The invention relates to an apparatus for analyzing heterogeneously catalyzed reactions comprising at least one reactor (3) through which a particulate catalyst flows and at least one reactant feed, wherein arranged downstream of each reactor (3) is a separation apparatus (17) for separating the particulate catalyst from a reaction product comprising condensable gases and arranged downstream of the separation apparatus (17) is a liquid separator (31) for separating liquid constituents from the reaction product, wherein the liquid separator (31) comprises a metallic tube (103) and a deflection body (119), wherein the metallic tube (103) is closed at its ends and the deflection body (119) is accommodated in the metallic tube (103) and the metallic tube (103) comprises a side feed (135) at a first end (105) and a gas outlet (113) at a second end (107) and the gas outlet (113) is connected to at least one sample vessel (37). The invention further relates to a process for analyzing heterogeneously catalyzed reactions in the apparatus.

A method for controlling temperature of a chemical reaction without measuring a temperature of the chemical reaction. Changes in mass of a chemical reaction are monitored and are used to calculate the temperature of the system. The reaction can be maintained at a desired temperature (T) without measuring the temperature. The disclosed method is useful for reactions that occur at non-equilibrium conditions where any measured temperature would presume steady-state conditions.

An addition system for introducing particulate material into an industrial process is disclosed. The addition system comprises a vessel for holding the particulate material, wherein the vessel has a top and a bottom; one or more weighing devices; a controller for controlling operation of the addition system; a base plate to support the vessel and optionally the controller; and three or more legs, each leg having an uppermost section that connects to the vessel and a foot that is connected to the base plate. The widest diameter of the vessel is less than the diameter of a circle drawn through the feet of the legs. The one or more weighing device are mounted on the base plate and support the legs of the vessel.

An addition system for introducing particulate material into an industrial process is disclosed. The addition system comprises a vessel for holding the particulate material, a weighing device, piping, a controller, and a frame to support the piping. The piping comprises a first valve for transferring the particulate material to the industrial process, and a second valve for transferring a first stream of pressurized gas from a source of pressurized gas to the vessel. The vessel comprises a filling nozzle located on the top of the vessel.

Disclosed is a valve for use in particulate material processing. The valve has a rotatable closure member having a convex sealing surface and a resilient sealing ring moveable between a first configuration in which the sealing ring forms a seal around a circumference of the convex sealing surface; and a second position in which a circumferential gap is defined between the convex sealing surface and the sealing ring. The valve body defines a fluid-directing surface extending around the fluid passage between the inlet and the sealing ring to define an annular clearance which tapers towards the sealing ring and becomes narrower than the annular gap. When there is a pressure drop across the valve and before the closure member is moved to fully open the valve, material flowing through the valve experiences a dynamic pressure rise towards the circumferential gap, decreasing flow velocity and wear.

A method for controlling temperature of a chemical reaction without measuring a temperature of the chemical reaction. Changes in mass of a chemical reaction are monitored and are used to calculate the temperature of the system. The reaction can be maintained at a desired temperature (T) without measuring the temperature. The disclosed method is useful for reactions that occur at non-equilibrium conditions where any measured temperature would presume steady-state conditions.

An addition system for introducing particulate material into an industrial process is disclosed. The addition system comprises a vessel for holding the particulate material, wherein the vessel has a top and a bottom; one or more weighing devices; a controller for controlling operation of the addition system; a base plate to support the vessel and optionally the controller; and three or more legs, each leg having an uppermost section that connects to the vessel and a foot that is connected to the base plate. The widest diameter of the vessel is less than the diameter of a circle drawn through the feet of the legs. The one or more weighing device are mounted on the base plate and support the legs of the vessel.

An addition system for introducing particulate material into an industrial process is disclosed. The addition system comprises a vessel for holding the particulate material, wherein the vessel has a top and a bottom; one or more weighing devices; a controller for controlling operation of the addition system; a base plate to support the vessel and optionally the controller; and three or more legs, each leg having an uppermost section that connects to the vessel and a foot that is connected to the base plate. The widest diameter of the vessel is less than the diameter of a circle drawn through the feet of the legs. The one or more weighing device are mounted on the base plate and support the legs of the vessel.

Disclosed is a valve for use in particulate material processing. The valve has a rotatable closure member having a convex sealing surface and a resilient sealing ring moveable between a first configuration in which the sealing ring forms a seal around a circumference of the convex sealing surface; and a second position in which a circumferential gap is defined between the convex sealing surface and the sealing ring. The valve body defines a fluid-directing surface extending around the fluid passage between the inlet and the sealing ring to define an annular clearance which tapers towards the sealing ring and becomes narrower than the annular gap. When there is a pressure drop across the valve and before the closure member is moved to fully open the valve, material flowing through the valve experiences a dynamic pressure rise towards the circumferential gap, decreasing flow velocity and wear.

An addition system for introducing particulate material into an industrial process is disclosed. The addition system comprises a vessel for holding the particulate material, a weighing device, piping, a controller, and a frame to support the piping. The piping comprises a first valve for transferring the particulate material to the industrial process, and a second valve for transferring a first stream of pressurized gas from a source of pressurized gas to the vessel. The vessel comprises a quick-release hatch located on the top of the vessel.