Sintered product having a relative density of greater than 90%, with, to more than 80% of the volume thereof, a stack of flat ceramic platelets, the assembly of the platelets having a mean thickness of less than 3 μm, having a width of greater than 50 mm, and including more than 20% of alumina, as a percentage on the basis of the weight of the product. The width of the product is the largest dimension measured in the plane in which the length of the product is measured, along a direction perpendicular to the direction of the length. The length of the product is the largest dimension thereof in a plane parallel to the general plane in which the platelets extend.

The present disclosure relates to compressed bone compositions, bone implants, and variants thereof. The present disclosure also relates to methods of preparing compressed bone compositions, bone implants, and variants thereof. The present disclosure also relates to methods of using the bone compositions, bone implants and variants thereof.

The present invention proposes an apparatus for demolding materials produced by means of the processing technique called freeze-casting. More specifically, it addresses to the application of a linear actuator to perform the sliding/extraction of solid-state parts in low-temperature condition from the containers used as a mold for manufacturing parts using freeze-casting. The device allows pressure to be applied to the material to be removed, resulting in ejection. The artifact also allows the displacement of the element with controlled displacement speed, providing the achievement of defect-free materials.

System for demolding materials obtained by means of the freeze-casting technique characterized in that it comprises a source of compressed air (1), a pressure regulator filter (2) coupled with a manometer (3), a directional valve (4), an actuator linear (5), a baton (6), a flow regulating valve (7), a fastening means (8), a metallic support (9) and a chamber for receiving the cooled material (10).

The present disclosure relates to compressed bone compositions, bone implants, and variants thereof. The present disclosure also relates to methods of preparing compressed bone compositions, bone implants, and variants thereof. The present disclosure also relates to methods of using the bone compositions, bone implants and variants thereof.

Disclosed herein is a method of: placing between a cooling element and an opposing surface a slurry of: a dielectric powder containing barium titanate, a dispersant, a binder, and water; maintaining the cooling element at a temperature below the opposing surface to cause the formation of ice platelets perpendicular to the surface of the cooling element and having the powder between the platelets; subliming the ice platelets to create voids; sintering the powder to form the dielectric material; and filling the voids with the polymeric material. The process can produce a composite having: a sintered dielectric material of barium titanate and platelets of a polymeric material embedded in the dielectric material. Each of the platelets is perpendicular to a surface of the composite.

Provided herein are methods for making a freeze-cast material having a internal structure, the methods comprising steps of: determining the internal structure of the material, the internal structure having a plurality of pores, wherein: each of the plurality of pores has directionality; and the step of determining comprises: selecting a temperature gradient and a freezing front velocity to obtain the determined internal structure based on the selected temperature gradient and the selected freezing front velocity; directionally freezing a liquid formulation to form a frozen solid, the step of directionally freezing comprising: controlling the temperature gradient and the freezing front velocity to match the selected temperature gradient and the selected freezing front velocity during directionally freezing; wherein the liquid formulation comprises at least one solvent and at least one dispersed species; and subliming the at least one solvent out of the frozen solid to form the material.

A method for building an ice structure includes making a plurality of ice logs and attaching the ice logs together to form a support structure. The support structure may be two or more stories high and may be constructed by freezing the ice logs together.

Provided herein are methods for making a freeze-cast material having a internal structure, the methods comprising steps of: determining the internal structure of the material, the internal structure having a plurality of pores, wherein: each of the plurality of pores has directionality; and the step of determining comprises: selecting a temperature gradient and a freezing front velocity to obtain the determined internal structure based on the selected temperature gradient and the selected freezing front velocity; directionally freezing a liquid formulation to form a frozen solid, the step of directionally freezing comprising: controlling the temperature gradient and the freezing front velocity to match the selected temperature gradient and the selected freezing front velocity during directionally freezing; wherein the liquid formulation comprises at least one solvent and at least one dispersed species; and subliming the at least one solvent out of the frozen solid to form the material.

A method for building an ice structure includes making a plurality of ice logs and attaching the ice logs together to form a support structure. The support structure may be two or more stories high and may be constructed by freezing the ice logs together.

Provided is a mold cooling system for the manufacturing of ceramic parts by freeze-casting including: a source (1) of cooling gas; a cooling gas cooling medium (7) fluidically connected to the cooling gas source (1); and a cooling cell (5), fluidly connected to the cooling gas cooling medium (7), including a mold (9) in its interior, wherein the cooling cell (5) includes a refrigerated cooling gas injection opening. Thus, a mold cooling system is provided for the manufacturing of ceramic parts by freeze-casting including the stages of: refrigerating a cooling gas coming from a cooling gas source (1); and injecting a cooling gas that is refrigerated in a cooling cell (5) including a mold (9) in its interior.