The present disclosure relates to a process for treating a feedstock containing tall oil, the process including separation of a light stream from the feedstock, followed by removal of a heavy fraction from the feedstock, in which process the separation of the light stream from the feedstock a fractionator is used and at least one product is collected from the light stream. The disclosure also relates to an apparatus for use in the process and use of a fractionator in dehydration of a feedstock containing tall oil.

A method of cleaning a condensate thermosyphon reboiler including modifying a flow rate of a hot oil stream introduced into the tube-side of a first condensate thermosyphon reboiler, modifying a flow rate of a condensate hydrocarbon stream introduced into the shell-side of the first condensate thermosyphon reboiler, and maintaining an operation of the condensate stabilizer system until the value of an overhead temperature of the first condensate thermosyphon reboiler is detected to have been modified from the first overhead temperature to a second overhead temperature. The method further includes modifying the flow rate of the condensate hydrocarbon stream from the second condensate flow rate to the first condensate flow rate, and modifying the flow rate of the hot oil stream from the second hot oil flow rate to the first hot oil flow rate.

The present invention provides a method for operating a rectification column (1000) for separating a mixture (S) containing a component A and a component B having a boiling point higher than that of the component A at an operating pressure of the rectification column (1000) which is lower than ambient pressure, wherein the method comprises a step for controlling the mass fraction of the component B in the product stream of the component A (P1) to a value within a first target range from 0.1% to 5.0% and the mass fraction of the component A in the product stream of the component B (P2) to a value within a second target range from 0.1% to 5.0%, wherein the control is carried out as a function of a controlling temperature (TC) for which a setpoint TC.sub.setpoint is calculated according to the equation TC.sub.setpoint=T2+F.Math.(T1−T2), where F is a factor which is in the range from 0.1 to 0.9 and T1 and T2 are reference temperatures, wherein in the case of a deviation in the measured control temperature (TC) from its setpoint TC.sub.setpoint being found the control temperature (TC) is readjusted to the setpoint TC.sub.setpoint by varying one or more of the following actuating variables: (i) heating of the column bottom (130) by the evaporator (200), (ii) the mass flow {dot over (m)}.sub.A42 of the reflux (A42) fed back into the rectification column, (iii) the mass flow {dot over (m)}.sub.P2 of the product stream P2 and (iv) the mass flow {dot over (m)}.sub.P1 of the product stream P1.

The present disclosure provides a control method for a rectification and purification system of electronic-grade chlorine trifluoride. A rectification device of electronic-grade chlorine trifluoride includes a two-stage cryogenic rectification device including a low-boiling column and a high-boiling column. An extraction agent is arranged in the two-stage cryogenic rectification device for further dissociating associated molecules of hydrogen fluoride and chlorine trifluoride to meet the requirements of electronic-grade chlorine trifluoride. The reflux ratio parameter stability of a vapor-liquid (chlorine trifluoride-hydrogen fluoride) phase equilibrium system can be effectively improved by a column plate temperature control method, thus realizing wide dynamic smooth running under various working conditions. The column plate temperature control method can achieve an effective separation of chlorine trifluoride and various impurity components by deep rectification technology, yielding electronic-grade chlorine trifluoride through purification.

Regenerative vapor energy recovery system and method for use with an ethanol plant. Regenerative vapors are partially condensed in a regenerative precondenser using a warm water stream. The warm water stream is fed to the regenerative precondenser and the partially condensed regenerative vapor stream is sent back to the ethanol plant where the stream is fully condensed using an existing condenser. The ethanol plant is thus operated at greater energy efficiency with lower operating costs than would be achieved with conventional systems.

A method for producing epoxyalkane includes the step of separating, in a separation column, a stream containing epoxyalkane, extractant, and diol. The separation column operates under conditions so as to enable the extractant and the diol to form an azeotrope, and a stream containing extractant and binary azeotrope is extracted from the side-draw of the separation column to liquid-liquid separation. The method can be used for the industrial production of epoxyalkane.

A method of separating linear alpha olefins includes: passing a feed stream comprising linear alpha olefins through a first column; distributing a C8− fraction to a top portion of the first column; distributing a C9+ fraction to a bottom portion of the first column; passing the C8− fraction directly to a top portion of a second column; passing the C9+ fraction directly to a bottom portion of a second column; distributing a C11+ fraction to the bottom portion of the second column; withdrawing a C10 fraction as a side draw from the second column; and passing a liquid stream and a vapor stream from the second column to the first column.

Heat exchangers (also referred to as exchangers herein) are provided that fit within a bottom sump of a distillation column. These heat exchangers may be at least partially submerged in the bottoms fluid of the distillation column so that the exterior surface of the heat exchanger can contribute to the total area of the heat exchanger. The internal configuration of the exchanger allows for annular coaxial flow of the hot fluid (condensing vapor stream) and eliminates the need for top and bottom channel heads.

A remediation plant for remediating drilling mud, cuttings, and fluids. The preferred plant includes a reboiler that is adapted to provide heat to the drilling mud, cuttings, and fluid, a mud drum that is operatively connected to the reboiler, a distillation column that is operatively connected to the reboiler, a heat exchanger that is operatively connected to the reboiler, a condenser that is operatively connected to the distillation column, a condenser tank that is operatively connected to the condenser, an oil-water separator that is operatively connected to the condenser tank, and a pump that is operatively connected to the oil-water separator. The preferred remediation plant is adapted to remove synthetic drilling fluid from drilling mud, cuttings, and fluids. A method for remediating drilling mud, cuttings, and fluid.

The present invention provides to a process for recovery of an organic compound (i.e. Ethanol, propanol, butanol, Acetone, iso-propyl alcohol) from a fermented broth which is produced from different fermentation technologies. The present invention particularly relates to an integrated process for ethanol separation from the fermentation broth using integrated vapor compressing unit (turbofans), evaporator (falling film) and a broth stripper column (vacuum distillation system). The process is operated under low temperature for the separation and recovery of the organic compound (particularly ethanol) from the fermented broth containing live microbes typically below or at 50° C. to ensure the activity of the microbes in the broth recycle. Again, the activity of the microbes is further ensured by maintaining the residence time of the microbe containing broth outside the Fermentor is less than or equal to 10 minutes.