B01J47/02

PRODUCTION APPARATUS OF NON-AQUEOUS ELECTROLYTE SOLUTION AND PRODUCTION METHOD OF NON-AQUEOUS ELECTROLYTE SOLUTION
20230052583 · 2023-02-16 · ·

Provided is a production apparatus of a non-aqueous electrolyte solution that can produce conveniently and at a low cost the non-aqueous electrolyte solution while readily controlling an acidic impurity concentration so as to be in a prescribed level.

The production apparatus of the non-aqueous electrolyte solution includes an original liquid tank that stores a liquid to be processed containing a non-aqueous electrolyte solution, and an ion-exchange resin container that accommodates a weakly basic anion-exchange resin, and also including a liquid circulation pipe that returns the liquid to be processed that is obtained after flowing the liquid to be processed from the original liquid tank through the ion-exchange resin container to the original liquid tank.

METHOD FOR MANUFACTURING IRON-CHROMIUM OXIDE USING ION EXCHANGE RESIN

The present invention relates to a method of preparing an iron-chromium oxide using an ion-exchange resin. Moreover, the present invention relates to a method of preparing an iron-chromium oxide that can be used as a cathode material for lithium-ion batteries. According to one aspect of the present invention, it has the effect of providing a cathode material for lithium-ion batteries with a high capacitance, while exhibiting a voltage similar to that of a transition-metal oxide (2-4.5 V vs Li.sup.+/Li).

METHOD FOR MANUFACTURING IRON-CHROMIUM OXIDE USING ION EXCHANGE RESIN

The present invention relates to a method of preparing an iron-chromium oxide using an ion-exchange resin. Moreover, the present invention relates to a method of preparing an iron-chromium oxide that can be used as a cathode material for lithium-ion batteries. According to one aspect of the present invention, it has the effect of providing a cathode material for lithium-ion batteries with a high capacitance, while exhibiting a voltage similar to that of a transition-metal oxide (2-4.5 V vs Li.sup.+/Li).

NEW LITHIUM-SODIUM SEPARATION METHOD
20230017362 · 2023-01-19 ·

Disclosed is a new continuous lithium-sodium separation method. A lithium-sodium separation mother solution, a first leacheate, a desorption solution, a second leacheate and a lithium-sodium separation adsorption tail solution respectively pass through a lithium-sodium separation mother solution feeding pipe (2), a first leacheate feeding pipe (3), a desorption solution feeding pipe (4), a second leacheate feeding pipe (5) and an adsorption tail solution top desorption solution feeding pipe (6) that are located above and below a rotary disc of a multi-way change-over valve system (1), respectively enter corresponding resin columns (7) by means of pore channels and channels in the multi-way change-over valve system (1), and then are discharged from an adsorption tail solution discharging pipe (8), a first leacheate discharging pipe (9), a qualified liquid discharging pipe (10), a second leacheate discharging pipe (11) and an adsorption tail solution top desorption solution discharging pipe (12), so as to complete the whole technological process, wherein the resin columns (7) are connected in series or in parallel by means of the channels located in the multi-way change-over valve system (1). The method is simple and easy to operate, the resin utilization rate is improved by 20% or more, the efficiency is improved by 40% or more, and the production cost can be reduced by 30-50%. The production reliability is improved, and all-year continuous operation can be realized.

NEW LITHIUM-SODIUM SEPARATION METHOD
20230017362 · 2023-01-19 ·

Disclosed is a new continuous lithium-sodium separation method. A lithium-sodium separation mother solution, a first leacheate, a desorption solution, a second leacheate and a lithium-sodium separation adsorption tail solution respectively pass through a lithium-sodium separation mother solution feeding pipe (2), a first leacheate feeding pipe (3), a desorption solution feeding pipe (4), a second leacheate feeding pipe (5) and an adsorption tail solution top desorption solution feeding pipe (6) that are located above and below a rotary disc of a multi-way change-over valve system (1), respectively enter corresponding resin columns (7) by means of pore channels and channels in the multi-way change-over valve system (1), and then are discharged from an adsorption tail solution discharging pipe (8), a first leacheate discharging pipe (9), a qualified liquid discharging pipe (10), a second leacheate discharging pipe (11) and an adsorption tail solution top desorption solution discharging pipe (12), so as to complete the whole technological process, wherein the resin columns (7) are connected in series or in parallel by means of the channels located in the multi-way change-over valve system (1). The method is simple and easy to operate, the resin utilization rate is improved by 20% or more, the efficiency is improved by 40% or more, and the production cost can be reduced by 30-50%. The production reliability is improved, and all-year continuous operation can be realized.

ION EXCHANGE SYSTEM AND METHOD FOR CONVERSION OF AQUEOUS LITHIUM SOLUTION
20230019776 · 2023-01-19 ·

Systems and methods use ion exchange to extract lithium from a lithium-containing feed solution such as a salar brine. Lithium ions are loaded into an ion exchange resin and then eluted while recharging the resin. Sodium hydroxide or sodium bicarbonate may be used to recharge the resin but are not directly mixed with the lithium-containing feed solution. An eluate stream is produced containing lithium hydroxide or lithium bicarbonate. Lithium hydroxide can be precipitated as lithium hydroxide or in a hydrate form. Lithium bicarbonate may be converted to lithium carbonate. The system and method optionally includes processing an eluate stream to recover one or more compounds for re-use in regenerating the resin bed.

Method for the preparation of controlled porosity supports for chromatographic separation

Disclosed herein are extraction chromatographic supports comprising a porous support, an inert filler, and metal ion binding extractant that may be used for chromatographic separation of metal ions. Also disclosed herein are methods for preparing and using the extraction chromatographic supports.

Method for the preparation of controlled porosity supports for chromatographic separation

Disclosed herein are extraction chromatographic supports comprising a porous support, an inert filler, and metal ion binding extractant that may be used for chromatographic separation of metal ions. Also disclosed herein are methods for preparing and using the extraction chromatographic supports.

Methods, compositions and kits useful for pH gradient cation exchange chromatography

The present disclosure relates to methods, compositions and kits useful for the enhanced pH gradient cation exchange chromatography of a variety of analytes. In various aspects, the present disclosure pertains to chromatographic elution buffer solutions that comprise a first buffer salt, a second buffer salt, a third buffer salt, and fourth buffer salt. The first buffer salt may be, for example, a diprotic acid buffer salt, the second buffer salt may be, for example, a divalent buffer salt with two amine groups, the third buffer salt may be, for example, a monovalent buffer salt comprising a single amine group, and the fourth buffer salt may be, for example, a zwitterionic buffer salt. Moreover, the buffer solution has a pH ranging from 3 to 11.

METHOD FOR PRODUCING LITHIUM HYDROXIDE

A method for producing lithium hydroxide that allows reducing a load of removing divalent or more ions with an ion-exchange resin is provided. The method for producing lithium hydroxide includes steps (1) to (3) below. (1) a neutralization step: a step of adding an alkali to a first lithium chloride containing liquid to obtain a post-neutralization liquid, (2) an ion-exchange step: a step of bringing the post-neutralization liquid into contact with an ion-exchange resin to obtain a second lithium chloride containing liquid, and (3) a conversion step: a step of electrodialyzing the second lithium chloride containing liquid to obtain a lithium hydroxide containing liquid. Since this producing method allows roughly removing divalent or more ions in the neutralization step, a load of metal removal with the ion-exchange resin is reducible.