Methods for treating cellulosic materials comprising introducing a liquid treating composition into the cellulosic material, the treating composition comprising a solution prepared from at least: (i) one or more of a copper amine complex or copper ammine complex, such as copper tetraamine carbonate, (ii) one or more of ammonia or a water-soluble amine and (iii) water; and exposing the cellulosic material provided thereby to carbon dioxide and/or carbonic acid to provide treated cellulosic material, and treated cellulosic materials prepared thereby.

Methods for treating cellulosic materials comprising introducing a liquid treating composition into the cellulosic material, the treating composition comprising a solution prepared from at least: (i) one or more of a copper amine complex or copper ammine complex, such as copper tetraamine carbonate, (ii) one or more of ammonia or a water-soluble amine and (iii) water; and exposing the cellulosic material provided thereby to carbon dioxide and/or carbonic acid to provide treated cellulosic material, and treated cellulosic materials prepared thereby.

A treatment process and wood products thereof including a product formulation of a single phase solution combining a wood preservative (durable component) with a Flame Retardant component (FR) to produce a durable Flame Retardant (dFR) treated wood product. The durable component comprises a range of copper based and non-copper based wood preservatives, while the FR component comprises alkali metal silicates and alkali metal aluminate compounds. The dFR working solution undergoes chemical impregnation (treatment) followed by a heat (fixation) process step that locks the chemical into the wood making it non-leachable. The dFR treated wood products are tested for their enhanced fire performance properties. When heated, wood undergoes thermal degradation and combustion producing gases, vapors, tars and chars. Using a cone calorimeter burn test method, dFR treated wood products show a significant reduction in heat release rate, mass loss rate and smoke generated values compared to untreated radiate pine.

Disclosed is a method of purification of utilized acetylation fluid recovered from a process of acetylating wood. The method involves subjecting the recovered acetylation fluid to cooling crystallization. By this method terpene and terpenoid impurities are removed, as well as other impurities. Disclosed is also a method of acetylating wood resulting in acetylated wood and utilized acetylation fluid comprising acetic acid, and purifying the utilized acetylation fluid by cooling crystallization.

Production method for modified lignocellulose materials. The present invention relates to a production method for modified lignocellulose materials, comprising the impregnation of a lignocellulose material, especially wood, with a solution of an acid and an alcohol as well as treatment of the material with superheated steam at elevated temperatures.

Method of treating wood products to improve fire resistance thereof. The method comprises treating wet wood objects with compositions comprising an aqueous solution of bisphosphonate selected from 1-hydroxyethane 1,1-diphosphonic acid, an alkanol amine, and optionally an alkaline agent, the composition having a pH in the range of 4.0 to 7.0 to impregnate the object with the compositions, and subjecting the object so obtained to drying to achieve aspiration of the pits of the wood object. The method can be used for protecting wood not only against fire but also against mould, rot, blue stain, insect such as termite attacks on wood, dimensional changes, or a combination thereof due to environmental influence.

A treatment process and wood products thereof including a product formulation of a single phase solution combining a wood preservative (durable component) with a Flame Retardant component (FR) to produce a durable Flame Retardant (dFR) treated wood product. The durable component comprises a range of copper based and non-copper based wood preservatives, while the FR component comprises alkali metal silicates and alkali metal aluminate compounds. The dFR working solution undergoes chemical impregnation (treatment) followed by a heat (fixation) process step that locks the chemical into the wood making it non-leachable. The dFR treated wood products are tested for their enhanced fire performance properties. When heated, wood undergoes thermal degradation and combustion producing gases, vapors, tars and chars. Using a cone calorimeter burn test method, dFR treated wood products show a significant reduction in heat release rate, mass loss rate and smoke generated values compared to untreated radiate pine.

A method for reinforcing and enhancing bamboo/wood materials employs a sulfuric acid hydrolysis method to prepare a nanocellulose dispersion solution; then with the nanocellulose dispersion solution having a certain concentration as a precursor, nano zinc oxide is in-situ produced on the surface of the nanocellulose; and the cellulose dispersion solution is improved by compounding. The obtained treatment solution is impregnated into the pores of bamboo/wood materials in a specific manner to play the role of filling, binding and consolidating the bamboo/wood tissues, so that the treated bamboo/wood materials have enhanced hardness, strength and dimension stability, and significantly-improved mildew- and corrosion-resistance. The method is suitable for the reinforcing and enhancing treatment of wood materials with relatively-loose texture, such as fast-growing wood and wood from a planted forest, and is also suitable for the reinforcement and restoration of slightly-rotten wood materials.

A method for improving the fire resistance of a cellulose material comprises mixing boric acid with methanol to form a boric acid ester, combining the borate ester with magnesium sulfate to form a low viscosity magnesium borate sulfate solution, treating the cellulose material with the magnesium borate sulfate solution, and heating the treated cellulose material to evaporate remaining alcohol and solvent to form a crystals of a complex mixture containing combinations of magnesium sulfate, boric acid, magnesium borate, magnesium borate sulfate and their hydrates.

A wood treatment method for reducing fungal growth utilizes a treatment solution comprising an aldehyde, a carrier solvent, an organic co-solvent, at least one surfactant, and at least one acid, base, or salt. In embodiments, the carrier solvent may comprise water and the organic co-solvent may comprise an alcohol or acetone. The aldehyde is impregnated into the wood, where it reacts with thiamine and other amino acids to promote cross-linking, reducing the porosity of the wood and thereby reducing the ability of various microbes and fungi to access the interior of the wood as a nutrient source.