Patent classifications
C07D303/02
Docosahexaenoyl ethanolamides
The invention describes novel mono or dihydroxy docosahexaenoic acid (DHA) analogs, their preparation, isolation, identification, purification and uses thereof.
Method for the epoxidation of an olefin with hydrogen peroxide
In the method for the epoxidation of an olefin, the olefin is continuously reacted with hydrogen peroxide in a mixed reactor in the presence of a water soluble epoxidation catalyst, comprising a manganese complex, the reaction is carried out in a reaction mixture comprising an aqueous liquid phase and an organic liquid phase with mixing of the liquid phases, reaction mixture is continuously withdrawn from the mixed reactor and separated into a separated aqueous phase and a separated organic phase, and part of the separated aqueous phase is continuously recycled into the mixed reactor, with the combined hold-up time of aqueous phase in withdrawing, separating phases and recycling aqueous phase being kept at less than 15 minutes.
Method for the epoxidation of an olefin with hydrogen peroxide
In the method for the epoxidation of an olefin, the olefin is continuously reacted with hydrogen peroxide in a mixed reactor in the presence of a water soluble epoxidation catalyst, comprising a manganese complex, the reaction is carried out in a reaction mixture comprising an aqueous liquid phase and an organic liquid phase with mixing of the liquid phases, reaction mixture is continuously withdrawn from the mixed reactor and separated into a separated aqueous phase and a separated organic phase, and part of the separated aqueous phase is continuously recycled into the mixed reactor, with the combined hold-up time of aqueous phase in withdrawing, separating phases and recycling aqueous phase being kept at less than 15 minutes.
FLAME-RETARDANT ACONITIC ACID-DERIVED MONOMERS
A flame-retardant aconitic acid-derived monomer, a process for forming a flame-retardant polymer, and an article of manufacture comprising a material that contains a flame-retardant aconitic acid-derived monomer are disclosed. The flame-retardant aconitic acid-derived monomer can have at least one phosphoryl or phosphonyl moiety with functional groups that can participate in a polymerization reaction, such as allyl, epoxy, or propylene carbonate functional groups. The process for forming the flame-retardant polymer can include forming an aconitic acid derivative, forming a phosphorus-based flame-retardant molecule, and reacting the aconitic acid derivative with the phosphorus-based flame-retardant molecule to form a flame-retardant aconitic acid-derived monomer, which is then polymerized. The aconitic acid derivative can be synthesized from aconitic acid obtained from a bio-based source. The material in the article of manufacture can be a resin or adhesive, and the article of manufacture can further comprise an electronic component.
PROCESS FOR REDUCING PROPYLENE CHLOROHYDRIN IN HYDROXYPROPYLATED PRODUCTS
A method of reducing the amount propylene chlorohydrin produced in a reaction to make a hydroxypropylated/crosslinked starch comprising removing residual propylene oxide from alkaline slurry. The residual propylene oxide is removed by the dewatering the alkaline slurry or by washing the starch in slurry at a pH of around 10. The starch is then neutralized in an acid solution and recovered from the second slurry and may or may not be washed, depending on whether the slurry while at pH around 10 to make a hydroxypropylated/crosslinked starch having less than 1 ppm propylene chlorohydrin.
COMPOSITE FOR NEUTRAL LAYER
The present application relates to a neutral layer composition. The present application can provide a neutral layer composition capable of forming a neutral layer, which can be effectively applied in the formation of a polymeric film comprising a vertically aligned self-assembled block copolymer.
LIQUID-CRYSTAL URETHANE COMPOUND, THERMALLY RESPONSIVE LIQUID-CRYSTAL POLYURETHANE ELASTOMER, AND PRODUCTION METHOD THEREFOR
The purpose of the present invention is to provide: a thermally responsive liquid-crystal polyurethane elastomer which is capable of being industrially continuously molded, and which is liquid crystal and has rubber elasticity at low temperatures (in the vicinity of room temperature); and a production method and a starting material therefor. This liquid-crystal urethane compound is obtained by reacting a mesogenic group-containing compound having at least active hydrogen groups, an alkylene oxide and/or a styrene oxide, and a diisocyanate compound.
LIQUID-CRYSTAL URETHANE COMPOUND, THERMALLY RESPONSIVE LIQUID-CRYSTAL POLYURETHANE ELASTOMER, AND PRODUCTION METHOD THEREFOR
The purpose of the present invention is to provide: a thermally responsive liquid-crystal polyurethane elastomer which is capable of being industrially continuously molded, and which is liquid crystal and has rubber elasticity at low temperatures (in the vicinity of room temperature); and a production method and a starting material therefor. This liquid-crystal urethane compound is obtained by reacting a mesogenic group-containing compound having at least active hydrogen groups, an alkylene oxide and/or a styrene oxide, and a diisocyanate compound.
METHOD FOR THE EPOXIDATION OF AN OLEFIN WITH HYDROGEN PEROXIDE
In the method for the epoxidation of an olefin, the olefin is continuously reacted with hydrogen peroxide in a mixed reactor in the presence of a water soluble epoxidation catalyst, comprising a manganese complex, the reaction is carried out in a reaction mixture comprising an aqueous liquid phase and an organic liquid phase with mixing of the liquid phases, reaction mixture is continuously withdrawn from the mixed reactor and separated into a separated aqueous phase and a separated organic phase, and part of the separated aqueous phase is continuously recycled into the mixed reactor, with the combined hold-up time of aqueous phase in withdrawing, separating phases and recycling aqueous phase being kept at less than 15 minutes.
METHOD FOR THE EPOXIDATION OF AN OLEFIN WITH HYDROGEN PEROXIDE
In the method for the epoxidation of an olefin, the olefin is continuously reacted with hydrogen peroxide in a mixed reactor in the presence of a water soluble epoxidation catalyst, comprising a manganese complex, the reaction is carried out in a reaction mixture comprising an aqueous liquid phase and an organic liquid phase with mixing of the liquid phases, reaction mixture is continuously withdrawn from the mixed reactor and separated into a separated aqueous phase and a separated organic phase, and part of the separated aqueous phase is continuously recycled into the mixed reactor, with the combined hold-up time of aqueous phase in withdrawing, separating phases and recycling aqueous phase being kept at less than 15 minutes.