Patent classifications
C22B1/02
METHOD FOR REUSING ACTIVE MATERIAL USING POSITIVE ELECTRODE SCRAP
There is provided a method of collecting and reusing an active material from a positive electrode scrap. The method of reusing a positive electrode active material according to the present disclosure includes (a-1) dry-milling a positive electrode scrap comprising an active material layer on a current collector to form the active material layer into a powdered state and separate the current collector, (a-2) thermally treating the active material layer in powder form in air for thermal decomposition of a binder and a conductive material in the active material layer, to collect an active material, (b) washing the active material collected from the step (a-2) with a lithium compound solution which is basic in an aqueous solution and drying, and (c) annealing the active material washed from the step (b) with an addition of a lithium precursor to obtain a reusable active material.
METHOD FOR REUSING ACTIVE MATERIAL USING POSITIVE ELECTRODE SCRAP
There is provided a method of collecting and reusing an active material from a positive electrode scrap. The method of reusing a positive electrode active material according to the present disclosure includes (a-1) dry-milling a positive electrode scrap comprising an active material layer on a current collector to form the active material layer into a powdered state and separate the current collector, (a-2) thermally treating the active material layer in powder form in air for thermal decomposition of a binder and a conductive material in the active material layer, to collect an active material, (b) washing the active material collected from the step (a-2) with a lithium compound solution which is basic in an aqueous solution and drying, and (c) annealing the active material washed from the step (b) with an addition of a lithium precursor to obtain a reusable active material.
Pyrometallurgical method for obtaining compounds of lithium and intermediates from alpha-spodumene and lepidolite
Pyrometallurgic process for obtaining lithium compounds and intermediates, the process being characterized by comprising the steps of a) contacting lithium aluminosilicate particles with at least a fluorine solid compound, b) heating until a temperature of 25 to 900° C. obtaining a solid mixture and c) carrying out at least a leaching process of the mixture in step b).
Use of cationic surfactants in the cyanidation of refractory carbonaceous ores for recovery of metals
A process for recovery of precious metals from ores or concentrates containing refractory carbonaceous material by cyanidation leaching. The process involves addition to the ores or concentrates at least one cationic surfactant before or during the addition of cyanide-containing solution. The agent enables the recovery of precious metals by cyanidation from high preg-robbing carbonaceous ores and improves the recovery of precious metals by cyanidation from medium to low preg-robbing carbonaceous ores. The agent also prevents froth and foaming formation during the cyanidation process.
Use of cationic surfactants in the cyanidation of refractory carbonaceous ores for recovery of metals
A process for recovery of precious metals from ores or concentrates containing refractory carbonaceous material by cyanidation leaching. The process involves addition to the ores or concentrates at least one cationic surfactant before or during the addition of cyanide-containing solution. The agent enables the recovery of precious metals by cyanidation from high preg-robbing carbonaceous ores and improves the recovery of precious metals by cyanidation from medium to low preg-robbing carbonaceous ores. The agent also prevents froth and foaming formation during the cyanidation process.
Method for improving quality of titanium-containing feedstock
A technique is provided, in which impure metal is efficiently separated and removed from titanium-containing raw material such as titanium slag or ilmenite and high titanium-containing raw material is produced. The method for improving quality of titanium-containing raw material containing slag, including steps of: oxidizing the titanium-containing raw material, selectively chlorinating impurities in the titanium-containing raw material, and separating and removing the impure chlorides to obtain high titanium-containing raw material. Alternatively, in this method, the oxidizing treatment and the selective chlorinating treatment are performed simultaneously.
Method for improving quality of titanium-containing feedstock
A technique is provided, in which impure metal is efficiently separated and removed from titanium-containing raw material such as titanium slag or ilmenite and high titanium-containing raw material is produced. The method for improving quality of titanium-containing raw material containing slag, including steps of: oxidizing the titanium-containing raw material, selectively chlorinating impurities in the titanium-containing raw material, and separating and removing the impure chlorides to obtain high titanium-containing raw material. Alternatively, in this method, the oxidizing treatment and the selective chlorinating treatment are performed simultaneously.
LI-ION BATTERY RECYCLING PROCESS AND SYSTEM FOR BLACK MASS FRACTIONATION AND RECOVERY OF SPECIFIC MATERIALS
A method is provided for recycling lithium-ion batteries containing plastics, electrolyte, carbon, metals, and lithium. The method includes: Lithium-ion batteries are ground to form ground battery material which is then pyrolyzed at a temperature between about 100° C. and 700° C. for a time sufficient to vaporize about 80 wt % to 100 wt % of electrolytes present in the ground battery material. The resulting material is further ground and screen classified to produce a screen oversize and a screen undersize. The screen oversize comprises metals and plastics, while the screen undersize comprises a black mass material. Lithium dissolution, triboelectric charging and electrostatic separation of the black mass material (not necessarily in that order) produces a liquid comprising dissolved lithium, a graphite product, and a concentrated metal fines product. Lithium is precipitated from the liquid comprising dissolved lithium, and the concentrated metal fines can be further treated by hydrometallurgy or pyrometallurgy processes.
LI-ION BATTERY RECYCLING PROCESS AND SYSTEM FOR BLACK MASS FRACTIONATION AND RECOVERY OF SPECIFIC MATERIALS
A method is provided for recycling lithium-ion batteries containing plastics, electrolyte, carbon, metals, and lithium. The method includes: Lithium-ion batteries are ground to form ground battery material which is then pyrolyzed at a temperature between about 100° C. and 700° C. for a time sufficient to vaporize about 80 wt % to 100 wt % of electrolytes present in the ground battery material. The resulting material is further ground and screen classified to produce a screen oversize and a screen undersize. The screen oversize comprises metals and plastics, while the screen undersize comprises a black mass material. Lithium dissolution, triboelectric charging and electrostatic separation of the black mass material (not necessarily in that order) produces a liquid comprising dissolved lithium, a graphite product, and a concentrated metal fines product. Lithium is precipitated from the liquid comprising dissolved lithium, and the concentrated metal fines can be further treated by hydrometallurgy or pyrometallurgy processes.
Method, arrangement, and pelletising plant
A method includes the introduction of a first medium into the compartment through an inlet and the heating of the first medium when it is present in the inlet. The heating takes place through the use of a combustion arrangement that is arranged in the inlet and that comprises fuel. The heating, the use of the combustion arrangement, includes in turn the ignition of the fuel, combustion of the fuel, and the transfer of the combustion heat to the first medium that is present at the combustion arrangement in the inlet. The combustion arrangement, is arranged in a region in the inlet, which in turn is arranged outside of the direct passage of the first medium in and through the inlet, such that the ignition of the fuel, the combustion of the fuel and the transfer of combustion heat to the first medium take place in this region.