C01B33/143

METHOD FOR MANUFACTURE OF MESOPOROUS SILICA IN THE PRESENCE OF WATER-SOLUBLE ODSO
20220411274 · 2022-12-29 ·

Methods of synthesis of mesoporous silica are disclosed. The mesoporous silica synthesized herein, like SBA-15, possesses a two-dimensional, hexagonal, through-hole structure with a space group p6mm. An effective quantity of one or more water-soluble oxidized disulfide oil (ODSO) compounds are used during synthesis to impart distinct characteristics.

METHOD FOR MANUFACTURE OF MESOPOROUS SILICA IN THE PRESENCE OF WATER-SOLUBLE ODSO
20220411274 · 2022-12-29 ·

Methods of synthesis of mesoporous silica are disclosed. The mesoporous silica synthesized herein, like SBA-15, possesses a two-dimensional, hexagonal, through-hole structure with a space group p6mm. An effective quantity of one or more water-soluble oxidized disulfide oil (ODSO) compounds are used during synthesis to impart distinct characteristics.

METHOD FOR MANUFACTURE OF MESOPOROUS SILICA IN THE PRESENCE OF THERMALLY EXPANDABLE MICROCELLS
20220396489 · 2022-12-15 ·

Methods of synthesis of mesoporous silica are disclosed. The mesoporous silica synthesized herein, like SBA-15, possesses a two-dimensional, hexagonal, through-hole structure with a space group p6mm. An effective quantity of one or more thermally expandable microcells are used during synthesis to impart distinct characteristics.

METHOD FOR MANUFACTURE OF MESOPOROUS SILICA IN THE PRESENCE OF THERMALLY EXPANDABLE MICROCELLS
20220396489 · 2022-12-15 ·

Methods of synthesis of mesoporous silica are disclosed. The mesoporous silica synthesized herein, like SBA-15, possesses a two-dimensional, hexagonal, through-hole structure with a space group p6mm. An effective quantity of one or more thermally expandable microcells are used during synthesis to impart distinct characteristics.

Method for manufacture of mesoporous silica in the presence of water-soluble ODSO

Methods of synthesis of mesoporous silica are disclosed. The mesoporous silica synthesized herein, like SBA-15, possesses a two-dimensional, hexagonal, through-hole structure with a space group p6mm. An effective quantity of one or more water-soluble oxidized disulfide oil (ODSO) compounds are used during synthesis to impart distinct characteristics.

Method for manufacture of mesoporous silica in the presence of water-soluble ODSO

Methods of synthesis of mesoporous silica are disclosed. The mesoporous silica synthesized herein, like SBA-15, possesses a two-dimensional, hexagonal, through-hole structure with a space group p6mm. An effective quantity of one or more water-soluble oxidized disulfide oil (ODSO) compounds are used during synthesis to impart distinct characteristics.

HYBRID ORGANIC-INORGANIC NANO-PARTICLES

The invention relates to a method of making hybrid organic-inorganic core-shell nano-particles, comprising the steps of a) providing colloidal organic particles comprising a synthetic polyampholyte as a template; b) adding at least one inorganic oxide precursor; and c) forming a shell layer from the precursor on the template to result in core-shell nano-particles. With this method it is possible to make colloidal organic template particles having an average particle size in the range of 10 to 300 nm; which size can be controlled by the comonomer composition of the polyampholyte, and/or by selecting dispersion conditions.

The invention also relates to organic-inorganic or hollow-inorganic core-shell nano-particles obtained with this method, to compositions comprising such nano-particles, to different uses of said nano-particles and compositions, and to products comprising or made from said nano-particles and compositions, including anti-reflective coatings and composite materials.

SILICA-BASED PARTICLE DISPERSION AND PRODUCTION METHOD THEREFOR

A silica-based particle dispersion including a silica-based particle group and a high polishing rate and high surface precision is achieved to a silica-based substrate or a NiP-plated substrate to be polished or the like. A silica-based particle dispersion containing a group including irregularly-shaped and non-irregularly-shaped silica-based particles, wherein the irregularly-shaped silica-based particles each have a plurality of small holes thereinside and a covering silica layer which covers the core, and the silica-based particle group satisfies [1]-[3]. [1] Having an average particle size (D.sub.1) of 100-600 nm, and a particle size (D.sub.2) of 30-300 nm in terms of specific surface area. [2] An irregular-shape degree D (D=D.sub.1/D.sub.3) represented by the average particle size (D.sub.1) and a projected area-equivalent particle size (D.sub.3) being in the range of 1.1-5.0. [3] When waveform separation is performed on a volume-reference particle size distribution, a multi-peak distribution in which three or more peaks are detected.

Porous silica-carbon composites and a method of producing the same

Porous silica-carbon composites are obtained by mixing fine particulate carbon dispersed in water by a surfactant, alkali metal silicate aqueous solution, and mineral acid so as to produce co-dispersion in which silica hydrosol, produced by reaction of the alkali metal silicate and the mineral acid, and the fine particulate carbon are uniformly dispersed, and gelling silica hydrosol, contained in the co-dispersion, and making the co-dispersion into porous bodies. The porous silica-carbon composites are prepared so as to have specific surface area from 20 to 1000 m.sup.2/g, pore volume from 0.3 to 2.0 ml/g, and average pore diameter from 2 to 100 nm.

Porous silica-carbon composites and a method of producing the same

Porous silica-carbon composites are obtained by mixing fine particulate carbon dispersed in water by a surfactant, alkali metal silicate aqueous solution, and mineral acid so as to produce co-dispersion in which silica hydrosol, produced by reaction of the alkali metal silicate and the mineral acid, and the fine particulate carbon are uniformly dispersed, and gelling silica hydrosol, contained in the co-dispersion, and making the co-dispersion into porous bodies. The porous silica-carbon composites are prepared so as to have specific surface area from 20 to 1000 m.sup.2/g, pore volume from 0.3 to 2.0 ml/g, and average pore diameter from 2 to 100 nm.