C01B33/405

SYNTHESIS OF HECTORITE-TYPE MINERAL
20220041458 · 2022-02-10 ·

A method of making a synthetic hectorite-type mineral is described, along with its resulting physical and rheological properties. The synthetic hectorite-type mineral is a 2:1 phyllosilicate essentially free of aluminum, and having a trioctahedral structure with Mg2+ and Li+ occupying octahedral sites. As a hydrogel, the synthetic hectorite-type mineral has a swell index of greater than 55 mL, and a yield point of greater than 290 Pa. The method of making uses a MgO/MgCO3 buffer system, with heating for about 2 hours at temperatures of no higher than 300° C. and pressures of no higher than 600 psi.

SYNTHETIC FUNCTIONALIZED ADDITIVES, METHODS OF SYNTHESIZING, AND METHODS OF USE

Some embodiments of the present disclosure are directed to synthetic functionalized additives, which may comprise a layered magnesium silicate. The present disclosure is also directed to drilling fluids that may comprise an aqueous base fluid and a synthetic functionalized additive. The present disclosure is further directed to methods for producing drilling fluids.

MAGNETIC NANO COMPOSITE MATERIAL BASED ON TWO-DIMENSIONAL LAYERED MATERIAL MAGADIITE, AND PREPARATION METHOD AND APPLICATION THEREOF

A magnetic nano composite material based on two-dimensional layered material magadiite, and a preparation method and an application thereof are provided. A co-precipitation method is used for one-step synthesis of the magnetic nano composite material based on the two-dimensional layered material magadiite. In the synthesized composite material, ferroferric oxide is uniformly supported on an interlayer and a surface of the magadiite. The composite material is applied for removing organic dyes in water pollution.

Layered silicate powder granules and method for producing the same

The invention has for its object to use an evaporation-spray drying process thereby providing layered silicate powder granules, each one containing a flat particle having an opening or recess in its surface center. Each of the layered silicate powder granule contains a flat particle including a layered silicate formed by evaporation-spray drying and a rheology modifier for modifying the crystal edge face of the layered silicate and having an opening or recess in its surface center.

CO-SYNTHESIS OF PHYLLOMINERALS WITH METALLIC PARTICLES AND PRODUCTS OBTAINED THERE-FROM

The present invention relates to methods for producing mixtures comprising noble metal and phyllomineral, and compositions obtained from said methods.

SILICATE-COATED BODY
20210198493 · 2021-07-01 ·

A silicate-coated body contains: a mica particle; a first silicate coating at least part of the mica particle; and an ionic organic colorant adsorbed to the first silicate. The ionic organic colorant includes at least one selected from the group consisting of amaranth, new coccine, phloxine B, rose bengal, acid red, fast green, indigo carmine, lithol rubine B, and lithol rubine BCA.

SILICATE-COATED BODY
20210171778 · 2021-06-10 ·

A silicate-coated body contains: a mica particle; a first silicate coating at least part of the mica particle; and a functional substance that is carried by the first silicate.

A PROCESS FOR DELAMINATION OF LAYERED SILICATES
20210047515 · 2021-02-18 ·

The invention relates to a process for delamination of a layered silicate in an aqueous medium, wherein in a first step a layered silicate is treated with a delamination agent, and in a second step the thus treated layered silicate is contacted with an aqueous medium, whereby the delamination agent is a compound having exactly one positively charged atom, the positively charged atom being selected from the group consisting of nitrogen and phosphorous; contains n.sub.f functional groups selected from the group consisting of hydroxyl groups, ether groups, sulfonic acid ester groups and carboxylic acid ester groups, n.sub.f being a number from 3 to 10; comprises a total number of carbon atoms n.sub.c being from 4 to 12; has a ratio n.sub.c/(1+n.sub.f) from 1 to 2, wherein n.sub.c is the total number of carbon atoms of the delamination agent and n.sub.f is the total number of functional groups in the delamination agent as defined under ii.; contains n.sub.t atoms selected from the group consisting of carbon, nitrogen, phosphorous, oxygen and sulfur, n.sub.t being 9; and wherein the delamination agent is used to treat the layered silicate in an amount of at least equal to the cation exchange capacity of the layered silicate. The invention further relates to the thus produced delaminated layered silicates, their use in the production of composite and coating material and as a barrier material. Moreover, the invention relates to compositions containing the thus produced delaminated layered silicates.

A PROCESS FOR DELAMINATION OF LAYERED SILICATES
20210047516 · 2021-02-18 ·

The invention relates to a process for delamination of a layered silicate in an aqueous medium, wherein in a first step a layered silicate having a layer charge L.sub.c from 0.25 to 1.0 and a charge equivalent area A.sub.s=47.6 .sup.2/(2L.sub.c), is treated with a delamination agent, and in a second step the thus treated layered silicate is contacted with an aqueous medium, whereby the delamination agent is a compound having exactly one positively charged atom, the positively charged atom being selected from the group consisting of nitrogen and phosphorous; contains of functional groups selected from the group consisting of hydroxyl groups, ether groups, sulfonic acid ester groups and carboxylic acid ester groups, n.sub.f being a number from 1 to 10; comprises a total number of carbon atoms n.sub.c being from 2 to 20; has a ratio n.sub.c/(1+n.sub.f) from 1 to 5, wherein n.sub.c is the total number of carbon atoms of the delamination agent and n.sub.f is the total number of functional groups in the delamination agent as defined under ii.; and has a charge equivalent area A.sub.d being from at least 0.90-fold to 3-fold of the charge equivalent area of the layered silicate A.sub.s; and wherein the delamination agent is used to treat the layered silicate in an amount of at least equal to the cation exchange capacity of the layered silicate, with the proviso that n.sub.f2, if L.sub.c0.6. The invention further relates to the thus produced delaminated layered silicates, their use in the production of composite and coating material and as a barrier material. Moreover, the invention relates to compositions containing the thus produced delaminated layered silicates.

Method for producing synthetic hectorite at low temperature and atmospheric pressure
10882752 · 2021-01-05 · ·

The present invention relates to a low-temperature/atmospheric-pressure method for producing synthetic hectorite and synthetic hectorite produced using the same, and more particularly, provides a method for producing synthetic hectorite at a low temperature and atmospheric pressure and synthetic hectorite produced using the same such that: a crystallization reaction may be carried out under a low-temperature/atmospheric-pressure condition by introducing a step of forming a precipitate and using a weak basic catalyst when the LiMg precipitates are formed; a reaction time may be reduced; synthetic hectorite with excellent major application properties may be prepared; and the properties may be easily controlled by controlling a composition ratio of a reactant.