The present invention provides a system and method for producing high-purity vanadium pentoxide powder. Industrial grade vanadium pentoxide is converted to vanadium oxytrichloride by low temperature fluidizing chlorination, wherein chlorinating gas is preheated via heat exchange between fluidizing gas and chlorination flue gas, and an appropriate amount of air is added to enable a part of carbon powder to combust so as to achieve a balanced heat supply during the chlorination, thereby increasing the efficiency of chlorination and ensuring good selectivity in low temperature chlorination. The vanadium oxytrichloride is purified by rectification, and then subjected to fluidized gas phase hydrolyzation and fluidized calcination, thereby producing a high-purity vanadium pentoxide product and a by-product of hydrochloric acid solution. The system and method have advantages of favorable adaptability to raw material, no discharge of contaminated wastewater, low energy consumption in production, low operation cost, stable product quality, etc.

The present invention provides a system and method for purifying and preparing vanadium pentoxide powder. Industrial grade vanadium pentoxide is converted to vanadium oxytrichloride by low temperature fluidizing chlorination, wherein chlorinating gas is preheated via heat exchange between fluidizing gas and chlorination flue gas, and an appropriate amount of air is added to enable a part of carbon powder to combust so as to achieve a balanced heat supply during the chlorination, thereby increasing the efficiency of chlorination and ensuring good selectivity in low temperature chlorination. The vanadium oxytrichloride is purified by rectification, and then subjected to fluidized gas phase ammonification, thereby obtaining ammonium metavanadate, and further obtaining a high-purity vanadium pentoxide powder product through fluidized calcination. The system and method have advantages of favorable adaptability to a raw material, no discharge of contaminated wastewater, low energy consumption and chlorine consumption in production, stable product quality and so on.

A method and system for producing nano-active powder materials. The method can be used with a reactor system comprising stages in which input particles flow under gravity progressively through stages of the reactor. A powder injector first stage in which ground input precursor powder is injected into the reactor. An externally heated preheater stage may be in the reactor, in which the precursor powder is heated to a temperature of calcination reaction. An externally heated calciner stage in the reactor, in which primary precursor volatile constituents can be rapidly removed calcination reactions as a high purity gas stream to produce the desired nano-active product. A post-processing reactor stage in which there is a change of the gas stream composition to produce the desired hot powder product by virtue of the nano-activity of the first powder material. A powder ejector stage in which the hot powder product is ejected from the reactor.

A catalyst comprising a microporous crystalline metallosilicate having a Constraint Index of 12, or 10, or 8, or 6 or less, a binder, a Group 1 alkali metal or a compound thereof and/or a Group 2 alkaline earth metal or a compound thereof, a Group 10 metal or a compound thereof, and, optionally, a Group 11 metal or a compound thereof; wherein the catalyst is calcined in a first calcining step before the addition of the Group 10 metal or compound thereof and optionally the Group 11 metal or compound thereof; and wherein the first calcining step includes heating the catalyst to first temperatures of greater than 500° C.; and wherein the catalyst is calcined in a second calcining step after the addition of the Group 10 metal or compound thereof and optionally the Group 11 metal or compound thereof wherein the second calcining step includes heating the catalyst to temperatures of greater than 400° C.

A fluidized-bed-type apparatus and method for treating gypsum, which activates or improves fluidity of gypsum powder to promote an effect of treatment of gypsum, such as modification or homogenization of the gypsum powder. The apparatus for treating gypsum includes a reactor vessel, a conditioned air supply port, a horizontal partition wall and a plurality of stationary vanes. The wall allows a conditioned air flow to flow upward into a reaction region. The vanes are arranged at an angular interval in a circumferential direction. A fluidized bed of calcined gypsum is provided in the vessel. The vane deflects the conditioned air flow flowing upward into the reaction region, toward a radially outward and circumferential direction of the reaction region. The calcined gypsum makes a saltational fluid motion or saltational movement in the vessel with the air flow.

A method of heat-treating a waste cathode material to recover lithium carbonate from the waste cathode material, and a lithium carbonate recovery method using the waste cathode material heat treatment method are provided. The method of heat-treating the waste cathode material includes heating an interior of a heat treatment furnace by burning a hydrocarbon fluid in the heat treatment furnace and producing lithium carbonate (Li.sub.2CO.sub.3) and residual metal oxide by reacting a waste cathode material in the heat treatment furnace with CO.sub.2 generated during burning of the hydrocarbon fluid.

The invention relates to a process for thermally treating, in particular synthesizing and/or drying and calcinating, a nano- and/or micro-scale or nano- and/or micro-crystalline battery material (BM) and/or battery material precursor (BM) in a thermal reactor (1), comprising the steps of: introducing a starting compound (AV) into the reactor (1), the starting material (AV) being a battery material (BM) and/or battery material precursor (BM) and the starting material (AV) being introduced into the reactor (1) in the form of a solution, slurry, suspension or in a solid state of matter, thermally treating the battery material (BM) and/or battery material precursor (BM) carried in a hot gas flow (HGS) in a treatment zone in the reactor (1) at a temperature of 150° C. to 1000° C., and discharging the battery material (BM) obtained from the reactor (1) in the form of a powder.

A process of calcining aluminium hydroxide (Al.sub.2O.sub.3.3H.sub.2O) to form alumina (Al.sub.2O.sub.3), for example in an alumina plant, such as a Bayer process plant, is disclosed. The process comprises combusting hydrogen and oxygen and generating steam and heat 5 and using the heat to calcine aluminium hydroxide and form alumina and more steam. An apparatus is also disclosed.

Systems and methods are provided for production of carbon nanotubes and H.sub.2 using a reaction system configuration that is suitable for large scale production. In the reaction system, a substantial portion of the heat for the reaction can be provided by using a heated gas stream. Optionally, the heated gas stream can correspond to a heated H.sub.2 gas stream. By using a heated gas stream, when the catalyst precursors for the floating catalyst-chemical vapor deposition (FC-CVD) type catalyst are added to the gas stream, the gas stream can be at a temperature of 1000° C. or more. This can reduce or minimize loss of catalyst precursor material and/or deposition of coke on sidewalls of the reactor. Additionally, a downstream portion of the reactor can include a plurality of flow channels of reduced size that are passed through a heat exchanger environment, such as a shell and tube heat exchanger. This can provide cooling of the gas flow after catalyst formation to allow for carbon nanotube formation, while also reducing the Reynolds number of the flow sufficiently to provide laminar flow within the region where carbon nanotubes are formed.

A method for manufacturing a carbon-containing particulate product. A starting material containing a carbonisable precursor material and/or carbon is dispersed in a gas and is conducted through a reaction zone in which at least some of the carbon contained in the product is formed, the gas flowing in a pulsed manner at least in the reaction zone