C25C7/02

Method for electrochemical extraction of uranium from seawater using oxygen vacancy (OV)-containing metal oxide

A method for electrochemical extraction of uranium from seawater using an oxygen vacancy (OV)-containing metal oxide includes the following steps: adding glycerin to a solution of indium nitrate in isopropanol, transferring a resulting mixture to a reactor, and conducting reaction to obtain a spherical indium hydroxide solid; dissolving the solid in deionized water, transferring a resulting solution to the reactor, and conducting reaction to obtain a flaky indium hydroxide solid; calcining the solid to obtain calcined OV-containing In.sub.2O.sub.3-x; adding the In.sub.2O.sub.3-x to ethanol, and adding a membrane solution; coating a resulting solution uniformly on carbon paper, and naturally drying the carbon paper; clamping dried carbon paper with a gold electrode for being used as a working electrode for a three-electrode system; and adding simulated seawater to an electrolytic cell, placing the three-electrode system in the simulated seawater, and stirring the simulated seawater for electrolysis to extract uranium from the seawater.

Method for electrochemical extraction of uranium from seawater using oxygen vacancy (OV)-containing metal oxide

A method for electrochemical extraction of uranium from seawater using an oxygen vacancy (OV)-containing metal oxide includes the following steps: adding glycerin to a solution of indium nitrate in isopropanol, transferring a resulting mixture to a reactor, and conducting reaction to obtain a spherical indium hydroxide solid; dissolving the solid in deionized water, transferring a resulting solution to the reactor, and conducting reaction to obtain a flaky indium hydroxide solid; calcining the solid to obtain calcined OV-containing In.sub.2O.sub.3-x; adding the In.sub.2O.sub.3-x to ethanol, and adding a membrane solution; coating a resulting solution uniformly on carbon paper, and naturally drying the carbon paper; clamping dried carbon paper with a gold electrode for being used as a working electrode for a three-electrode system; and adding simulated seawater to an electrolytic cell, placing the three-electrode system in the simulated seawater, and stirring the simulated seawater for electrolysis to extract uranium from the seawater.

ELECTROLYTIC REDUCTION SYSTEM AND METHOD OF VANADIUM ELECTROLYTE
20220216495 · 2022-07-07 ·

Disclosed are an electrolytic reduction system of a vanadium electrolyte and a method for producing the electrolyte. The electrolytic reduction system includes a separating device and an electrolytic tank. The separating device is configured to separate a mixture consisting of a vanadium pentoxide (V2O5) solid and a sulfate acid solution, thereby obtaining a vanadium solution from a liquid discharging port of the separating device and a vanadium solid from a solid discharging port. The vanadium solution includes pentavalent vanadium ions. The electrolytic tank connects to the liquid discharging port of the separating device to contain the vanadium solution. In the method for producing the vanadium electrolyte, other chemical reagents are unnecessarily to be added into the mixture, and the vanadium solution is subjected to an electrolytic reduction process, such that the pentavalent vanadium ions are reduced to tetravalent vanadium ions and trivalent vanadium ions in the electrolytic tank.

ELECTROLYTIC REDUCTION SYSTEM AND METHOD OF VANADIUM ELECTROLYTE
20220216495 · 2022-07-07 ·

Disclosed are an electrolytic reduction system of a vanadium electrolyte and a method for producing the electrolyte. The electrolytic reduction system includes a separating device and an electrolytic tank. The separating device is configured to separate a mixture consisting of a vanadium pentoxide (V2O5) solid and a sulfate acid solution, thereby obtaining a vanadium solution from a liquid discharging port of the separating device and a vanadium solid from a solid discharging port. The vanadium solution includes pentavalent vanadium ions. The electrolytic tank connects to the liquid discharging port of the separating device to contain the vanadium solution. In the method for producing the vanadium electrolyte, other chemical reagents are unnecessarily to be added into the mixture, and the vanadium solution is subjected to an electrolytic reduction process, such that the pentavalent vanadium ions are reduced to tetravalent vanadium ions and trivalent vanadium ions in the electrolytic tank.

PLATE EDGE PROTECTOR
20220298662 · 2022-09-22 ·

An edge protector 1 mountable to a cathode plate 2, the edge protector 1 comprising a set of elongate channels 3. Each elongate channel 10, 20, 30 defining a slot. The set of elongate channels 3 including a first and second channel 10, 20 adapted to receive and cover respective side edges 4a, 4c of the cathode plate 2, and a third channel 30 adapted to receive and cover a lower edge 4b of the cathode plate 2. The first, second and third channels 10, 20, 30 being channels of a first, second and third body 12, 22, 32 respectively. Wherein, the edge protector 1 further includes a first and a second insert 40a-b. The first insert 40a being adapted to be inserted into or over a feature 14 of a first end 16a of the first body 12 and a feature 24a of a first end 26a of the second body 22 to form a first corner 6a. The second insert 40b being adapted to be inserted into or over a feature 24b of a second end 26b of the second body 22 and a feature 34 of a first end 36a of the third body 32 to form a second corner 6b. The first and second corners 6a-b are overmoulded with a first and second mouldable material respectively. The first corner 6a being separately overmoulded to the second corner 6b.

PLATE EDGE PROTECTOR
20220298662 · 2022-09-22 ·

An edge protector 1 mountable to a cathode plate 2, the edge protector 1 comprising a set of elongate channels 3. Each elongate channel 10, 20, 30 defining a slot. The set of elongate channels 3 including a first and second channel 10, 20 adapted to receive and cover respective side edges 4a, 4c of the cathode plate 2, and a third channel 30 adapted to receive and cover a lower edge 4b of the cathode plate 2. The first, second and third channels 10, 20, 30 being channels of a first, second and third body 12, 22, 32 respectively. Wherein, the edge protector 1 further includes a first and a second insert 40a-b. The first insert 40a being adapted to be inserted into or over a feature 14 of a first end 16a of the first body 12 and a feature 24a of a first end 26a of the second body 22 to form a first corner 6a. The second insert 40b being adapted to be inserted into or over a feature 24b of a second end 26b of the second body 22 and a feature 34 of a first end 36a of the third body 32 to form a second corner 6b. The first and second corners 6a-b are overmoulded with a first and second mouldable material respectively. The first corner 6a being separately overmoulded to the second corner 6b.

METHOD FOR CLEANLY EXTRACTING METALLIC SILVER

A method for cleanly extracting metallic silver includes: mixing an acidic solution containing Ce.sup.4+ and NO.sub.3.sup.− with a silver-containing material for leaching; after the leaching is completed, carrying out a solid-liquid separation to obtain a leaching solution containing Ce.sup.3+ and Ag.sup.+; and electrolyzing the leaching solution, wherein an oxidation reaction of Ce′ occurs at an anode to realize a regeneration of Ce.sup.4+ and an electrolytic reduction occurs at a cathode to reduce Ag.sup.+ to obtain the metallic silver. Ce.sup.4+ is used as a leaching agent and an intermediate oxidant to implement a cyclic operation of solution leaching and electrolytic regeneration on the silver-containing material. Almost no NO.sub.x and waste liquid are caused by the extraction process, and the invention is clean and environmentally friendly.

METHOD FOR CLEANLY EXTRACTING METALLIC SILVER

A method for cleanly extracting metallic silver includes: mixing an acidic solution containing Ce.sup.4+ and NO.sub.3.sup.− with a silver-containing material for leaching; after the leaching is completed, carrying out a solid-liquid separation to obtain a leaching solution containing Ce.sup.3+ and Ag.sup.+; and electrolyzing the leaching solution, wherein an oxidation reaction of Ce′ occurs at an anode to realize a regeneration of Ce.sup.4+ and an electrolytic reduction occurs at a cathode to reduce Ag.sup.+ to obtain the metallic silver. Ce.sup.4+ is used as a leaching agent and an intermediate oxidant to implement a cyclic operation of solution leaching and electrolytic regeneration on the silver-containing material. Almost no NO.sub.x and waste liquid are caused by the extraction process, and the invention is clean and environmentally friendly.

Electrolytic method for extracting tin and/or lead contained in an electrically conductive mixture

The invention related to a method for extracting tin and/or lead contained in an electrically conductive mixture derived from waste, using a solution comprising methane sulphonic acid as an electrolytic solution.

Electrolytic method for extracting tin and/or lead contained in an electrically conductive mixture

The invention related to a method for extracting tin and/or lead contained in an electrically conductive mixture derived from waste, using a solution comprising methane sulphonic acid as an electrolytic solution.