The present technique presents a structured packing module 100 for a gas phase reactor 2, the structured packing module 100 comprising a structured packing 1 having a central axis 5x extending along a longitudinal direction, and may further comprise an inner tube 5 extending coaxially with the structured packing and along the longitudinal direction. The structured packing 1 includes a plurality of corrugated sheets 10, 20, 30, each arranged circumferentially around the central axis 5x and having a first end 101 and a second end 102 spaced apart from each other along the longitudinal direction. Each corrugated sheet 10, 20, 30 includes corrugations 9 extending between the first end 101 and the second end 102 and disposed at an acute angle A greater than or equal to 5 degree and less than or equal to 30 degree with respect to a line 5y parallel to the central axis 5x. The corrugated sheets 10, 20, 30 are arranged to radially overlap with each other such that the corrugations 9 of adjacently disposed corrugated sheets 10, 20, 30 are arranged in a crisscross relationship. The structured packing module 100 includes a gas flow path 40 comprising at least one inter-sheet gas flow path 42 defined between the adjacently disposed corrugated sheets 10, 20, 30.

A reactor for the synthesis of urea comprising a vertical shell and perforated baffles or trays (3) arranged to define compartments of the reactor, wherein each baffle comprises an array of individual perforated tiles (10) wherein each tile (101) comprises side walls (101A-101D) and a top face (101F), the side walls having first perforations for the liquid and said top face having second perforations for the gas, wherein said second perforations are smaller than said first perforations, and the tiles are distributed over the baffle with a two-dimensional pattern where adjacent tiles are separated by gaps (17).

A device is provided having a structure for conducting a first fluid, the structure having in addition an interface for conducting a second fluid. The first fluid can be brought into contact with the second fluid at the interface of the structure. A flow interrupter (120.0) for interrupting a flow of the second fluid is situated at the interface of the structure.

A method for enabling gas exchange and chemical reactions with one or more liquid streams contained in a reactive process vessel are provided. One or more exchange layers within the process vessel can be composed of both collector media and releaser media. The exchange layers allow elements to facilitate increased performance of vessel operations by promoting gas component mixing and diffusion. Improved rates of gas component exchange mean less coking and more gas components available for reaction.

A process for performing a continuous gas/liquid biphasic high-pressure reaction, wherein a gas and a liquid are introduced into a backmixed zone of a reactor and in the backmixed zone the gas is dispersed in the liquid by stirring, injection of gas and/or a liquid jet, a reaction mixture consecutively traverses the backmixed zone and a zone of limited backmixing, and a liquid reaction product is withdrawn at a reaction product outlet of the zone of limited backmixing, wherein the reactor comprises: an interior formed by a cylindrical vertically oriented elongate shell, a bottom and a cap, wherein the interior is divided by means of internals into the backmixed zone, the zone of limited backmixing and a cavity, a first cylindrical internal element which in the interior extends in the longitudinal direction of the reactor and which delimits the zone of limited backmixing from the backmixed zone, backmixing-preventing second internal elements in the form of random packings, structured packings or liquid-permeable trays arranged in the zone of limited backmixing and a third internal element which in the interior extends in the longitudinal direction of the reactor and is open at the bottom, wherein the third internal element forms the cavity in which gas bubbles collect and do not escape upwards, thus preventing the volume of the cavity from being occupied by liquid and reducing the reaction volume. The reaction volume of the reactor used in the process can be reversibly reduced in simple fashion. The invention further relates to a process for adapting the reaction volume of a reactor suitable for performing a gas/liquid biphasic high-pressure reaction having an outlet for a liquid reaction product in which an internal element is arranged so as to form a cavity open at the bottom in which gas bubbles collect and do not escape upwards, thus preventing the volume of the cavity from being occupied by liquid and reducing the reaction volume.

A process for performing a continuous gas/liquid biphasic high-pressure reaction, wherein a gas and a liquid are introduced into a backmixed zone of a reactor and in the backmixed zone the gas is dispersed in the liquid by stirring, injection of gas and/or a liquid jet, a reaction mixture consecutively traverses the backmixed zone and a zone of limited backmixing, and a liquid reaction product is withdrawn at a reaction product outlet of the zone of limited backmixing, wherein the reactor comprises: an interior formed by a cylindrical vertically oriented elongate shell, a bottom and a cap, wherein the interior is divided by means of internals into the backmixed zone, the zone of limited backmixing and a cavity, a first cylindrical internal element which in the interior extends in the longitudinal direction of the reactor and which delimits the zone of limited backmixing from the backmixed zone, backmixing-preventing second internal elements in the form of random packings, structured packings or liquid-permeable trays arranged in the zone of limited backmixing and a third internal element which in the interior extends in the longitudinal direction of the reactor and is open at the bottom, wherein the third internal element forms the cavity in which gas bubbles collect and do not escape upwards, thus preventing the volume of the cavity from being occupied by liquid and reducing the reaction volume. The reaction volume of the reactor used in the process can be reversibly reduced in simple fashion. The invention further relates to a process for adapting the reaction volume of a reactor suitable for performing a gas/liquid biphasic high-pressure reaction having an outlet for a liquid reaction product in which an internal element is arranged so as to form a cavity open at the bottom in which gas bubbles collect and do not escape upwards, thus preventing the volume of the cavity from being occupied by liquid and reducing the reaction volume.

A device is provided having a structure for conducting a first fluid, the structure having in addition an interface for conducting a second fluid. The first fluid can be brought into contact with the second fluid at the interface of the structure. A flow interrupter (120.0) for interrupting a flow of the second fluid is situated at the interface of the structure.

A device is provided having a structure for conducting a first fluid, the structure having in addition an interface for conducting a second fluid. The first fluid can be brought into contact with the second fluid at the interface of the structure. A flow interrupter (120.0) for interrupting a flow of the second fluid is situated at the interface of the structure.

A method for enabling gas exchange and chemical reactions with one or more liquid streams contained in a reactive process vessel are provided. One or more exchange layers within the process vessel can be composed of both collector media and releaser media. The exchange layers allow elements to facilitate increased performance of vessel operations by promoting gas component mixing and diffusion. Improved rates of gas component exchange mean less coking and more gas components available for reaction.

The present invention relates to different liquid distributors for monolith in multiphase applications. The present invention more particularly relates to distributor devices in the form of a single injection and multiple injection pipe distributors; shower head distributor comprising a plurality of holes for plunging liquid; a packing of spherical particles with a pre-distributor to split the liquid into manifold streams, before entry into the monolith bed. The present invention provides liquid distributors for monolith in multiphase applications providing improved liquid distribution into the monolith bed resulting in uniform fluid flow in each channel so as to make maximum use of the catalyst surface area.