A method for forming an ultra-high temperature (UHT) composite structure includes dispensing a first polymeric precursor with a spinneret; forming a first plurality of nanofibers from the first polymeric precursor; depositing the first plurality of nanofibers with a collector; and applying a fluid, with a nozzle, onto the first plurality of nanofibers disposed on the collector. The fluid includes a second polymeric precursor.

The present invention relates to inorganic fibres having a composition comprising: 65.7 to 70.8 wt % SiO.sub.2; 27.0 to 34.2 wt % CaO; 0.10 to 2.0 wt % MgO; and optional other components providing the balance up to 100 wt %,
wherein the sum of SiO.sub.2 and CaO is greater than or equal to 97.8 wt %; and the other components, when present, comprise no more than 0.80 wt % Al.sub.2O.sub.3; and wherein the amount of MgO and other components are configured to inhibit the formation of surface crystallite grains upon heat treatment at 1100° C. for 24 hours, wherein said surface crystallite grains comprise an average crystallite size in a range of from 0.0 to 0.90 μm.

A process for the manufacture of inorganic fibres comprises: (a) selecting a composition and proportion of: (i) silica sand; (ii) lime comprising at least 0.10 wt % magnesia; and (iii) optional additives comprising a source of oxides or non-oxides of one or more of the lanthanides series of elements, or combinations thereof; (b) mixing the silica sand; lime; and optional additives to form a mixture; (c) melting the mixture in a furnace; and (d) shaping the molten mixture into inorganic fibres. The raw materials selection comprises composition selection and proportion selection of the raw materials to obtain an inorganic fibre composition comprising a range of from 61.0 wt % and 70.8 wt % silica; less than 2.0 wt % magnesia; less than 2.0% incidental impurities; and no more than 2.0 wt % of metal oxides and/or metal non-oxides derived from said optional additives; with calcia providing the balance up to 100 wt %; and wherein the inorganic fibre composition comprises no more than 0.80 wt % Al.sub.20.sub.3 derived from the incidental impurities and/or the optional additives.

A catalyst-free synthesis method for the formation of a metalorganic compound comprising a desired (first) metal may include, for example, selecting another (second) metal and an organic solvent, with the second metal being selected to (i) be more reactive with respect to the organic solvent than the first metal and (ii) form, upon exposure of the second metal to the organic solvent, a reaction by-product that is more soluble in the organic solvent than the metalorganic compound. An alloy comprising the first metal and the second metal may be first produced (e.g., formed or otherwise obtained) and then treated with the organic solvent in a liquid phase or a vapor phase to form a mixture comprising (i) the reaction by-product comprising the second metal and (ii) the metalorganic compound comprising the first metal. The metalorganic compound may then be separated from the mixture in the form of a solid.

A method for injecting a loaded suspension into a fibrous texture having a three-dimensional or multilayer weaving includes the injection of a suspension containing a powder of solid particles into the volume of the fibrous texture. The injection of the loaded suspension is carried out by at least one hollow needle in communication with a loaded suspension supply device, each needle being movable in at least one direction extending between a first face and a second opposite face of the fibrous texture so as to inject the loaded suspension at one or more determined depths in the fibrous texture.

The present invention relates to inorganic fibres having a composition comprising: 61.0 to 70.8 wt % SiO.sub.2; 28.0 to 39.0 wt % CaO; 0.10 to 0.85 wt % MgO other components, if any, providing the balance up to 100 wt %, The sum of SiO.sub.2 and CaO is greater than or equal to 98.8 wt % and the other components comprise less than 0.70 wt % Al.sub.2O.sub.3, if any.

A gas turbine engine component includes a gas turbine engine component body formed of a ceramic matrix composite material having at least one fastener integrally formed with the gas turbine engine component body as a single-piece structure. The gas turbine engine component body initially comprises a rigidized preform structure formed from a polymer based material. The at least one fastener connects the gas turbine engine component body to an engine support structure.

A catalyst-free synthesis method for the formation of a metalorganic compound comprising a desired (first) metal may include, for example, selecting another (second) metal and an organic solvent, with the second metal being selected to (i) be more reactive with respect to the organic solvent than the first metal and (ii) form, upon exposure of the second metal to the organic solvent, a reaction by-product that is more soluble in the organic solvent than the metalorganic compound. An alloy comprising the first metal and the second metal may be first produced (e.g., formed or otherwise obtained) and then treated with the organic solvent in a liquid phase or a vapor phase to form a mixture comprising (i) the reaction by-product comprising the second metal and (ii) the metalorganic compound comprising the first metal. The metalorganic compound may then be separated from the mixture in the form of a solid.

An alumina fiber aggregate that is formed of alumina short fibers and has been subjected to needling treatment, wherein the alumina short fibers have an average fiber diameter of 6.0 μm or more and 10.0 μm or less and a specific surface area of 0.2 m.sup.2/g or more and 1.0 m.sup.2/g or less, and a residual percentage (%) of high-temperature-cycle opened gap pressure of the alumina fiber aggregate is 45% or more. A value obtained by subtracting twice the standard error of a length-weighted geometric mean diameter of fiber diameters of the alumina short fibers from the length-weighted geometric mean diameter is 6.0 μm or more. A proportion of alumina short fibers having a fiber diameter of more than 10.0 μm is preferably 5.0% or less on a number basis.

A microstructure comprises a plurality of interconnected units wherein the units are formed of graphene tubes. The graphene tubes may be formed by photo-initiating the polymerization of a monomer in a pattern of units to form a polymer microlattice, removing unpolymerized monomer, coating the polymer microlattice with a metal, removing the polymer microlattice to leave a metal microlattice, depositing graphitic carbon on the metal microlattice, converting the graphitic carbon to graphene, and removing the metal microlattice. A ceramic may be deposited on the graphene and another graphene layer may be deposited on top of the ceramic to create a multi-layered sp.sup.2-bonded carbon tube.