A synthesis method and a synthesis device of cyclododecene according to the present invention have a high conversion rate of cyclododecatriene which is a reactant and a high selectivity of cyclododecene which is a required product, and even so, have an effect of significantly decreasing a reaction time. In addition, the method and the device have an excellent conversion rate of cyclododecatriene and an excellent selectivity of cyclododecene, while maintaining excellent reactivity without an organic solvent such as ethanol. Therefore, a volume of the reactor relative to an output of cyclododecene may be further decreased. Moreover, the method and the device may minimize costs for facilities and process, are practical, decrease a process time, and are industrially advantageous for mass production as compared with the conventional art.

The invention relates to a process for preparing a solid support for a procatalyst suitable for preparing a catalyst composition for olefin polymerization, said process for preparing said solid support comprising reacting a compound R.sup.4.sub.zMgX.sup.4.sub.2-z with a silane compound Si(OR.sup.5).sub.4-n(R.sup.6).sub.n in a solvent and mixing the resulting mixture with a mixing device and at a certain mixing speed in order to give a solid support Mg(OR.sup.1).sub.xX.sup.1.sub.2-x said solid support obtained having an average particle size of at most 17 μm, preferably at most 16 or 14 μm, more preferably at most 12 μm. The invention further relates to a solid support, a process for preparing a procatalyst and said procatalyst as well as polyolefins obtained using said procatalyst.

The present invention addresses the problem of providing a method for producing microparticles. Composite microparticles are separated by mixing at least two kinds of fluids to be processed in a thin film fluid that is formed between approachable and separable opposing processing surfaces that relatively rotate, wherein the fluids to be processed are a metal fluid comprising at least two kinds of metal elements that are dissolved in a solvent in the form of metal and/or metal compound and a fluid for separation containing at least one kind of separating substance for separating a composite substance comprising the at least two kinds of metal elements. The molar ratio between the at least two kinds of metal elements contained in the resulting microparticles is controlled by controlling the circumferential speed of the rotation at a confluence where the metal fluid and the fluid for separation merge at this time.

A process for washing a particulate substance comprising: (i) combining a particulate substance and a first washing medium in a first vessel to form a slurry and washing the particulate substance with said washing medium; (ii) transferring the slurry to a hydrocyclone; (iii) removing a first by-product stream depleted in particulate substance and a first product stream enriched in particulate substance from the hydrocyclone; (iv) transferring the first product stream to a second vessel and in the presence of a second washing medium forming a slurry and washing the particulate substance with said second washing medium e.g. by agitation thereof; (v) transferring the slurry to a hydrocyclone; (vi) removing a second by-product stream depleted in particulate substance and a second product stream enriched in particulate substance from the hydrocyclone.

A method of manufacture of high-solids hydroxide slurries from caustic calcined carbonate powder is described, whereby the properties of the slurry are its low resistance to shear thinning to facilitate transport, a high stability for transport and storage, ease of reconstitution after long periods of storage, and, as required, a high concentration of chemically reactive species at the particle surface. The method achieves these specifications by mixing caustic calcined carbonate or hydroxide powder with water in an insulated reactor vessel, and agitating the slurry sufficiently such that the hydration reaction causes the water to spontaneously boil, such that the remaining hydration proceeds spontaneously under the fixed conditions of boiling through the water loss. The mixing process is preferably carried out by a shear pump. A viscosity modifier, such as acetic acid, is used to thin the slurry to enable the mixing system to maintain uniform mixing. The reaction is terminated when the boiling has spontaneously ceased and the temperature has spontaneously dropped to a set point though the reactor heat losses, where the processing time is sufficiently long that the slurry meets the desired specifications.

Disclosed herein is a constant shear continuous reactor device, comprising: an annular gas delivery tube comprising a gas inlet and a gas outlet; a first annular liquid delivery tube comprising a first liquid inlet and a first liquid outlet arranged concentrically around the annular gas delivery tube along a common axis, where the first liquid outlet is located at a downstream position relative to the gas outlet or is coterminous with the gas outlet; and an annular reactor wall tube comprising a final liquid inlet, a mixing zone section and a reactor outlet, where the annular reactor wall tube is arranged concentrically around the first annular liquid delivery tube along the common axis.

A reactor system for producing modacrylic polymer having a main tank with at least one feed inlet, a mixing element inside the main tank, a secondary tank connected to the main tank with an overflow channel, a reaction terminator feed and a level meter for the secondary tank, an outlet at the bottom of the secondary tank, a level control valve that controls the outlet, a collection area connected to the outlet, and a control unit configured to control the level control valve to determine output amount to be transferred to the collection area from the secondary tank according to data received from the level meter in order to keep the level in the secondary tank constant. The temperature in the main tank and the secondary tank is continuously measured and the main tank and the secondary tank temperature difference is arranged such that it does not exceed +5° C.

An apparatus to simulate biocide performance in crude oil pipeline conditions is disclosed. The apparatus includes: a reactor to simulate a two-phase crude oil pipeline which includes a crude oil phase above a water phase. The reactor has an agitator to control a flow of the water phase in the reactor in response to a motor that drives an agitation rate of the agitator. A crude oil inlet supplies crude oil to the reactor for the crude oil phase. A water inlet supplies water to the reactor for the water phase. A control circuit is configured by code to control a proportion of the water to the crude oil supplied to the reactor and to control the motor to drive a desired agitation rate of the agitator. A biocide inlet supplies biocide to the reactor. A water sample outlet enables sampling of the water phase of the reactor.

A synthesis reactor including a container and a control unit is provided. The container includes an outer shell, an inner tank that is disposed in the outer shell and that cooperates with the outer shell to define an interlayer space therebetween, and a heater that is disposed in the interlayer space and that is attached directly to an outer surface of the inner tank. The control unit includes a controller that is electrically connected to the heater and that is configured to control heating temperature of the heater.

The present invention is concerned with a process for providing a homogeneous particle-containing slurry comprising the steps of:

(a) providing a vessel comprising at least one impeller rotating around a vertical axis of the vessel, the vessel further comprising an inlet and an outlet;
(b) introducing the particle-containing slurry into the vessel or introducing components forming the particle-containing slurry into the vessel;
(c) rotating the at least one impeller at least around the vertical axis for homogenizing and/or maintaining a homogeneous particle distribution within the slurry;
(d) withdrawing the homogeneous particle-containing slurry via the outlet;
(e) stopping the at least one impeller for a maximum time T, whereby T is calculated according to the following relations:

[00001]$\begin{array}{cc}{u}_T=\sqrt{\frac{4g\left({\rho }_p-{\rho }_f\right)D_p}{3{\rho }_f{C}_D}}& \left(1\right)\\ C_D=\frac{24}{\mathrm{Re}}\left[1+0.173{\mathrm{Re}}^{0.657}\right]& \left(2\right)\\ T=\frac{h}{u_T}& \left(3\right)\end{array}$