B01J19/0066

Apparatus and method for continuous solvothermal synthesis of nanoparticles

An apparatus and a method for continuous solvothermal synthesis of nanoparticles, are provided. The apparatus includes an inlet section, a reactor section, a flexible quenching unit, and an outlet section. The inlet section separately receives reactants including the solvent and a precursor solution that are allowed to flow into the reactor section. The reactor section includes multiple spiral turns such that each of the spiral turns includes a helical channel followed by a counter-helical channel for enabling mixing of the reactants to cause solvothermal reactions between them. The counter-helical channel changes the direction of flow of reactants upon flow of said reactants from the helical channel to the counter-helical channel. The flexible quenching section enclosing a portion of the reactor section quenches a slurry formed as a result of the solvothermal reactions, wherein the slurry includes the nanoparticles of targeted characteristics. The outlet section facilitates withdrawal of the slurry.

Gastrointestinal tract simulation system, compartments therefor, and method

Gastrointestinal tract simulation system and compartment therefor. The compartment comprising a vessel having an open top surrounded by a peripheral edge portion and an air-tight lid system configured to be placed onto the peripheral edge portion. The lid system comprises a body with a plurality of passageways extending through the body and providing access to the interior of the vessel, the plurality of passageways comprising passageways for fluid transfer tubes and passageways for mounting at least one sensor component. The lid system is provided with releasable sealing elements for sealing the plurality of passageways and at least one pressing element which is common to at least a number of the sealing elements and configured for applying pressure to each of the respective sealing elements to effect the sealing of the respective passageways.

Metal supported powder catalyst matrix and processes for multiphase chemical reactions

A catalytic membrane composite that includes porous supported catalyst particles durably enmeshed in a porous fibrillated polymer membrane is provided. The porous fibrillated polymer membrane may be manipulated to take the form of a tube, disc, or diced tape and used in multiphase reaction systems. The supported catalyst particles are composed of at least one finely divided metal catalyst dispersed on a porous support substrate. High catalytic activity is gained by the effective fine dispersion of the finely divided metal catalyst such that the metal catalyst covers the support substrate and/or is interspersed in the pores of the support substrate. In some embodiments, the catalytic membrane composite may be introduced to a stirred tank autoclave reactor system, a continuous flow reactor system, or a Parr Shaker reaction system and used to effect the catalytic reaction.

CONTINUOUS PROCESS FOR PREPARING ETHYLENE GLYCOL FROM A CARBOHYDRATE SOURCE

Ethylene glycol is prepared from a carbohydrate source by reaction of the carbohydrate source with hydrogen in a continuous process, wherein hydrogen, the carbohydrate source and a liquid diluent are continuously fed into a continuous stirred tank reactor wherein a catalyst system is present, which catalyst system comprises a tungsten compound and at least one hydrogenolysis metal selected from the groups 8, 9 or 10 of the Periodic Table of the Elements, to achieve the reaction between the carbohydrate source and hydrogen to ethylene glycol; wherein continuously a product mixture comprising ethylene glycol and diluent is removed from the continuous stirred tank reactor; and wherein continuously or periodically further at least a tungsten compound is added to the continuous stirred tank reactor (CSTR).

Energy Storage Transportation Method and Energy Carrier System

An energy carrier system is provided that produces ammonia with high efficiency and that further produces hydrogen as final product and uses the hydrogen as energy. An energy storage transportation method is further provided that is carried out by using energy carrier system. The energy carrier system includes nitric acid production device, an ammonia production device, and hydrogen production device. The nitric acid production device includes a photo-reactor, a gas supply unit that supplies photo-reactor with gas to be treated containing a nitrogen oxide, water, and oxygen, and light source disposed in the photo-reactor. The light source radiates light including ultraviolet of a wavelength shorter than 175 nm. The energy storage transportation method includes nitric acid production step of producing nitric acid from a nitrogen oxide, ammonia production step of producing ammonia through reduction of nitric acid, and hydrogen production step of producing hydrogen through decomposition of the ammonia.

Reactor assembly

A reactor assembly is provided for heating plastic material. The reactor assembly includes: a reactor vessel including a central axis; and an agitator mounted within the reactor vessel. The agitator includes: one or more blade(s) distal from the central axis for mixing contents of the reactor vessel in use; and one or more wearing parts mounted to the blade(s) to extend from the blade(s).

INHERENTLY SAFE OXYGEN/HYDROCARBON GAS MIXER

Provided herein is a gas mixer for the safe mixing of a hydrocarbon containing gas with a gaseous oxidant. The gas mixer and method for mixing described includes a closed mixing vessel where bubbles of gas injected at the bottom of the vessel are mixed during their rise to the top of the vessel, forming a homogeneous mixture that can safely be removed. This simple design and method allows for safe mixing of gases and is applicable to catalytic oxidative processes such as oxidative dehydrogenation of paraffins where there is a risk of thermal runaway of reactions.

A METHOD AND A SYSTEM FOR PRODUCING AN OIL RICH FRACTION FROM BIOMASS
20230235507 · 2023-07-27 ·

The invention relates to a method for producing an oil rich fraction (OF) from primary feedstock (FS) that comprises water, first salt, second salt, and biomass. The feedstock (FS) is provided to a first reaction zone (Z1) of a conversion reactor (100), where it is allowed to react at a temperature of at least 350° C. in a pressure of at least 160 bar to form converted primary feedstock. The method comprises separating from the converted primary feedstock a first salt rich fraction (SF1), a second salt rich fraction (SF2), and an oil rich fraction (OF). The method comprises withdrawing the oil rich fraction (OF) from the first reaction zone (Z1) and withdrawing the first salt rich fraction (SF1) and the second salt rich fraction (SF2) from the conversion reactor (100). In the method the first salt rich fraction (SF1) comprises at least some of the first salt dissolved in the water, the second salt rich fraction (SF2) comprises at least some of the second salt in solid form, and at least one of the first salt and the second salt is a salt capable of catalysing the reaction of the biomass of the primary feedstock (FS) with the water of the primary feedstock (FS) to produce the oil rich fraction (OF). A device for the same.

REDUCED GRAPHENE-COBALT CHROMATE COMPOSITE COMPOSITION FOR HUMIDITY SENSOR APPLICATIONS AND ITS FABRICATION PROCESS AND SYSTEM

The present invention generally relates to a system for preparing reduced graphene-cobalt chromate composite for humidity sensor applications comprises a first glass beaker for pouring 3-7 grams of sucrose; a preheated muffle furnace for heating the first glass beaker containing sucrose for 5-15 minutes at 450-500° C. in an oxygen environment and obtaining the black foam of rGO after hydrating the sugar; a second glass beaker for mixing 3-7 grams rGO, 3-7 grams carbamide, 3-7 grams cobaltous, and 3-7 grams chromium nitrate and dissolving with double-distilled water; and a magnetic stirrer for stirring the mixed solution for 450 minutes to generate a homogenous solution and burning the uniform mixture at 425° C. in the preheated muffle furnace for 20 minutes to obtain graphene-cobalt chromate composite.

Self cleaning reactor system

This invention relates to a self cleaning reactor and to a process for the oligomerization of ethylene that employs a self-cleaning reactor. The reactor includes a mass of inert, particulate cleaning bodies that are entrained by the liquid in the reactor and scour the internal surfaces of the reactor during normal operation. This scouring action reduces the level of fouling on the reactor surfaces. Foulant material (polyethylene) is removed from the process on a continuous basis but the cleaning bodies remain within the reactor.