Techniques are disclosed for milling an iron-containing raw material in the presence of a nitrogen source to generate anisotropically shaped particles that include iron nitride and have an aspect ratio of at least 1.4. Techniques for nitridizing an anisotropic particle including iron, and annealing an anisotropic particle including iron nitride to form at least one a″-Fe16N2 phase domain within the anisotropic particle including iron nitride also are disclosed. In addition, techniques for aligning and joining anisotropic particles to form a bulk material including iron nitride, such as a bulk permanent magnet including at least one a″-Fe16N2 phase domain, are described. Milling apparatuses utilizing elongated bars, an electric field, and a magnetic field also are disclosed.

Techniques are disclosed for milling an iron-containing raw material in the presence of a nitrogen source to generate anisotropically shaped particles that include iron nitride and have an aspect ratio of at least 1.4. Techniques for nitridizing an anisotropic particle including iron, and annealing an anisotropic particle including iron nitride to form at least one a″-Fe16N2 phase domain within the anisotropic particle including iron nitride also are disclosed. In addition, techniques for aligning and joining anisotropic particles to form a bulk material including iron nitride, such as a bulk permanent magnet including at least one a″-Fe16N2 phase domain, are described. Milling apparatuses utilizing elongated bars, an electric field, and a magnetic field also are disclosed.

A method is provided for producing metal hybrid graphene. The method includes providing a ball mill chamber filled with inert gas and metal balls; inserting graphene, nanographite, and nanosized transition metal; into the chamber; turning the chamber; and extracting the metal hybrid graphene. The transition metal is at least one of nickel, copper, cobalt, tungsten, iron, chromium and/or manganese.

A cubic boron nitride sintered material includes cubic boron nitride and a binder. The binder includes a first material and a second material. The first material is one or two or more first chemical species each including at least one first metallic element selected from the group consisting of tungsten, cobalt, and aluminum. Each of the first chemical species is a metal, an alloy, an intermetallic compound, a compound, or a solid solution. The second material is one or two or more second chemical species each including at least one second metallic element selected from the group consisting of titanium, zirconium, hafnium, vanadium, niobium, tantalum, and chromium. Each of the second chemical species is a solid solution derived from at least one selected from the group consisting of nitride, carbide, and carbonitride. In each of the second chemical species, 0.1 atom % to 10 atom % of aluminum is dissolved.

Disclosed herein is a method comprising disposing a container containing a metal and/or ferromagnetic solid and abrasive particles in a static magnetic field; where the container is surrounded by an induction coil; activating the induction coil with an electrical current, to heat up the metallic or ferromagnetic solid to form a fluid; generating sonic energy to produce acoustic cavitation and abrasion between the abrasive particles and the container; and producing nanoparticles that comprise elements from the container, the metal and/or the ferromagnetic solid and the abrasive particles. Disclosed herein too is a composition comprising first metal or a first ceramic; and particles comprising carbides and/or nitrides dispersed therein. Disclosed herein too is a composition comprising nanoparticles comprising chromium carbide, iron carbide, nickel carbide, γ-Fe and magnesium nitride.

A material of formula Li.sub.aTi.sub.b(A.sub.xS.sub.3-x).sub.c wherein A is a metalloid element chosen from selenium, tellurium and mixtures thereof, and the stoichiometric coefficients a, b, c and x are such that 0<x<2.2; 0.4≤a≤4.5; 0.9≤b≤1.1; and 0.9≤c≤1.1.

Provided is a thermoelectric material having an intermetallic compound in an Al—Fe—Si system as a main component, exhibiting a thermoelectric effect in a temperature range from a room temperature to 600° C., and becoming a p-type or n-type thermoelectric material by a composition control, a manufacturing method thereof, and a thermoelectric power generation module thereof. A thermoelectric material according to the present invention including at least Al, Fe, and Si and represented by a general formula of Al.sub.12+p−qFe.sub.38.5+3qSi.sub.49.5−p−2q (where p satisfies 0≤p≤16.5 and q satisfies −0.34≤q≤0.34) and including a phase represented by Al.sub.2Fe.sub.3Si.sub.3 as a main phase.

Techniques are disclosed for milling an iron-containing raw material in the presence of a nitrogen source to generate anisotropically shaped particles that include iron nitride and have an aspect ratio of at least 1.4. Techniques for nitridizing an anisotropic particle including iron, and annealing an anisotropic particle including iron nitride to form at least one α″-Fe.sub.16N.sub.2 phase domain within the anisotropic particle including iron nitride also are disclosed. In addition, techniques for aligning and joining anisotropic particles to form a bulk material including iron nitride, such as a bulk permanent magnet including at least one α″-Fe.sub.16N.sub.2 phase domain, are described. Milling apparatuses utilizing elongated bars, an electric field, and a magnetic field also are disclosed.

Techniques are disclosed for milling an iron-containing raw material in the presence of a nitrogen source to generate anisotropically shaped particles that include iron nitride and have an aspect ratio of at least 1.4. Techniques for nitridizing an anisotropic particle including iron, and annealing an anisotropic particle including iron nitride to form at least one α″-Fe.sub.16N.sub.2 phase domain within the anisotropic particle including iron nitride also are disclosed. In addition, techniques for aligning and joining anisotropic particles to form a bulk material including iron nitride, such as a bulk permanent magnet including at least one α″-Fe.sub.16N.sub.2 phase domain, are described. Milling apparatuses utilizing elongated bars, an electric field, and a magnetic field also are disclosed.

The disclosure discloses a method for preparing a γ′-Fe.sub.4N soft magnetic material by using liquid nitrogen through high-speed ball milling, and belongs to the field of the soft magnetic material. According to the method of the disclosure, high energy in the liquid nitrogen is used for obtaining a nanometer material Fe.sub.xN with a nitrogen atom supersaturation degree through cryogrinding. At a low temperature, the material is very brittle, and a surface volume ratio is very high, so that a content of nitrogen atoms adsorbed on a surface of a sample is as high as 22%. Through 300° C. post-annealing, γ′-Fe.sub.4N is directly obtained from α-Fe through phase change, so that a nanometer crystal γ′-Fe.sub.4N soft magnetic material is prepared. The method of the disclosure has the advantages that an operation is simple and convenient, the cost is low, the large-scale industrialized production can be realized, and the method belongs to a novel alternative method for preparing a high-grade soft magnetic material with ideal magnetism. The γ′-Fe.sub.4N soft magnetic material prepared by the method of the disclosure has the advantages of high Ms, low coercivity and high surface resistivity, and can be used for a transformer and an inductor operated in a high-frequency semiconductor switch.