Patent classifications
B01J2219/1245
Device and process for producing undecylenic acid methyl ester using methyl ricinoleate as raw material
A device and a process for producing undecylenic acid methyl ester using methyl ricinoleate as raw material are provided. The device comprises a feed pump, a raw material pre-heater, a microwave catalytic reactor, a microwave generator, a temperature controller and an infrared sensor, a condenser, a product tank and a discharge pump. The feed pump is connected with the raw material pre-heater, which is connected with the inlet of the microwave catalytic reactor. The outlet of the microwave catalytic reactor is connected with the condenser, which is connected to the product tank and the discharge pump. The microwave catalytic reactor is located in the microwave generator, which is connected with the temperature controller and the infrared sensor. The process is as follows: high-purity methyl ricinoleate, used as the raw material, is converted to methyl undecene and heptaldehyde by microwave-assisted pyrolysis process, followed by isolation and purification to produce methyl undecene.
Chemical reaction apparatus
In order to provide a chemical reaction apparatus that can suppress a situation where microwaves are concentrated on a partial portion in a reactor, and that can more uniformly irradiate a content with the microwaves, a chemical reaction apparatus includes: a horizontal flow-type reactor in which a liquid content horizontally flows with an unfilled space being provided thereabove; a microwave generator that generates microwaves; and a waveguide that transmits the microwaves generated by the microwave generator to the unfilled space in the reactor, wherein a top of the reactor is curved with respect to a flow direction of the content.
METHOD FOR THERMAL PRECONDITIONING OF NATURAL GRAPHITE FLAKES USING ELECTROMAGNETIC WAVES
An apparatus for processing graphite particles is disclosed. The apparatus may comprise an electromagnetic radiation emitting device including a microwave device coupled to the reaction chamber for the creation of electromagnetic waves, the electromagnetic waves comprising microwaves. The apparatus may also comprise an inlet attached to the reaction chamber for introducing graphite particles, and an outlet attached to the reaction chamber for allowing processed graphite particles to exit the reaction chamber. The graphite particles in the reaction chamber thermally altered by exposure to the electromagnetic radiation such that the graphite particles are heated
Chemical reaction method using chemical reaction apparatus
A chemical reaction method includes preparing a chemical reaction apparatus including a horizontal flow reactor partitioned into multiple chambers by multiple partition plates. A liquid content horizontally flows with an unfilled space provided thereabove. a microwave generator and a waveguide that transmits microwaves to the unfilled space are also included. The reactor is inclined such that, in each of the chambers, a weir height on an inlet side is higher than a weir height on an outlet side by at least an overflow depth at the partition plate on the outlet side. The content is flowed over each of the multiple partition plates inside the reactor. The content flowing inside the reactor is irradiated with microwaves. The inclination angle of the reactor is changed in each of the chambers so that a weir height on an inlet side is higher than a weir height on an outlet side.
Heavy fossil hydrocarbon conversion and upgrading using radio-frequency or microwave energy
Conversion of heavy fossil hydrocarbons (HFH) to a variety of value-added chemicals and/or fuels can be enhanced using microwave (MW) and/or radio-frequency (RE) energy. Variations of reactants, process parameters, and reactor design can significantly influence the relative distribution of chemicals and fuels generated as the product. In one example, a system for flash microwave conversion of HFH includes a source concentrating microwave or RF energy in a reaction zone having a pressure greater than 0.9 atm, a continuous feed having HFH and a process gas passing through the reaction zone, a HFH-to-liquids catalyst contacting the HFH in at least the reaction zone, and dielectric discharges within the reaction zone. The HFH and the catalyst have a residence time in the reaction zone of less than 30 seconds. In some instances, a plasma can form in or near the reaction zone.
Heavy fossil hydrocarbon conversion and upgrading using radio-frequency or microwave energy
Conversion of heavy fossil hydrocarbons (HFH) to a variety of value-added chemicals and/or fuels can be enhanced using microwave (MW) and/or radio-frequency (RF) energy. Variations of reactants, process parameters, and reactor design can significantly influence the relative distribution of chemicals and fuels generated as the product. In one example, a system for flash microwave conversion of HFH includes a source concentrating microwave or RF energy in a reaction zone having a pressure greater than 0.9 atm, a continuous feed having HFH and a process gas passing through the reaction zone, a HFH-to-liquids catalyst contacting the HFH in at least the reaction zone, and dielectric discharges within the reaction zone. The HFH and the catalyst have a residence time in the reaction zone of less than 30 seconds. In some instances, a plasma can form in or near the reaction zone.
Chemical reaction apparatus
In order to suppress discharge of an unreacted content in a chemical reaction apparatus for irradiating a content with microwaves, a chemical reaction apparatus includes: a horizontal flow-type reactor in which a liquid content horizontally flows with an unfilled space being provided thereabove; a microwave generator that generates microwaves; and a waveguide that transmits the microwaves generated by the microwave generator to the unfilled space in the reactor, wherein the inside of the reactor is partitioned into multiple chambers to by overflow-type partition plates and that allow the content to flow thereover and an underflow-type partition plate that allows the content to flow thereunder.
Ferromagnetic-particle manufacturing apparatus
A method for manufacturing a ferromagnetic-particle includes preparing a manufacturing apparatus including a single mode cavity that resonates with a microwave of a predetermined wavelength; a microwave oscillator electrically connected to the single mode cavity and configured to introduce the microwave of a predetermined wavelength into the single mode cavity; a pipe disposed to pass linearly through an inside of the single mode cavity, the pipe being formed of a dielectric material; and a pump configured to introduce, from one end of the pipe, an alkaline reaction liquid in which metal ions of a ferromagnetic metal and hydroxide ions are dissolved; and reacting the reaction liquid in the pipe, introduced by the pump, by introducing the microwave into the single mode cavity so as to generate the ferromagnetic-particle in the pipe.
Ferromagnetic-particle manufacturing apparatus
A method for manufacturing a ferromagnetic-particle includes preparing a manufacturing apparatus including an induction heating coil; a radiofrequency power source electrically connected to the induction heating coil and configured to form an alternating field inside the induction heating coil; a pipe disposed to pass through the induction heating coil, in which at least a partial area of the pipe in an axial direction thereof is formed of a dielectric material and an area, which is nearer to one end of the pipe than the area formed of a dielectric material, is formed of a conductive material; and a pump configured to introduce, from the one end of the pipe, an alkaline reaction liquid in which metal ions of a ferromagnetic metal and hydroxide ions are dissolved; reacting the reaction liquid in the pipe, introduced by the pump, by forming an alternating field inside the induction heating coil; and generating the ferromagnetic-particle in the pipe based on the reaction of the reaction liquid in the pipe.
CHEMICAL REACTION METHOD USING CHEMICAL REACTION APPARATUS
A chemical reaction method includes preparing a chemical reaction apparatus including a horizontal flow reactor partitioned into multiple chambers by multiple partition plates. A liquid content horizontally flows with an unfilled space provided thereabove. a microwave generator and a waveguide that transmits microwaves to the unfilled space are also included. The reactor is inclined such that, in each of the chambers, a weir height on an inlet side is higher than a weir height on an outlet side by at least an overflow depth at the partition plate on the outlet side. The content is flowed over each of the multiple partition plates inside the reactor. The content flowing inside the reactor is irradiated with microwaves. The inclination angle of the reactor is changed in each of the chambers so that a weir height on an inlet side is higher than a weir height on an outlet side.