C03C1/006

Spherical silicon oxycarbide particle material and manufacturing method thereof
10179737 · 2019-01-15 · ·

Provided are spherical silicon oxycarbide particle material and manufacturing method thereof, wherein the average particle size is in the range of 0.1-100 m and having a sphericity of 0.95-1.0. Spherical silicon oxycarbide particle material and manufacturing method thereof are provided as follows. Organotrialkoxysilane is hydrolyzed in a pH 3-6 acetic acid aqueous solution, thereafter an alkaline aqueous solution such as a pH 7-12 ammonia water was added to the obtained hydrolysate. The condensation reaction is performed in an alkaline range to form spherical polysilsesquioxane particles that are spherical silicon oxycarbide precursors that has no melting point or softening point. Sintering was then performed at a sintering temperature of 600-1400 C. under inert atmosphere to obtain spherical silicon oxycarbide particle material.

CONTINUOUS SOL-GEL METHOD FOR PRODUCING QUARTZ GLASS

The invention relates to a continuous sol-gel method for producing quartz glass, comprising the following steps: (a) continuously metering a silicon alkoxide into a first reactor (R1) and carrying out an at least partial hydrolysis process by adding an aqueous mineral acid, thereby obtaining a first product flow (A); (b) continuously producing an aqueous silicic acid dispersion by continuously mixing water and silicic acid in a second reactor, thereby obtaining a second product flow (B); (c) continuously mixing the product flows (A) and (B) in a third reactor (R3) in order to produce a pre-sol, thereby obtaining a third product flow (C); (d) continuously adding an aqueous base to the product flow (C), thereby obtaining a sol; (e) continuously filling the exiting sol into moulds, thereby obtaining an aquagel; (f) drying the aquagel, thereby obtaining xerogels; and (g) sintering the xerogels, thereby obtaining quartz glass, with the proviso that at least one of the steps (a) to (e) additionally includes a degassing process of at least one feed material used in the step.

WATER SOLVATED GLASS/AMORPHOUS SOLID IONIC CONDUCTORS

The disclosure provides a water-solvated glass/amorphous solid that is an ionic conductor-an electronic insulator, and a dielectric as well as electrochemical devices and processes that use this material, such as batteries, including rechargeable batteries, fuel cells, capacitors, electrolysis cells, and electronic devices. The electrochemical devices and products use a combination of ionic and electronic conduction as well as internal electric dipoles.

Foamed glass beads and process of making same
12103887 · 2024-10-01 · ·

Foamed glass beads can be made from glass, a hydrated foaming agent, a hydrated binding agent, a sealing agent, a fluxing agent, and a solvent. The hydrated binding agent can hold the glass and the hydrated foaming agent in solution. The glass can be derived from glass cullet that is ground into powder. The glass powder, the hydrated foaming agent, the hydrated binding agent, the sealing agent, the fluxing agent, and the solvent can be mixed together to create a preform material that is pelletized to make preform pellets. The preform pellets can be dried and then heated to a predetermined temperature. The heating process can create the final, foamed glass beads.

POLYPHOSPHATE GLASS MICROSPHERES, METHODS OF MAKING AND USES THEREOF
20180265402 · 2018-09-20 ·

Polyphosphate glass microspheres (PGMs) are prepared using a polyphosphate coacervate. PGMs can be loaded with various therapeutic agents and can be used for various medical and dental procedures and treatments.

Method for producing sulfide solid electrolyte

A method for producing a sulfide glass ceramic, including reacting a lithium compound, a phosphorus compound and a halogen compound in a solvent that contains a hydrocarbon and an ether compound to produce a sulfide glass that contains a Li element, a P element, a S element and one or more halogen elements, and heating the sulfide glass to produce a sulfide glass ceramic.

CONTROLLED RELEASE SOLID SCALE INHIBITORS
20180179434 · 2018-06-28 ·

Compositions and methods of preparation and use for controlled release solid scale inhibitors used in hydraulic fracturing operations in oil and gas wells. The controlled release scale inhibitors comprise amorphous glass which is a reaction product of a phosphorus-containing compound, a calcium-containing compound, a magnesium-containing compound and base. The composition has a predetermined dissolution rate for controlled release of scale inhibitors in induced hydraulic fractures in hydraulic fracturing treatment of oil or gas wells.

METHOD FOR PRODUCING OPAQUE QUARTZ GLASS, AND BLANK MADE FROM THE OPAQUE QUARTZ GLASS

In one method for producing opaque quartz glass, a green body is produced from a slip containing fine, amorphous SiO.sub.2 particles and coarse SiO.sub.2 reinforcement bodies and the green body is sintered by way of a sintering treatment into a blank made from the opaque quartz glass. The reinforcement bodies with a specific density D.sub.K1 are here embedded in a SiO.sub.2 matrix with a specific glass density D.sub.M. Starting from this, in order to provide a blank of opaque quartz glass that is less susceptible to cracking and illustrates homogeneous transmission even in the case of small wall thicknesses, in one aspect sinterable reinforcement bodies are used, the specific density D.sub.K0 of which prior to the sintering treatment is lower than the specific glass density D.sub.M, and which due to the sintering treatment reach the specific density D.sub.K1 which differs from the specific glass density D.sub.M by less than 10%.

Glass Precursor Gel

A glass precursor gel and a method of making a glass product from the glass precursor gel are disclosed. The glass precursor gel includes a bulk amorphous oxide-based matrix that is homogeneously chemically mixed and includes 30 mol % to 90 wt.% silica and at least one of the following: (A) 0.1 mol % to 25 mol % of one or more alkali oxides in sum total, (B) 0.1 mol % to 25 mol % of one or more alkaline earth oxides in sum total, (C) 1 mol % to 20 mol % boric oxide, (D) 5 mol % to 80 mol % lead oxide, or (E) 0.1 mol % to 10 mol % aluminum oxide. A method of making a glass product from the glass precursor gel involves obtaining the glass precursor gel, melting the glass precursor gel into molten glass, and forming the molten glass into a glass product.

WATER SOLVATED GLASS/AMORPHOUS SOLID IONIC CONDUCTORS

The disclosure provides a water-solvated glass/amorphous solid that is an ionic conductor-an electronic insulator, and a dielectric as well as electrochemical devices and processes that use this material, such as batteries, including rechargeable batteries, fuel cells, capacitors, electrolysis cells, and electronic devices. The electrochemical devices and products use a combination of ionic and electronic conduction as well as internal electric dipoles.