C03B23/09

Method for reducing or eliminating residue in a glass container and a glass container made in accordance therewith

A method of preparing a glass medical container is provided including the steps of providing a glass blank and forming a channel through a part of the glass blank, the channel being substantially free of tungsten or derivatives thereof. In a further aspect of the subject invention, a glass medical container is provided including a glass body having a channel extending through a part of the glass body, the channel being substantially free of tungsten or derivatives thereof. With the subject invention, tungsten or derivatives thereof can be generally or altogether completely avoided in glass medical containers.

GLASS CONTAINER COMPRISING A GLASS BOTTOM WITH IMPROVED PROPERTIES

A glass container is provided that includes a tube, a circular bottom, and a longitudinal axis. A curved glass heel extends from an outer end the bottom to the first end of the tube. The two-dimensional distance h(x,y) between a contact plane and the outer surface. The two-dimensional distance is measured in a direction parallel to the axis. The slope magnitude of the outer surface at the given position x,y is given by


√{square root over ((dh/dx).sup.2+(dh/dy).sup.2)}.

The 75% quantile of values that have been determined for the term


√{square root over ((dh/dx).sup.2+(dh/dy).sup.2)}×d1/h(xy).sub.delta

for all given positions x,y within a circular area having a radius of 0.4×d2/2 and that correspond to the centre is less than 4100 μm/mm. The adjacent positions x,y increase stepwise by 200 μm, and h(x,y).sub.delta=h(x,y).sub.max−h(x,y).sub.min, h(x,y).sub.max is a maximum value for h(x,y) and h(x,y).sub.min is a minimum value for h(x,y) being determined in that circular area.

GLASS CONTAINER COMPRISING A GLASS BOTTOM WITH IMPROVED PROPERTIES

A glass container is provided that includes a tube, a circular bottom, and a longitudinal axis. A curved glass heel extends from an outer end the bottom to the first end of the tube. The outer surface has a topography defined by a function ĥ(x) that is an azimuthal average of a distance between a contact plane and the outer surface at any given position located on a circle having the centre and the radius |x|. The values ĥ for ĥ(x) are determined for a plurality of circles the radius of which increases stepwise by 500 μm starting with a circle around the centre having a radius of 500 μm. The values ĥ are determined in a range from x=−0.4×d2/2 to x=+0.4×d2/2, d2 having a size such that at least 4 values ĥ are determined and can be fitted with a curvature function

[00001] h ^ ( x ) = - c × x 2 1 + 1 - c 2 × x 2 + h 0 .

BOTTOM FORMING PROCESS

A process for preparing a glass container that includes: providing a glass tube with a first portion, a second portion, and a longitudinal axis (L.sub.tube); holding the first portion in a first clamping chuck and the second portion in a second clamping chuck; rotating the glass tube around the longitudinal axis (L.sub.tube); heating, via a heater, the glass tube above a glass transition temperature; separating the first and second portions from one another by pulling apart along the longitudinal axis (L.sub.tube) while the heated glass tube is still rotating by moving the first and the second chucks away from each other; and moving the heater, while moving the first and second chucks away from each other, so that the heater follows a mass that remains at a circular end region of the first and/or second portion.

BOTTOM FORMING PROCESS

A process for preparing a glass container that includes: providing a glass tube with a first portion, a second portion, and a longitudinal axis (L.sub.tube); holding the first portion in a first clamping chuck and the second portion in a second clamping chuck; rotating the glass tube around the longitudinal axis (L.sub.tube); heating, via a heater, the glass tube above a glass transition temperature; separating the first and second portions from one another by pulling apart along the longitudinal axis (L.sub.tube) while the heated glass tube is still rotating by moving the first and the second chucks away from each other; and moving the heater, while moving the first and second chucks away from each other, so that the heater follows a mass that remains at a circular end region of the first and/or second portion.

METHOD OF MANUFACTURING GLASS VESSEL, AND APPARATUS FOR MANUFACTURING GLASS VESSEL
20210122662 · 2021-04-29 ·

A method of producing a glass vessel includes holding a borosilicate glass tube with a first holding device, and holding an open end portion of the glass tube with a second holding device such that the second holding device is spaced apart from the first holding device. Heat is applied to the glass tube by a burner to separate the open end portion and form a bottom portion on the open end portion. Fire-blast treatment of an inner surface of the open end portion with a flame from a point burner is performed during at least a part of (i) applying heat to the borosilicate glass tube for separation, (ii) applying heat to the separated open end portion for bottom portion formation, and/or (iii) a period applying heat to the separated open end portion and prior to releasing the glass vessel from the second holding device.

Device and method for producing a medical glass container
10981822 · 2021-04-20 · ·

A device for producing a high-purity medical glass container from a hollow cylindrical glass blank extending along an axial direction (X) and having at least one open end, wherein the glass blank has a mouldable moulded section extending in the axial direction (X) from the open end. The device comprises a first moulding tool and a second moulding tool, where the first moulding tool has a moulding pin. The moulding pin can be moved via the open end of the hollow cylindrical glass blank in the moulded section thereof along the axial direction (X), wherein the moulding pin is fixed in a fixing unit of the first moulding tool. The moulded section can be deformed by the second moulding tool in such a way that an inner surface of the moulded section is in contact with the moulding pin, whereby the moulded section forms a channel.

Methods for minimizing SHR in glass articles by producing a gas flow during pharmaceutical part converting

Systems for producing articles from glass tube include a converter having a base with a plurality of processing stations and a turret moveable relative to the base. The turret indexes a plurality of holders for holding the glass tubes successively through the processing stations. The systems further include a gas flow system or a suction system for producing a flow of gas through the glass tube during one or more heating, forming, separating or piercing operations. The flow of gas through the glass tube produced by the gas flow system or suction system may be sufficient to evacuate or purge volatile constituents of the glass from the glass tube and/or pierce a meniscus formed on the glass tube during separation, thereby reducing the Surface Hydrolytic Response (SHR) of the interior surface of the glass tube and articles made therefrom.

Methods for minimizing SHR in glass articles by producing a gas flow during pharmaceutical part converting

Systems for producing articles from glass tube include a converter having a base with a plurality of processing stations and a turret moveable relative to the base. The turret indexes a plurality of holders for holding the glass tubes successively through the processing stations. The systems further include a gas flow system or a suction system for producing a flow of gas through the glass tube during one or more heating, forming, separating or piercing operations. The flow of gas through the glass tube produced by the gas flow system or suction system may be sufficient to evacuate or purge volatile constituents of the glass from the glass tube and/or pierce a meniscus formed on the glass tube during separation, thereby reducing the Surface Hydrolytic Response (SHR) of the interior surface of the glass tube and articles made therefrom.

GLASS ASSEMBLY, METHOD OF MAKING THE SAME AND ELECTROCHEMICAL SENSOR
20210140915 · 2021-05-13 ·

The present disclosure discloses a glass assembly, for forming an electrochemical sensor, comprising a glass immersion tube, a glass membrane connected to a distal end of the immersion tube, wherein the glass which forms the immersion tube contains no lead, no lead compound, no lithium, and no lithium compound.