B01J2219/00182

Method and Apparatus for Continuous Production of Mesophase Pitch
20230062059 · 2023-03-02 · ·

A process and apparatus for the continuous conversion of isotropic carbonaceous materials into anisotropic mesophase pitch is disclosed. The invention disclosed herein addresses the need for lower production costs compared with traditional batch mesophase conversion of isotropic pitch. A unique thermal processing and in-process separation of reacted mesophase from the continuous matrix of fresh or partially reacted isotropic pitch is provided. Potential uses are for further continuous processing into carbon fibers or carbon form densification.

Gas-to-gas reactor and method of using
11661384 · 2023-05-30 · ·

A device and a process to propagate molecular growth of hydrocarbons, either straight or branched chain structures, that naturally occur in the gas phase of a first gas to gas phase molecules of a second gas having higher molecular chain lengths than the hydrocarbons of the first gas. According to one embodiment, the device includes a grounded reactor vessel having a gas inlet, a product outlet, and an electrode within the vessel; a power supply coupled to the electrode for creating an electrostatic field within the vessel for converting the first gas to a second gas.

Reaction apparatus and method

Provided are an apparatus and a method for reaction for use in a co-precipitation reaction for preparing a catalyst or a cathode active material for a lithium secondary battery, which injects a raw material (a solution) at least between impellers according to the solution level in a vessel, thereby making a stirring speed uniform and, in particular, minimizing a concentration difference between solutions. The apparatus for the reaction may comprise: a reaction vessel; a stirring means provided inside the reaction vessel and having multistage impellers; and a raw material injecting means, comprising at least one injection nozzle connected to the reaction vessel, for injecting a raw material at least between impellers.

SYNTHETIC PRODUCT PRODUCTION SYSTEM AND CARBON DIOXIDE TREATMENT SYSTEM

A synthetic product production system is provided with: a synthesis plant for producing a synthetic product by synthesizing a hydrogen-containing gas and carbon dioxide; and a carbon dioxide supply line for supplying the carbon dioxide to the synthesis plant from a recovery and storage plant including a recovery device for recovering the carbon dioxide from a carbon dioxide-containing gas and an injection facility for fixing the recovered carbon dioxide into a stratum.

APPARATUS AND METHOD FOR ESTERIFICATION REACTION

An esterification reaction apparatus and an esterification reaction method, the esterification reaction apparatus comprising a reaction tank having an accommodation part, in which a raw material containing carboxylic acid and alcohol is accommodated, a heating unit configured to individually heat partition regions that are partitioned into N regions in a vertical direction of the accommodation part, and a controller configured to control the heating unit so that only the partition regions in which a liquid is accommodated among the N partition regions are heated, thereby performing an esterification reaction of the raw material.

Thermal conversion vessel used in a process for amidification of acetone cyanohydrin

The invention relates to a thermal conversion vessel (200) used during amidification step of acetone cyanohydrin (ACH), in the industrial process for production of a methyl methacrylate (MMA) or methacrylic acid (MAA). The thermal conversion vessel (200) is used for converting an hydrolysis mixture of α-hydroxyisobutyramide (HIBAM), α-sulfatoisobutyramide (SIBAM), 2-methacrylamide (MACRYDE) and methacrylique acid (MAA), into a mixture of 2-methacrylamide (MACRYDE). It comprises:—at least one compartment (C1, C2, C3, . . . Ci) comprising an inner wall (206a, 206b, . . . 206i) separating said compartment into two communicating parts (C1a, C1b) by a passage provided between the bottom of said vessel and said inner wall,—said compartment having a space above said inner wall, for separating gas phase from liquid phase during thermal conversion,—said compartment being connected to an outlet valve (204a, 204b, . . . 204i). Such vessel allows obtaining a high yield thermal conversion in very safe conditions.

Evaporative gas generating device, method for producing evaporative gas, hydrogen bromide production device, and method for producing hydrogen bromide
09835325 · 2017-12-05 · ·

An evaporative gas generating device and a method for producing evaporative gas. A hydrogen bromide production device and a method for producing hydrogen bromide are also disclosed. The hydrogen bromide production device is provided with an evaporative gas generating device (1) that generates bromine gas, and a reactor (3) that reacts the bromine gas with hydrogen gas to form hydrogen bromide. The evaporative gas generating device (1) is provided with a container (10) that accommodates liquid bromine (B), and heating jackets (35, 36) that supply heat to a wall surface of the container (10), and heat and evaporate the liquid bromine (B) within a liquid accommodating part (15) of the container (10) to raise the temperature of the bromine gas within the evaporative gas accommodating part (16).

Multi-compartment reactor and method for controlling retention time in a multi-compartment reactor

A method is disclosed for controlling retention time in a reactor, such as an autoclave, having a plurality of compartments separated by dividers with underflow openings. A retention time of the reaction mixture is calculated and compared with an optimal retention time, and the volumes of the reaction mixture in the compartments are adjusted while maintaining the flow rate of the reaction mixture, so as to change the retention time to a value which is closer to the optimal retention time. The reactor may include a level sensor in the last compartment for generating volume data; a control valve for controlling the liquid level in the last compartment; and a controller which receives volume data from the level sensor and controls operation of the control valve.

SOLID-LIQUID PHASE REACTOR FOR PREPARING POWER PRODUCT
20230173446 · 2023-06-08 ·

The present disclosure relates to the field of reactor technologies and in particular to a solid-liquid phase reactor for preparing a powder product, which includes a vessel shell, a material-restricting partition net, a solid reactant charge opening, and a reaction solution make-up opening. The material-restricting partition net is disposed in a cavity of the vessel shell and connected to the vessel shell. The material-restricting partition net is enclosed to form a semi-closed material-restricting zone with an upward-facing opening itself or together with an inner wall of a vessel. A frame of the semi-closed material-restricting zone is rigid. The solid reactant charge opening is in communication with the facing-up opening of the semi-closed material-restricting zone, and the reaction solution make-up opening is in communication with an internal space of the semi-closed material-restricting zone.

Pressure vessel with flushing device

The invention relates to a pressure vessel, having: a reaction chamber (2) as a pressure space for the initiation and/or facilitation of chemical and/or physical pressure reactions of samples (P) accommodated in the reaction chamber (2); a fluid inlet (20) with a feed valve (21) which is adjustable between an open position, for the feed of a fluid, preferably a flushing gas, into the reaction chamber (2), and a closed position, for stopping the feed of the fluid; a fluid outlet (30) with a discharge valve (31), which is adjustable between an open position, for the discharge of a fluid out of the reaction chamber (2), and a closed position, for stopping the discharge of the fluid out of the reaction chamber (2); and an oxygen sensor (33) for detecting an oxygen content in the reaction chamber (2). The pressure vessel (1) furthermore has a control device which is configured to control the feed valve (21) and the discharge valve (31) on the basis of the oxygen content detected by the oxygen sensor (33), such that the reaction chamber (2) is flushed via the feed and discharge valves (21, 31) situated in the open position, and at least the discharge valve (31) switches from the open position into the closed position as soon as a predetermined oxygen content is undershot. The invention also relates to a corresponding method.