A method of preparing iron oxide nanoparticles using an herbal mixture comprising Capparis spinosa, Cichorium intybus, Solanum nigrum, Cassia occidentalis, Terminalia arjuna, Achillea millefolium, and Tamarix gallica. The method produces crystalline γ-Fe.sub.2O.sub.3 nanoparticles which are superparamagnetic. The iron oxide nanoparticles are used in a method of killing or inhibiting the growth of a bacteria and/or fungus, particularly in the form of a biofilm. The nanoparticles are also used in a method of treating colon cancer.

A piezoelectric body contains potassium, sodium, and niobium, and has a perovskite structure. A Raman shift of peaks assigned to A.sub.1g obtained by performing Raman spectroscopic analysis on a plurality of measurement regions is 400 cm.sup.−1 or more and 700 cm.sup.−1 or less. A difference between a maximum value and a minimum value of the Raman shift among the peaks in the plurality of measurement regions is 11.0 cm.sup.−1 or less.

A method of synthesizing bimetallic oxide nanocomposites includes the steps of: providing a first metal salt solution; adding an oxidizing agent to the first metal salt solution while degassing the solution with an inert gas; heating the first metal salt solution; adding a second metal salt solution to the heated first metal salt solution to form a reaction mixture; adding a solution comprising a poly (ionic liquid) into the reaction mixture; adding a first base into the reaction mixture; adding a second base while stirring and maintaining a temperature ranging from about 40° C. to about 65° C. to provide a solution including a bimetallic oxide nanocomposite precipitate. The first metallic salt solution can include FeCl.sub.3 dissolved in water. The second metallic salt solution can include CuCl.sub.2 dissolved in water. The bimetallic oxide nanocomposites can be combined with epoxy resin to coat a steel stubstrate.

The purpose of the present disclosure is to provide a CNT fiber that is constituted of aligned carbon nanotubes (CNTs), is thin, has little irregularity in thickness, has excellent winding properties when undergoing coiling processing, and has superior conductivity. Provided is a CNT fiber constituted of carbon nanotubes (CNTs) having a thickness of 0.01 μm-3 mm, having a coefficient of variation for irregularity in thickness of 0.2 or less, having a distribution rate a for deviation from roundness of 40% or greater, and a distribution rate b of 70% or greater. Also provided is a method for manufacturing the CNT fiber.

A negative electrode active material according to an embodiment includes at least a titanic oxide compound. The intensity ratio of an infrared absorption spectrum after pyridine adsorption and desorption on a surface of the negative electrode active material satisfies relationships represented by the following formula [{I(3663 cm.sup.−1)/I(3738 cm.sup.−1)}>0.7] and the following formula [{I(2981 cm.sup.−1)/I(2930 cm.sup.−1)}<1], provided that, in the above formulae, {I(3663 cm.sup.−1)}, {I(3738 cm.sup.−1)}, {I(2981 cm.sup.−1)}, and {I(2930 cm.sup.−1)} indicate integrated intensities in regions of infrared wavenumbers.

A method for manufacturing monocrystalline graphene, includes supplying an aromatic carbon gas onto a single-crystalline metal catalyst to manufacture the monocrystalline graphene.

Methods of synthesis of mesoporous silica are disclosed. The mesoporous silica synthesized herein, like SBA-15, possesses a two-dimensional, hexagonal, through-hole structure with a space group p6mm. An effective quantity of one or more water-soluble oxidized disulfide oil (ODSO) compounds are used during synthesis to impart distinct characteristics.

Oxide compositions comprising a modified structure which includes the formula ABO.sub.z. The A component may comprise at a cation of least one element selected from the group consisting of Mg, Ca, Sr, Ba, Sc, Y, La, Ce, Pr, Nd, Gd, and Zn, and the B component may comprise a cation of at least one element selected from the group consisting of V, Cr, Mn, Fe, Co, and Ni. Batteries and supercapacitors comprising the oxide compositions of the present disclosure and methods of making the oxide compositions of the present disclosure are also provided.

A method of making Si.sub.3N.sub.4 nanotubes and nanorods comprising adding agricultural husk material powder to a container, wherein the container is a covered boron nitride crucible, creating an inert atmosphere of nitrogen inside the container, applying heat, heating the agricultural husk material, and reacting the agricultural husk material and forming silicon nitride, wherein the silicon nitride is nanotubes and nanorods.

Provided are graphene nanosheets having a polyaromatic hydrocarbon concentration of less than about 0.7% by weight. Also provided are Graphene nanosheets having a polyaromatic hydrocarbon concentration of about 0.01% to about 0.5%.