A method of forming nanocrystalline graphene according to an embodiment may include: arranging a substrate having a pattern in a reaction chamber; injecting a reaction gas into the reaction chamber, where the reaction gas includes a carbon source gas, an inert gas, and a hydrogen gas that are mixed; generating a plasma of the reaction gas in the reaction chamber; and directly growing the nanocrystalline graphene on a surface of the pattern using the plasma of the reaction gas at a process temperature. The pattern may include a first material and the substrate may include a second material different from the first material.

Disclosed herein are graphene coatings characterized by a porous, three-dimensional, spherical structure having a hollow core, along with methods for forming such graphene coatings on glasses, glass-ceramics, ceramics, and crystalline materials. Such coatings can be further coated with organic or inorganic layers and are useful in chemical and electronic applications.

Nano-structures of Aluminum Nitride and a method of producing nano-structures of Aluminum Nitride from nut shells comprising milling agricultural nuts into a fine nut powder, milling nanocrystalline Al.sub.2O.sub.3 into a powder, mixing, pressing the fine nut powder and the powder of nanocrystalline Al.sub.2O.sub.3, heating the pellet, maintaining the temperature of the pellet at about 1400° C., cooling the pellet, eliminating the residual carbon, and forming nano-structures of AlN. An Aluminum Nitride (AlN) product made from the steps of preparing powders of agricultural nuts using ball milling, preparing powders of nanocrystalline Al.sub.2O.sub.3, mixing the powders of agricultural nuts and the powders of nanocrystalline Al.sub.2O.sub.3 forming a homogenous sample powder of agricultural nuts and Al.sub.2O.sub.3, pressurizing, pyrolizing the disk, and reacting the disk and the nitrogen atmosphere and forming AlN.

The present invention relates to composite particles containing silicon and carbon, wherein a domain size region of vacancies of 2 nm or less is 44% by volume or more and 70% by volume or less when volume distribution information of domain sizes obtained by fitting a small-angle X-ray scattering spectrum of the composite particles with a spherical model in a carbon-vacancy binary system is accumulated in ascending order, and a true density calculated by dry density measurement by a constant volume expansion method using helium gas is 1.80 g/cm.sup.3 or more and 2.20 g/cm.sup.3 or less.

A conductive material, and a method for preparing the same are provided. The conductive material has a structure where a plurality of graphene sheets are interconnected, wherein an oxygen content is 1 wt % or higher based on the total weight of the conductive material, and a D/G peak ratio is 2.0 or less when the Raman spectrum is measured.

Calcium hydroxide nanoparticles (Ca(OH).sub.2NPs) synthesized using carob pulp extract may be hexagonal nanoparticles with a diameter ranging from about 31.22 nm to about 81.22 nm. The Ca(OH).sub.2NPs may be synthesized by heating ethylene glycol, adding calcium hydroxide to the ethylene glycol to provide a first mixture, heating the first mixture, adding a carob pulp aqueous extract to the first mixture to form a second mixture, heating the second mixture, adding sodium hydroxide (NaOH) to the second mixture to form a third mixture, heating the third mixture, resting the third mixture at room temperature after heating, centrifuging the third mixture, collecting a colloid sediment, extracting any unwanted contaminants from the colloid sediment, and drying the colloid sediment to obtain Ca(OH).sub.2NPs.

The present application discloses a sulfide solid electrolyte and a method for the preparation thereof, an all solid state lithium secondary battery, and an apparatus containing the all solid state lithium secondary battery. The sulfide solid electrolyte is obtained by compounding at least Li.sub.2S, P.sub.2S.sub.5 and a dopant M.sub.xS.sub.2O.sub.3, wherein M is one or more selected from Na, K, Ba and Ca, and 1≤x≤2.

A method for continuously mass-manufacturing graphene using thermal plasma, the method for continuously mass-manufacturing graphene includes the steps of: (a) injecting an inert gas into a plasma device to generate plasma; (b) injecting expandable graphite and graphite intercalation compounds (GIC) into the plasma device in constant amounts; and (c) allowing the expandable graphite and GIC to be expanded by thermal plasma treatment so that graphene is exfoliated.

A component for a lithium battery including a first layer including a lithium garnet having a porosity of 0 percent to less than 25 percent, based on a total volume of the first layer; and a second layer on the first layer and having a porosity of 25 percent to 80 percent, based on a total volume of the second layer, wherein the second layer is on the first layer and the second layer has a composition that is different from a composition of the first layer.

Disclosed herein are graphene coatings characterized by a porous, three-dimensional, spherical structure having a hollow core, along with methods for forming such graphene coatings on glasses, glass-ceramics, ceramics, and crystalline materials. Such coatings can be further coated with organic or inorganic layers and are useful in chemical and electronic applications.