner tube and the internal wall of the reaction outer tube, wherein the hollow cavity is filled with hydrogen, nitrogen or inert gas for protection, and is able to maintain a pressure of about 0.01 to about 5 MPa; and also to a process of producing high purity granular polysilicon using the reactor. The fluidized bed reactor according to the present invention uses induction heating to heat directly the silicon particles inside the reaction chamber, such that the temperature of the reaction tube is lower than that inside the reaction chamber, which accordingly avoids deposition on the tube wall and results in more uniform heating, and thus is useful for large diameter fluidized bed reactors with much increased output for a single reactor.

Disclosed is a hydrothermal synthesis device for continuously preparing an inorganic slurry using a hydrothermal method. The hydrothermal synthesis device includes a mixer to mix at least one precursor solution for preparing an inorganic material, injected via at least one supply tube, to prepare an intermediate slurry, a connection tube provided at a side of the mixer, continuously discharging the prepared intermediate slurry to a reactor, and having an inner surface contacting a precursor solution mixture on which abrasive polishing has been performed, and the reactor performing hydrothermal reaction of the intermediate slurry supplied from the connection tube by receiving a liquid stream heated to supercritical or subcritical conditions using a heat exchanger and connected to the connection tube into which the intermediate slurry prepared from the mixer is introduced and to at least one injection tube into which the heated liquid stream is injected.

An apparatus for producing a mixed solution, comprising a mixing vessel for preparing an aqueous mixed solution containing a dicarboxylic acid and an Nb compound and a filter for the aqueous mixed solution connected to the mixing vessel via a pipe, the mixing vessel being anticorrosive and equipped with a stirring unit, a heating unit and a cooling unit for the aqueous mixed solution, wherein the aqueous mixed solution prepared in the mixing vessel is fed to the filter via the pipe and filtered in the filter under increased pressure.

A small reactor, which contains an inorganic transparent substrate, which contains: a reaction channel configured to allow a chemical reaction to proceed therein; a supply channel, which is connected to one end of the reaction channel, and is configured to supply samples to be reacted in the reaction channel; and a discharge channel, which is connected to the other end of the reaction channel, and is configured to discharge a reaction product from the reaction channel, wherein the inorganic transparent substrate is in the shape of an arc-shaped curve.