B01J19/126

Large capacity natural material composition conversion apparatus using microwave with preset pressure function

A large capacity natural material composition conversion apparatus using a microwave with a preset pressure function includes a chamber including a sealed reaction space accommodating a material, an radiator configured to heat the material by radiating a microwave into the reaction space, a pressure regulator configured to regulate a pressure of the reaction space by supplying a gas into the reaction space, and a controller configured to control the pressure regulator and the radiator, and preliminarily increase a pressure of the reaction space by controlling the pressure regulator before heating the material.

MICROWAVE TREATMENT APPARATUS AND METHOD FOR PRODUCING CARBON FIBER

Provided is a microwave treatment apparatus that can properly treat a treatment target using microwaves. The apparatus includes: a vessel 10 in which a treatment target 2 is arranged; a microwave irradiating unit 20 that irradiates an internal portion of the vessel 10 with microwaves; and heat generating member 30 that is provided inside the vessel 10 along the treatment target 2, generates heat by absorbing part of microwaves used for irradiation by the microwave irradiating unit 20, and transmits part of the microwaves. The microwave irradiating unit 20 irradiates a portion in which the heat generating member 30 is provided with microwaves, thereby heating the treatment target 2 from the outside through heat generation at the heat generating member 30, and directly heating the treatment target 2 with microwaves transmitted through the heat generating member 30.

COMPLEX MODALITY REACTOR FOR MATERIALS PRODUCTION AND SYNTHESIS
20230201788 · 2023-06-29 · ·

A system for producing carbonaceous materials is disclosed that includes an energy source configured to emit microwave energy and a plasma reactor coupled to receive the microwave energy and configured to produce plasma in response to exposure of one or more process gases to the microwave energy. In some instances, the plasma reactor includes a first chamber having a rectangular cross-section and configured to receive the microwave energy from the energy source as sinusoidal waveform, a second chamber having a cylindrical cross-section and configured to receive microwave energy from the first chamber as a radial waveform having an energy maxima at a radial center of the cylindrical cross-section, the second chamber including an opening to receive one or more process gases and configured to ignite a plasma plume, and a gas-solid separator configured to separate solid materials from the plasma plume.

Biomass Direct Reduced Iron
20230203606 · 2023-06-29 ·

A process for producing direct reduced iron (“DRI”) from iron ore and biomass in a single stage fluidised bed includes injecting (a) iron ore, (b) gaseous oxygen and (c) a solid reductant including biomass into a reaction zone of the fluidized bed operating in a temperature range of 750-850#C and reducing iron ore and forming DRI in the fluidized bed and discharging DRI having a metallisation of at least 70% from the fluidised bed.

METHODS FOR PREPARING HYDROGEN AND SOLID CARBON FROM A GASEOUS HYDROCARBON SOURCE USING MICROWAVES AND/OR RADIO WAVES
20230202839 · 2023-06-29 ·

Provided are methods for preparing hydrogen and solid carbon. Illustrative methods comprise providing a feedstock comprising gaseous hydrocarbons to a microwave-inert reaction vessel and/or a radio wave-inert reaction vessel. The reaction vessel has solid carbon, about 0% water and about 0% molecular oxygen inside the reaction vessel and the carbon inside the reaction vessel is operable to heat the feedstock comprising gaseous hydrocarbons. The carbon is then exposed to microwaves and/or radio waves until the solid carbon is at a temperature of at least 1200 Kelvin, thereby forming hydrogen and solid carbon. Once formed, the hydrogen and solid carbon are separated.

Method for preparing sea urchin-shaped zinc oxide nanowire
11685665 · 2023-06-27 ·

According to an embodiment, a method for preparing a sea urchin-shaped zinc oxide (ZnO) nanowire comprises preparing a mixture of a ZnO nano-powder and a graphite powder and irradiating the mixture, in a container, with a microwave.

SYSTEM AND METHOD FOR PREPARING CARBON NANOFIBER AND HYDROGEN THROUGH CONTINUOUS MICROWAVE PYROLYSIS
20230192490 · 2023-06-22 ·

The present disclosure relates to a system and a method for preparing carbon nanofiber and hydrogen through continuous microwave pyrolysis. The system includes four apparatus. The melting and feeding apparatus is to heat and melt feedstocks. The microwave pyrolysis apparatus is for catalytic pyrolysis and includes a feedstock inlet, a gas outlet and a carbon outlet. The gas purification and utilization apparatus is for hydrogen purification and residual gas separation, The power generation apparatus includes a generator and a small internal combustion engine utilizing residual gas as fuel, and the generated smoke is conveyed to the melting and feeding apparatus for feedstocks melting. According to the present disclosure, a poly-generation system for co-producing high-performance carbon materials and hydrogen through plastic wastes with greatly increased energy utilization rate is formed to solve the technical problems of low product yield and high energy consumption in traditional pyrolysis.

Device and process for producing undecylenic acid methyl ester using methyl ricinoleate as raw material

A device and a process for producing undecylenic acid methyl ester using methyl ricinoleate as raw material are provided. The device comprises a feed pump, a raw material pre-heater, a microwave catalytic reactor, a microwave generator, a temperature controller and an infrared sensor, a condenser, a product tank and a discharge pump. The feed pump is connected with the raw material pre-heater, which is connected with the inlet of the microwave catalytic reactor. The outlet of the microwave catalytic reactor is connected with the condenser, which is connected to the product tank and the discharge pump. The microwave catalytic reactor is located in the microwave generator, which is connected with the temperature controller and the infrared sensor. The process is as follows: high-purity methyl ricinoleate, used as the raw material, is converted to methyl undecene and heptaldehyde by microwave-assisted pyrolysis process, followed by isolation and purification to produce methyl undecene.

Engineered feed process in catalytic cracking, simultaneus radicalization of hydrogen gas aided by electromagnetic waves to convert natural and synthetic hydrocarbon waste into gasoline and gas oil

A method and process of producing gasoline and diesel from hydrocarbon wastes, by gradually heating the hydrocarbon waste in a reducing atmosphere, up to 550° C. During the heating process and at various temperature points long chains of hydrocarbon are broken down into smaller hydrocarbon chains. During the heating process radical hydrogen gas is introduced to the reactor where the radical hydrogen gas reacts with smaller hydrocarbon chains to produce 45% coke petroleum oil, 45% liquid hydrocarbons composed of gasoline and gasoil and 10% gases including methane, ethane, propane and steam. The radicalized hydrogen atoms are produced at low temperatures and atmospheric pressure. Hydrogen gas is produced by dissolving aluminum scraps are dissolved in a sodium hydroxide solution in a reactor. As hydrogen gas is produced the reactor is heated to 120° C. in the presence of electromagnetic waves causing the breakdown of hydrogen gas into hydrogen gas radicals.

Methods and Systems for Microwave Assisted Production of Graphitic Materials
20220371896 · 2022-11-24 ·

Systems and methods for plasma based synthesis of graphitic materials. The system includes a plasma forming zone configured to generate a plasma from radio-frequency radiation, an interface element configured to transmit the plasma from the plasma forming zone to a reaction zone, and the reaction zone configured to receive the plasma. The reaction zone is further configured to receive feedstock material comprising a carbon containing species, and convert the feedstock material to a product comprising the graphitic materials in presence of the plasma.