Systems and methods provide distillation systems and associated distillation methods. A distillation system can include a distillation chamber for distilling a biomass. A heat source can be applied to the distillation chamber to heat the biomass. A source of vacuum can be applied to the distillation chamber to remove a solvent from the distillation chamber. A magnetically driven spinner apparatus can be positioned within the distillation chamber and including at least a first paddle for generating a splash agitation of the biomass in the distillation chamber, wherein the magnetically driven spinner apparatus does not extend through any wall of the distillation chamber. A drive assembly can include a motor to cause rotational movement of the magnetically driven spinner apparatus within the distillation chamber.

Devices and methods for the high-pressure treatment of bulk material by extraction and/or impregnation. The bulk material is arranged in the interior volume of a pressure vessel device and is treated at a high pressure while sealed off from the surroundings. The high-pressure treatment is performed batchwise in a closed system in the pressure vessel device in a pressure-tight fashion. The bulk material is fed batchwise to the interior volume with the pressure vessel device closed and being arranged on at least one treatment level and, after the high-pressure treatment has occurred, being discharged batchwise from the interior volume with the pressure vessel device closed. The invention furthermore relates to the use of a supporting tray module with at least one treatment level for the high-pressure treatment in a closed system.

In an autoclave apparatus for a high-pressure acid leaching process which advances leaching by stirring heated and pressurized material slurry and sulfuric acid by stirrers in compartments in an autoclave main body of a plurality of compartments, transfers slurry from an upstream side compartment to a downstream one to advance leaching, liquid flow ports for slurry transfer that open and close by doors are provided on the partition walls, the liquid flow ports for slurry transfer are installed at positions where the heights from the lowermost portion the autoclave to the center of gravity are 0.1 to 0.3 times an autoclave diameter and distances from the center lines of the partition walls to the center of gravity are 0.05 to 0.25 times the autoclave diameter, and the liquid flow ports for slurry transfer have shapes which do not reach end portions of the partition walls.

A method of preparing paprika red pigment with low polycyclic aromatic hydrocarbons includes (1) drying, crushing and granulating mature peppers to obtain pepper particles; (2) extracting the pepper particles with a vegetable oil in a rotocel extractor to obtain a paprika red pigment solution; (3) extracting the paprika red pigment solution with an ethanol solution in a liquid-liquid extractor to remove spicy substances; (4) running the paprika red pigment solution through a low-pressure chromatography column to remove polycyclic aromatic hydrocarbons; and (5) concentrating the paprika red pigment solution to obtain the paprika red pigment with low polycyclic aromatic hydrocarbons.

The present invention discloses an apparatus for effective and efficient extraction of resin from plant materials. The apparatus includes at least an agitator and a tank. The tank is a square tank and is made of one piece of plastic that is sloped and folded (V-shaped) at the bottom. The agitator includes a single impellor or pulsator having two sides. The pulsator creates fluid currents in an upwards and downwards direction. Top portion pushes fluid up and bottom portion pushes fluid down. As a result of agitation, trichomes get separated and pass-through openings of the false bottom surface and are collected on the V-shaped bottom surface. This collection of the trichomes on the V-shaped bottom surface ensures that the trichomes do not move or go upward. The false bottom surface ensures that the trichomes are not getting hit by the agitator again post their collection on the V-shaped bottom surface.

An apparatus and method of high pressure treatment of bulk material by extraction and/or impregnation may involve treating bulk material in an internal volume of a pressure vessel apparatus at a high pressure level in a range from 40 to 1000 bar under isolation from the environment. The high pressure treatment may be performed charge-wise in a closed system in the pressure vessel apparatus in that the bulk material is supplied charge-wise to the internal volume with the pressure vessel apparatus closed and is positioned in at least one treatment plane. Upon completion of the high pressure treatment, the bulk material is discharged charge-wise from the internal volume with the pressure vessel apparatus closed. This also gives advantages in terms of handling, especially also with regard to material flow, and with regard to operational reliability.

An apparatus and method for high pressure treatment of bulk material by extraction and/or impregnation may involve high pressure treating bulk material in a high pressure treatment volume of a pressure vessel apparatus at a high pressure level, especially high pressure in the range from 40 to 1000 bar. The method comprises at least the three following step sequences that are each controllable individually: pressurization, high pressure treatment, and depressurization. The high pressure treatment is performed in a continuous manner in the high pressure treatment volume. The high pressure treatment volume or the entire pressure vessel apparatus is in a fixed arrangement during the high pressure treatment. The continuity of the high pressure treatment is ensured solely by means of the high pressure treatment volume. This especially enables engineering optimization of high pressure treatment processes, for example extraction.

A system for sand cleaning including: a cleaning unit arranged to receive oil impregnated sand; the unit including a chamber having an impeller, said impeller arranged to agitate the oil impregnated sand in a base of the unit; an aperture in the base of the unit arranged to discharge the treated sand; an oil outlet adjacent to a top of the unit arranged to discharge the separated oil.

Devices and methods for the high-pressure treatment of bulk material by extraction and/or impregnation. The bulk material is arranged in the interior volume of a pressure vessel device and is treated at a high pressure while sealed off from the surroundings. The high-pressure treatment is performed batchwise in a closed system in the pressure vessel device in a pressure-tight fashion. The bulk material is fed batchwise to the interior volume with the pressure vessel device closed and being arranged on at least one treatment level and, after the high-pressure treatment has occurred, being discharged batchwise from the interior volume with the pressure vessel device closed. The invention furthermore relates to the use of a supporting tray module with at least one treatment level for the high-pressure treatment in a closed system.

A method of preparing paprika red pigment with low polycyclic aromatic hydrocarbons includes (1) drying, crushing and granulating mature peppers to obtain pepper particles; (2) extracting the pepper particles with a vegetable oil in a rotocel extractor to obtain a paprika red pigment solution; (3) extracting the paprika red pigment solution with an ethanol solution in a liquid-liquid extractor to remove spicy substances; (4) running the paprika red pigment solution through a low-pressure chromatography column to remove polycyclic aromatic hydrocarbons; and (5) concentrating the paprika red pigment solution to obtain the paprika red pigment with low polycyclic aromatic hydrocarbons.