A method of making an overbased calcium sulfonate or calcium magnesium sulfonate grease using one or more delay periods between the addition of at least a portion of a facilitating acid, such as DDBSA, and at least a portion of the next subsequently added ingredient. The delay period may be a temperature adjustment delay or a holding delay period. An overbased calcium sulfonate or calcium magnesium sulfonate grease composition comprises 0.5%-5% of a facilitating acid, allows for a reduced amount of overbased calcium sulfonate below 22%, and allows for a reduced amount of calcium hydroxyapatite to provide 10-25% of hydroxide equivalent basicity of the total hydroxide equivalent basicity due to calcium hydroxyapatite and added calcium hydroxide, while maintaining a high dropping point.

An overbased calcium magnesium sulfonate grease composition and method of manufacture comprising both overbased calcium sulfonate and overbased magnesium sulfonate in a ratio range of 60:40 to 100:1. The grease is made according to any known method for making an overbased calcium sulfonate grease by using the overbased magnesium sulfonate in addition to the overbased calcium sulfonate. A portion of the magnesium sulfonate may be added prior to conversion and another portion after conversion, with or without one or more delay periods between the addition of water or other reactive ingredient and the addition of magnesium sulfonate. The grease can be made using calcium hydroxyapatite and/or added calcium carbonate as calcium containing bases for reacting with complexing acids, a non-aqueous converting agent delay method, added alkali metal hydroxide, or any combination thereof. The grease has a high dropping point and reduced thickener yield.

An overbased calcium magnesium sulfonate grease composition and method of manufacture comprising both overbased calcium sulfonate and overbased magnesium sulfonate in a ratio range of 60:40 to 100:1. The grease is made according to any known method for making an overbased calcium sulfonate grease by using the overbased magnesium sulfonate in addition to the overbased calcium sulfonate. A portion of the magnesium sulfonate may be added prior to conversion and another portion after conversion, with or without one or more delay periods between the addition of water or other reactive ingredient and the addition of magnesium sulfonate. The grease can be made using calcium hydroxyapatite and/or added calcium carbonate as calcium containing bases for reacting with complexing acids, a non-aqueous converting agent delay method, added alkali metal hydroxide, or any combination thereof. The grease has a high dropping point and reduced thickener yield.

The invention provides a lubricating oil composition comprising: a base oil; and coated particles made of nanoparticles and phosphonic acid coating at least a portion of the surface of the nanoparticles.

The invention provides a lubricating oil composition comprising: a base oil; and coated particles made of nanoparticles and phosphonic acid coating at least a portion of the surface of the nanoparticles.

To provide a lubricant composition for shock absorbers, a shock absorber, and a method for adjusting the friction of a lubricant composition for shock absorbers, each capable of satisfying both operational stability and ride comfort particularly at the time of a minute amplitude. The lubricant composition for shock absorbers contains a base oil and a friction adjusting agent, wherein the friction adjusting agent contains a pentaerythritol ester, the pentaerythritol ester contains a pentaerythritol tetraester at the highest proportion or in an amount of 50 mass % or more, and the pentaerythritol ester content is 0.5 mass % or more.

To provide a lubricant composition for shock absorbers, a shock absorber, and a method for adjusting the friction of a lubricant composition for shock absorbers, each capable of satisfying both operational stability and ride comfort particularly at the time of a minute amplitude. The lubricant composition for shock absorbers contains a base oil and a friction adjusting agent, wherein the friction adjusting agent contains a pentaerythritol ester, the pentaerythritol ester contains a pentaerythritol tetraester at the highest proportion or in an amount of 50 mass % or more, and the pentaerythritol ester content is 0.5 mass % or more.

To prevent nuisance marine growth in a valve, particularly a ball valve, used to regulate a flow of seawater, a compound for lubricating and preventing nuisance marine growth is provided in the valve. The nuisance marine growth preventing compound includes a substantially uniform mixture of marine grease and an antifouling agent. The compound is introduced into the valve such that the compound is provided between and contacts a valve body and a ball that regulates the flow of seawater within the valve, and inhibits nuisance marine growth at a space between the ball and the valve body which is occupied by the compound.

To prevent nuisance marine growth in a valve, particularly a ball valve, used to regulate a flow of seawater, a compound for lubricating and preventing nuisance marine growth is provided in the valve. The nuisance marine growth preventing compound includes a substantially uniform mixture of marine grease and an antifouling agent. The compound is introduced into the valve such that the compound is provided between and contacts a valve body and a ball that regulates the flow of seawater within the valve, and inhibits nuisance marine growth at a space between the ball and the valve body which is occupied by the compound.

Provided is a grease composition which can be used as a lubricant for roller bearings, exhibits excellent high temperature durability and rust preventive property, and can prevent premature flaking on the rolling surface due to hydrogen embrittlement. A roller bearing 1 is obtained by sealing a grease composition 7 in the periphery of a rolling element 4, this grease composition 7 is composed of a base oil excluding an ester-based synthetic oil, a thickener, and an additive, the additive contains (a) an alkanolamine and (b) 2,2,4-trimethyl-1,2-dihydroquinoline or a polymer thereof but does not contain an organic sulfonate, and (a) and (b) are contained at from 0.1 to 10 parts by weight with respect to 100 parts by weight of a total amount of the base oil and the thickener, respectively.