Patent classifications
B01J8/34
Devices and methods of using small form aluminum in consecutive batch aluminum chlorohydrate processes
A method of producing aluminum chlorohydrate comprises adding small form aluminum metal pellets to a reactant receiving space of a reactor tank to form a pellet bed; adding aqueous hydrochloric acid to the reactant receiving space of the reactor tank; and continuously circulating the aqueous hydrochloric acid through the pellet bed. In some embodiments, the continuously circulating aqueous hydrochloric acid dispels reaction gases from the pellet bed. Methods described herein can, in some cases, further comprise consecutively adding additional small form aluminum metal pellets to the reactant receiving space of the reactor tank as the small form aluminum metal pellets are consumed in the pellet bed.
REGENERATION DEVICE, DEVICE FOR PREPARING LOW-CARBON OLEFINS, AND USE THEREOF
A regeneration device, a device for preparing low-carbon olefins, and a use thereof are provided. The regeneration device includes a first regenerator and a second regenerator; a first activation zone of the first regenerator is connected to the second regenerator through a pipeline, such that a catalyst in the first activation zone is able to be delivered to the second regenerator; and the second regenerator is connected to a gas-solid separation zone of the first regenerator through a pipeline, such that a catalyst in the second regenerator is able to be delivered to the gas-solid separation zone. The regeneration device can adjust the coke content, coke content distribution, and coke species in a dimethyl ether/methanol to olefins (DMTO) catalyst to control an operation window of the DMTO catalyst, which improves the selectivity for low-carbon olefins and the atomic economy of a methanol-to-olefins (MTO) technology.
REGENERATION DEVICE, DEVICE FOR PREPARING LOW-CARBON OLEFINS, AND USE THEREOF
A regeneration device, a device for preparing low-carbon olefins, and a use thereof are provided. The regeneration device includes a first regenerator and a second regenerator; a first activation zone of the first regenerator is connected to the second regenerator through a pipeline, such that a catalyst in the first activation zone is able to be delivered to the second regenerator; and the second regenerator is connected to a gas-solid separation zone of the first regenerator through a pipeline, such that a catalyst in the second regenerator is able to be delivered to the gas-solid separation zone. The regeneration device can adjust the coke content, coke content distribution, and coke species in a dimethyl ether/methanol to olefins (DMTO) catalyst to control an operation window of the DMTO catalyst, which improves the selectivity for low-carbon olefins and the atomic economy of a methanol-to-olefins (MTO) technology.
FLUIDIZED BED REACTOR AND METHOD FOR OPERATING THE FLUIDIZED BED REACTOR
The present invention relates to a fluidized bed reactor comprising a reaction chamber for particulate matter, the reaction chamber having at least one particulate matter inlet (3) for the particulate matter and at least one primary particulate matter outlet for the particulate matter, and a fluidizing grate having multiple openings for an operating fluid to fluidize particulate matter above the fluidizing grate.
FLUIDIZED BED REACTOR AND METHOD FOR OPERATING THE FLUIDIZED BED REACTOR
The present invention relates to a fluidized bed reactor comprising a reaction chamber for particulate matter, the reaction chamber having at least one particulate matter inlet (3) for the particulate matter and at least one primary particulate matter outlet for the particulate matter, and a fluidizing grate having multiple openings for an operating fluid to fluidize particulate matter above the fluidizing grate.
Baffles in a fluidized bed cooler
A fluidized bed cooler for cooling a urea-containing granular material may include a cooler chamber having a product inlet opening, a product outlet opening, a perforated plate disposed in the cooler chamber, and at least one cooling medium entry opening disposed beneath the perforated plate. The product inlet opening may be disposed above the perforated plate, and a baffle plate may be disposed between the product inlet opening and the perforated plate. A distributor plate may be disposed between the baffle plate and the perforated plate. An area of the distributor plate may be 10% to 50% greater than an area of the baffle plate.
Baffles in a fluidized bed cooler
A fluidized bed cooler for cooling a urea-containing granular material may include a cooler chamber having a product inlet opening, a product outlet opening, a perforated plate disposed in the cooler chamber, and at least one cooling medium entry opening disposed beneath the perforated plate. The product inlet opening may be disposed above the perforated plate, and a baffle plate may be disposed between the product inlet opening and the perforated plate. A distributor plate may be disposed between the baffle plate and the perforated plate. An area of the distributor plate may be 10% to 50% greater than an area of the baffle plate.
METHOD FOR REGULATING THE GAS VELOCITY OF THE EMPTY BED IN A FLUIDIZED BED
The invention relates to a method for regulating the gas velocity of the empty bed in a fluidized bed, wherein solid catalysts are used as fluidized particles or as a part of fluidized particles, characterized in that the gas velocity of the empty bed μ of the reaction zone of the fluidized bed is measured, compared with the bed average catalyst density ρ of the solid catalysts in the reaction zone of the fluidized bed, the gas velocity of the empty bed μ being adjusted as required such that the gas velocity of the empty bed μ and the bed average catalyst density ρ satisfy the formula (I) below: ρ=0.356μ.sup.3−4.319μ.sup.2−35.57μ+M; wherein M=250−; where μ is provided in m/s and ρ is provided in kg/m.sup.3. The method can be used for the industrial production of lower olefin.
METHOD FOR REGULATING THE GAS VELOCITY OF THE EMPTY BED IN A FLUIDIZED BED
The invention relates to a method for regulating the gas velocity of the empty bed in a fluidized bed, wherein solid catalysts are used as fluidized particles or as a part of fluidized particles, characterized in that the gas velocity of the empty bed μ of the reaction zone of the fluidized bed is measured, compared with the bed average catalyst density ρ of the solid catalysts in the reaction zone of the fluidized bed, the gas velocity of the empty bed μ being adjusted as required such that the gas velocity of the empty bed μ and the bed average catalyst density ρ satisfy the formula (I) below: ρ=0.356μ.sup.3−4.319μ.sup.2−35.57μ+M; wherein M=250−; where μ is provided in m/s and ρ is provided in kg/m.sup.3. The method can be used for the industrial production of lower olefin.
DEVICES AND METHODS OF USING SMALL FORM ALUMINUM IN CONSECUTIVE BATCH ALUMINUM CHLOROHYDRATE PROCESSES
A method of producing aluminum chlorohydrate comprises adding small form aluminum metal pellets to a reactant receiving space of a reactor tank to form a pellet bed; adding aqueous hydrochloric acid to the reactant receiving space of the reactor tank; and continuously circulating the aqueous hydrochloric acid through the pellet bed. In some embodiments, the continuously circulating aqueous hydrochloric acid dispels reaction gases from the pellet bed. Methods described herein can, in some cases, further comprise consecutively adding additional small form aluminum metal pellets to the reactant receiving space of the reactor tank as the small form aluminum metal pellets are consumed in the pellet bed.