An instrument and method for high pressure microwave assisted chemistry are disclosed. The method includes the steps of applying microwave radiation to a sample in a sealed vessel while measuring the temperature of the sample and measuring the pressure generated inside the vessel and until the measured pressure reaches a designated set point, opening the vessel to release gases until the pressure inside the vessel reaches a lower designated set point, closing the vessel, and repeating the steps of opening the vessel at designated pressure set points and closing the vessel at designated pressure set points to the sample until the sample reaction reaches a designated high temperature. The designated set points can controllably differ from one another as the reaction proceeds. Microwave energy can be applied continuously or intermittently during the opening and closing steps. The apparatus includes a microwave cavity, a microwave transparent pressure resistant reaction vessel in the cavity, a cap on the reaction vessel, a pressure sensor for measuring pressure in the vessel, a temperature sensor, and means for opening and closing the cap at predetermined pressure set points measured by the pressure sensor to release pressure from the vessel.

Microwave chemical processing system having a microwave plasma reactor, and a multi-stage gas-solid separation system are disclosed. The microwave energy source has a waveguide, a reaction zone, and an inlet configured to receive the input material, and the input material is converted into separated components. The separated components include hydrogen gas and carbon particles. The multi-stage gas-solid separation system has a first cyclone separator to filter the carbon particles from the separated components, and a back-pulse filter system coupled to the output of the first cycle separator to filter the carbon particles from the output from the first cyclone separator.

A system and method are provided for the separation of hydrogen from natural gas feedstock to form hydrocarbon radicals. Aspects of the system include perpendicular magnetic and electric fields, a method of radical formation that separates hydrogen from the reaction process, and a separation method based on centrifugal forces and phase transitions. The gases rotate in the chamber due to the Lorentz force without any mechanical motion. Rotation separates gases and liquids by centrifugal force. The lighter species are collected from the mid region endpoint of the apparatus and fed back for further reaction. A new concept of controlled turbulence is introduced to mix various species. A novel magnetic field device is introduced comprised of two specially magnetized cylinders. A novel control of temperatures, pressures, electron densities and profiles by, RF, microwaves, UV and rotation frequency are possible especially when atomic, molecular, cyclotron resonances are taken into account. The electrodes can be coated with catalysts; the entire apparatus can be used as a new type of chemical reactor.

A device for producing a tetrahydroborate, the device including a reaction chamber inside which a hydrogen plasma is generated, a sample stage which is provided in the reaction chamber and on which a borate is placed, and a hydrogen ion shielding member which is provided to cover at least some of the borate to be placed.

Provided are methods for preparing hydrogen and solid carbon. Illustrative methods comprise providing a feedstock comprising gaseous hydrocarbons to a microwave-inert reaction vessel and/or a radio wave-inert reaction vessel. The reaction vessel has solid carbon, about 0% water and about 0% molecular oxygen inside the reaction vessel and the carbon inside the reaction vessel is operable to heat the feedstock comprising gaseous hydrocarbons. The carbon is then exposed to microwaves and/or radio waves until the solid carbon is at a temperature of at least 1200 Kelvin, thereby forming hydrogen and solid carbon. Once formed, the hydrogen and solid carbon are separated.

A fluid treatment device with a new configuration is provided. The fluid treatment device is provided with an upstream treatment unit defined by treatment surfaces that rotate relative to each other, and a downstream treatment unit arranged downstream of the upstream treatment unit. The upstream treatment unit is configured such that, by passing the fluid to be treated into an upstream treatment space defined by the treatment surfaces, the fluid to be treated is subjected to upstream treatment. The downstream treatment unit is provided with a downstream treatment space which performs the function of retaining and mixing the fluid to be treated by means of a labyrinth seal. An upstream outlet of the fluid to be treated from the upstream treatment unit opens into the downstream treatment space, and the downstream treatment space is configured to use the labyrinth seal to perform the function of controlling retention time. The downstream treatment space is provided with narrow seal spaces, and retention spaces arranged upstream of the seal spaces and wider than the seal spaces, and the upstream outlet opens to a retention space.

A photochemical reactor (1) having a hollow container body (10) having a side wall (11) made of a material arranged to contain an excited luminous plasma with electromagnetic fields and defining a closed excitation chamber (12) in which, in use, an excitable material (15) is present in such a way to obtain a discharge of the excited luminous plasma by microwave irradiation. The hollow container body (10) is provided with at least a hollow (20) that protrudes into the excitation chamber (12) and at least a microwave radiation source positioned, in use, in the hollow (20), and arranged to emit radiations in such a way to excite the excitable material (15) producing a luminous plasma.

The present invention provides a hybrid reforming system for producing syngas through a reforming reaction between carbon dioxide plasma and a hydrocarbon material, the system comprising: a carbon dioxide feeder (110) which feeds carbon dioxide; a hydrocarbon material feeder (120) which feeds the hydrocarbon material; a plasma reformer (200) which respectively receives carbon dioxide and the hydrocarbon material from the carbon dioxide feeder (110) and the hydrocarbon material feeder (120), and produces primary syngas through a reforming reaction while producing the carbon dioxide plasma using electromagnetic waves; a wet carbon-refining device (130) which is arranged at a gas exhaust end of the plasma reformer (200) and filters and refines carbon contained in the primary syngas; and a catalyst dry-reformer (140) which is arranged at a gas exhaust end of the wet carbon-refining device (130) and produces secondary syngas by making the refined syngas undergo a catalyst dry-reforming reaction.

An apparatus for forming diamond, which contains a reaction chamber, means for providing tetrahedranoidal reactant molecules to the reaction chamber; and means for providing single carbon atoms in the reaction chamber to provide for reaction between the single carbon atoms and tetrahedranoidal reactant molecules.

A system for converting hydrocarbon materials into a product includes a hydrocarbon feedstock source, a process gas source, an energy generator, and a cylindrical reaction chamber. The reaction chamber has a conductive inner surface that forms a resonant cavity. The resonant cavity is configured to support a standing TM010 electromagnetic wave. The reaction chamber is also configured to receive feedstock from the feedstock source, process gas from the process gas source, and convert the feedstock into a product stream in the presence of the TM010 electromagnetic wave.