A process for the separation of electrolyte from the carbon in a solid carbon/electrolyte cathode product formed at the cathode during molten carbonate electrolysis. The processes allow for easy separation of the solid carbon product from the electrolyte without any observed detrimental effect on the structure and/or stability of the resulting solid carbon nanomaterial.

Disclosed herein is a method of converting a carbon material to graphene, the method comprising the step of subjecting an amorphous carbon material pellet submerged in a molten inorganic material that comprises an alkaline earth halide to an electrochemical reaction in an inert atmosphere for a period of time, wherein the amorphous carbon material pellet is converted to a graphene pellet comprising graphene flakes by said reaction.

The embodiments of the present disclosure relate to a method and apparatus for producing a carbon nanomaterial product (CNM) product that may comprise carbon nanotubes and various other allotropes of nanocarbon. The method and apparatus employ a consumable carbon dioxide (CO.sub.2) and a renewable carbonate electrolyte as reactants in an electrolysis reaction in order to make CNTs. In some embodiments of the present disclosure, operational conditions of the electrolysis reaction may be varied in order to produce the CNM product with a greater incidence of a desired allotrope of nanocarbon or a desired combination of two or more allotropes.

The embodiments of the present disclosure relate to a method and apparatus for producing a carbon nanomaterial product (CNM) product that may comprise carbon nanotubes and various other allotropes of nanocarbon. The method and apparatus employ a consumable carbon dioxide (CO.sub.2) and a renewable carbonate electrolyte as reactants in an electrolysis reaction in order to make CNTs. In some embodiments of the present disclosure, operational conditions of the electrolysis reaction may be varied in order to produce the CNM product with a greater incidence of a desired allotrope of nanocarbon or a desired combination of two or more allotropes.

The embodiments herein relate to methods, apparatus, and systems for forming and purifying solid carbon material from a molten carbonate salt electrolyte. Various embodiments also provide methods, apparatus, and systems for recycling certain materials including the carbonate salt electrolyte, carbon dioxide, water, etc. Advantageously, the system utilizes carbon dioxide in one or more processes, for example to purify the solid carbon and regenerate the carbonate salt electrolyte. These methods, apparatus, and systems provide an efficient technique to consume carbon dioxide in the production of solid carbon, with substantial advantages over systems that attempt to form solid carbon from a stream of carbon dioxide provided directly to an electrolysis reactor.

The present application belongs to the technical field of aluminum metallurgy, and specifically relates to a method for producing metallic aluminum and polysilicon with a high-silicon aluminum-containing resource. The method includes: pretreating the high-silicon aluminum-containing resource to obtain an aluminum-silicon oxide material; the aluminum-silicon oxide material is used to produce a metallic aluminum product and a copper-aluminum-silicon alloy with silicon enriched by molten salt electrolysis in a double-chamber electrolytic cell; and the copper-aluminum-silicon alloy is used to produce an aluminum-silicon alloy and/or polysilicon by molten salt electrolysis in a single-chamber electrolytic cell, and further separating the aluminum-silicon alloy by physical methods to obtain polysilicon. The present application has characteristics such as low production cost, continuous electrolysis operations, high product quality, and environmental friendliness.

The present application belongs to the technical field of aluminum metallurgy, and specifically relates to a method for producing metallic aluminum and polysilicon with a high-silicon aluminum-containing resource. The method includes: pretreating the high-silicon aluminum-containing resource to obtain an aluminum-silicon oxide material; the aluminum-silicon oxide material is used to produce a metallic aluminum product and a copper-aluminum-silicon alloy with silicon enriched by molten salt electrolysis in a double-chamber electrolytic cell; and the copper-aluminum-silicon alloy is used to produce an aluminum-silicon alloy and/or polysilicon by molten salt electrolysis in a single-chamber electrolytic cell, and further separating the aluminum-silicon alloy by physical methods to obtain polysilicon. The present application has characteristics such as low production cost, continuous electrolysis operations, high product quality, and environmental friendliness.

A method for producing a hydrocarbon including: preparing a molten salt containing a carbonate of a first metal; obtaining precipitates containing a first metal carbide by applying a voltage to the molten salt; and obtaining a gas containing the hydrocarbon and a hydroxide of the first metal by hydrolyzing the first metal carbide.

The embodiments of the present disclosure relate to a method and apparatus for producing a carbon nanomaterial product (CNM) product that may comprise carbon nanotubes and various other allotropes of nanocarbon. The method and apparatus employ a consumable carbon dioxide (CO.sub.2) and a renewable carbonate electrolyte as reactants in an electrolysis reaction in order to make CNTs. In some embodiments of the present disclosure, operational conditions of the electrolysis reaction may be varied in order to produce the CNM product with a greater incidence of a desired allotrope of nanocarbon or a desired combination of two or more allotropes.

The embodiments of the present disclosure relate to a method and apparatus for producing a carbon nanomaterial product (CNM) product that may comprise carbon nanotubes and various other allotropes of nanocarbon. The method and apparatus employ a consumable carbon dioxide (CO.sub.2) and a renewable carbonate electrolyte as reactants in an electrolysis reaction in order to make CNTs. In some embodiments of the present disclosure, operational conditions of the electrolysis reaction may be varied in order to produce the CNM product with a greater incidence of a desired allotrope of nanocarbon or a desired combination of two or more allotropes.