C07C59/08

NOVEL MAGNESIUM HYDROXIDE-BASED SOLID SOLUTION, AND RESIN COMPOSITION AND PRECURSOR FOR HIGHLY ACTIVE MAGNESIUM OXIDE WHICH INCLUDE SAME

[Problem] To provide a magnesium hydroxide-based solid solution which has smaller primary particles and secondary particles and improved reactivity with an acid as compared with conventional magnesium hydroxide (Mg(OH).sub.2), improves the flame retardancy and mechanical strength of a resin, and also forms a non-sedimenting slurry, providing the same handleability as a liquid.

[Structure] A magnesium hydroxide-based solid solution represented by the following formula (1): Mg(OH).sub.2-xR.sub.x (Formula 1), wherein R represents a monovalent organic acid, and x represents 0<x<1. The magnesium hydroxide-based solid solution is a magnesium oxide (MgO) precursor. A flame retardant for a synthetic resin, including the magnesium hydroxide-based solid solution as an active ingredient. A synthetic resin composition characterized by including 0.1 to 50 parts by weight of the magnesium hydroxide-based solid solution (b) per 100 parts by weight of a synthetic resin (a); and a molded article thereof.

NOVEL MAGNESIUM HYDROXIDE-BASED SOLID SOLUTION, AND RESIN COMPOSITION AND PRECURSOR FOR HIGHLY ACTIVE MAGNESIUM OXIDE WHICH INCLUDE SAME

[Problem] To provide a magnesium hydroxide-based solid solution which has smaller primary particles and secondary particles and improved reactivity with an acid as compared with conventional magnesium hydroxide (Mg(OH).sub.2), improves the flame retardancy and mechanical strength of a resin, and also forms a non-sedimenting slurry, providing the same handleability as a liquid.

[Structure] A magnesium hydroxide-based solid solution represented by the following formula (1): Mg(OH).sub.2-xR.sub.x (Formula 1), wherein R represents a monovalent organic acid, and x represents 0<x<1. The magnesium hydroxide-based solid solution is a magnesium oxide (MgO) precursor. A flame retardant for a synthetic resin, including the magnesium hydroxide-based solid solution as an active ingredient. A synthetic resin composition characterized by including 0.1 to 50 parts by weight of the magnesium hydroxide-based solid solution (b) per 100 parts by weight of a synthetic resin (a); and a molded article thereof.

METHOD FOR PRODUCING VAPOR COMPOSITION CONTAINING LACTIC ACID
20170253553 · 2017-09-07 ·

The method for producing a vapor composition containing lactic acid of the present invention is capable of suppressing the generation of by-products such as acetaldehyde and carbon monoxide due to pyrolysis of a lactic acid species during vaporization. Furthermore, a lactic acid oligomer generated can be effectively used without loss, and a vapor composition containing lactic acid can be industrially efficiently produced stably for a long time. The present invention relates to a method for producing a vapor composition containing lactic acid including: feeding a liquid composition containing lactic acid to a vaporizer; mixing the liquid composition with a liquid composition containing a lactic acid oligomer contained in the vaporizer to prepare a liquid mixture; and heating the liquid mixture to vaporize part of the liquid mixture, whereby a vapor composition containing lactic acid is produced.

METHOD FOR PRODUCING VAPOR COMPOSITION CONTAINING LACTIC ACID
20170253553 · 2017-09-07 ·

The method for producing a vapor composition containing lactic acid of the present invention is capable of suppressing the generation of by-products such as acetaldehyde and carbon monoxide due to pyrolysis of a lactic acid species during vaporization. Furthermore, a lactic acid oligomer generated can be effectively used without loss, and a vapor composition containing lactic acid can be industrially efficiently produced stably for a long time. The present invention relates to a method for producing a vapor composition containing lactic acid including: feeding a liquid composition containing lactic acid to a vaporizer; mixing the liquid composition with a liquid composition containing a lactic acid oligomer contained in the vaporizer to prepare a liquid mixture; and heating the liquid mixture to vaporize part of the liquid mixture, whereby a vapor composition containing lactic acid is produced.

METHOD FOR PRODUCING VAPOR COMPOSITION CONTAINING LACTIC ACID
20170253553 · 2017-09-07 ·

The method for producing a vapor composition containing lactic acid of the present invention is capable of suppressing the generation of by-products such as acetaldehyde and carbon monoxide due to pyrolysis of a lactic acid species during vaporization. Furthermore, a lactic acid oligomer generated can be effectively used without loss, and a vapor composition containing lactic acid can be industrially efficiently produced stably for a long time. The present invention relates to a method for producing a vapor composition containing lactic acid including: feeding a liquid composition containing lactic acid to a vaporizer; mixing the liquid composition with a liquid composition containing a lactic acid oligomer contained in the vaporizer to prepare a liquid mixture; and heating the liquid mixture to vaporize part of the liquid mixture, whereby a vapor composition containing lactic acid is produced.

Co-Crystals Comprising Levothyroxine And A Dicarboxylic Acid

The present invention relates to co-crystals comprising levothyroxine and a dicarboxylic acid, preferably L-tartaric acid or oxalic acid, and processes for the preparation thereof. Furthermore, the invention relates to a pharmaceutical composition comprising a co-crystal of the present invention, preferably the co-crystal comprising levothyroxine and L-tartaric acid or oxalic acid, and at least one pharmaceutically acceptable excipient. The pharmaceutical composition of the present invention can be used as a medicament, in particular for the treatment of hypothyroidism.

PURIFICATION OF MAGNESIUM LACTATE FROM FERMENTATION BROTHS HAVING HIGH AMOUNTS OF IMPURITIES
20210395788 · 2021-12-23 ·

A process for efficient purification of magnesium lactate from fermentation broths derived from non-homogeneous feedstocks that contain soluble and insoluble impurities is provided. The fermentation broth, having high amounts of impurities and containing magnesium lactate in a soluble form, is separated from insoluble impurities, concentrated to particularly high concentrations of the magnesium lactate at elevated temperatures, and subsequently cooled by gradual and controlled cooling such that magnesium lactate crystals of high purity are formed.

PURIFICATION OF MAGNESIUM LACTATE FROM FERMENTATION BROTHS HAVING HIGH AMOUNTS OF IMPURITIES
20210395788 · 2021-12-23 ·

A process for efficient purification of magnesium lactate from fermentation broths derived from non-homogeneous feedstocks that contain soluble and insoluble impurities is provided. The fermentation broth, having high amounts of impurities and containing magnesium lactate in a soluble form, is separated from insoluble impurities, concentrated to particularly high concentrations of the magnesium lactate at elevated temperatures, and subsequently cooled by gradual and controlled cooling such that magnesium lactate crystals of high purity are formed.

METHOD OF MAKING COBALT COMPOUNDS FOR FEED SUPPLEMENTS
20210380621 · 2021-12-09 · ·

A method of making a cobalt compound for feed supplements includes the steps of dissolving cobalt acetate tetrahydrate in water to form a mixture, adding an acid to the mixture, sonicating the mixture for a selected time, removing acetic acid from the mixture, and separating crystals of the cobalt compound from the mixture.

METHOD OF MAKING COBALT COMPOUNDS FOR FEED SUPPLEMENTS
20210380621 · 2021-12-09 · ·

A method of making a cobalt compound for feed supplements includes the steps of dissolving cobalt acetate tetrahydrate in water to form a mixture, adding an acid to the mixture, sonicating the mixture for a selected time, removing acetic acid from the mixture, and separating crystals of the cobalt compound from the mixture.