The present invention provides a plasma treatment detection indicator including a color-changing layer that changes color by plasma treatment, exhibiting excellent heat resistance, with the gasification of the color-changing layer or the scattering of the fine debris of the color-changing layer caused by the plasma treatment being suppressed to the extent that electronic device properties are not affected. Specifically, the present invention provides a plasma treatment detection indicator comprising a color-changing layer that changes color by plasma treatment, the color-changing layer comprising metal oxide fine particles containing at least one element selected from the group consisting of Mo, W, Sn, V, Ce, Te, and Bi, the metal oxide fine particles having a mean particle size of 50 μm or less.

Nanocrystalline metal powders comprising tungsten, molybdenum, rhenium and/or niobium can be synthesized using a combustion reaction. Methods for synthesizing the nanocrystalline metal powders are characterized by forming a combustion synthesis solution by dissolving in water an oxidizer, a fuel, and a base-soluble, ammonium precursor of tungsten, molybdenum, rhenium, or niobium in amounts that yield a stoichiometric burn when combusted. The combustion synthesis solution is then heated to a temperature sufficient to substantially remove water and to initiate a self-sustaining combustion reaction. The resulting powder can be subsequently reduced to metal form by heating in a reducing gas environment.

Nanocrystalline metal powders comprising tungsten, molybdenum, rhenium and/or niobium can be synthesized using a combustion reaction. Methods for synthesizing the nanocrystalline metal powders are characterized by forming a combustion synthesis solution by dissolving in water an oxidizer, a fuel, and a base-soluble, ammonium precursor of tungsten, molybdenum, rhenium, or niobium in amounts that yield a stoichiometric burn when combusted. The combustion synthesis solution is then heated to a temperature sufficient to substantially remove water and to initiate a self-sustaining combustion reaction. The resulting powder can be subsequently reduced to metal form by heating in a reducing gas environment.

Disclosed are an electrode active material for lithium secondary batteries, comprising at least one selected from compounds represented by the following formula 1, and a lithium secondary battery comprising the same.
Li.sub.xMo.sub.4−yM.sub.yO.sub.6−zA.sub.z  (1) wherein 0≦x≦2, 0≦y≦0.5, 0≦z≦0.5, M is a metal or transition metal cation having an oxidation number of +2 to +4, and A is a negative monovalent or negative bivalent anion.

Disclosed are an electrode active material for lithium secondary batteries, comprising at least one selected from compounds represented by the following formula 1, and a lithium secondary battery comprising the same.
Li.sub.xMo.sub.4−yM.sub.yO.sub.6−zA.sub.z  (1) wherein 0≦x≦2, 0≦y≦0.5, 0≦z≦0.5, M is a metal or transition metal cation having an oxidation number of +2 to +4, and A is a negative monovalent or negative bivalent anion.

The present specification relates to a preparation method for rod-shaped molybdenum oxide and a preparation method for a molybdenum oxide composite, the preparation method for rod-shaped molybdenum oxide according to the present invention may be carried out under low temperature and pressure conditions, and thus has an advantage in that it is possible to mass produce rod-shaped molybdenum oxide, and the preparation method for a molybdenum oxide composite according to the present invention has an advantage in that the molybdenum oxide composite may be synthesized at a temperature which is equal to or less than the boiling point of ethanol, and the amount of an ethanol solvent used is reduced.

The present specification relates to a preparation method for rod-shaped molybdenum oxide and a preparation method for a molybdenum oxide composite, the preparation method for rod-shaped molybdenum oxide according to the present invention may be carried out under low temperature and pressure conditions, and thus has an advantage in that it is possible to mass produce rod-shaped molybdenum oxide, and the preparation method for a molybdenum oxide composite according to the present invention has an advantage in that the molybdenum oxide composite may be synthesized at a temperature which is equal to or less than the boiling point of ethanol, and the amount of an ethanol solvent used is reduced.

The present invention relates to a method for preparing uniform metal oxide nanoparticles. According to the preparation method of the present invention, it is possible to maintain the temperature and pressure inside the reactor in a stable and constant manner by removing water generated in the reaction step for forming metal oxide nanoparticles. Thus, the uniformity of nanoparticles formed is increased, and the reproducibility between batches can be increased even in a repeated process and and a large-scale reaction. Therefore, the preparation method of the present invention can be used to synthesize uniform nanoparticles reproducibly in large quantities.

The present invention provides an ink composition for forming a color-changing layer that changes color by plasma treatment, the ink composition exhibiting excellent heat resistance, with the gasification of the color-changing layer or the scattering of the fine debris of the color-changing layer caused by plasma treatment being suppressed to the extent that electronic device properties are not affected. The invention provides an ink composition for forming a color-changing layer that changes color by plasma treatment, the ink composition comprising metal oxide particles containing at least one element selected from the group consisting of Mo, W, Sn, V, Ce, Te, and Bi, and a binder resin.

The invention relates to a class of electrochemical energy storage materials and a preparation method and application thereof. A porous metal oxide-based electrochemical energy storage material at least comprises a host metal oxide with a hierarchical pore structure; wherein, the host metal oxide is a single crystal, quasicrystal, or twin crystal structure with ordered atomic lattice arrangement, the crystal is rich in oxygen atom vacancy defects, the structural general formula is M.sub.xO.sub.y−z, wherein M is selected from one or more combinations of niobium element, molybdenum element, titanium element, vanadium element, manganese element, iron element, cobalt element, nickel element, copper element, zinc element, tungsten element, tantalum element, and zirconium element; and 1≤x≤2, 1≤y≤5, and 0.1≤z≤0.9, preferably Nb.sub.2O.sub.5−z.