The invention relates to the preparation of synthetic melted mica materials, and specifically relates to a stone casting process and to the composition of an initial feedstock, and may be used in the creation of novel types of stone casting in the metallurgical, mining/enrichment, refractory and construction industries. A method for producing melt-cast potassium fluorine-phlogopite includes preparing feedstock by mixing mica-containing and fluorine-containing components, melting the produced feedstock, pouring the melt into a mold, allowing to sit, removing the casting from the mold, and cooling; according to the claimed invention, the mica-containing component consists of vermiculite (60-90 wt % and the fluorine-containing component consists of potassium cryolite 10-40 wt %, wherein, the feedstock is melted via the sequential stepped heating thereof, and the feedstock is prepared by layering components, wherein the top layer of the feedstock consists of a mixture of components, and the melt is poured into a preheated mold. The use of the present invention allows for enhancing the chemical purity of the potassium fluorine-phlogopite, increasing the corrosion and erosion resistance of the material, and improving the accuracy of the chemical composition of the yielded product.

The invention relates to the preparation of synthetic melted mica materials, and specifically relates to a stone casting process and to the composition of an initial feedstock, and may be used in the creation of novel types of stone casting in the metallurgical, mining/enrichment, refractory and construction industries. A method for producing melt-cast potassium fluorine-phlogopite includes preparing feedstock by mixing mica-containing and fluorine-containing components, melting the produced feedstock, pouring the melt into a mold, allowing to sit, removing the casting from the mold, and cooling; according to the claimed invention, the mica-containing component consists of vermiculite (60-90 wt % and the fluorine-containing component consists of potassium cryolite 10-40 wt %, wherein, the feedstock is melted via the sequential stepped heating thereof, and the feedstock is prepared by layering components, wherein the top layer of the feedstock consists of a mixture of components, and the melt is poured into a preheated mold. The use of the present invention allows for enhancing the chemical purity of the potassium fluorine-phlogopite, increasing the corrosion and erosion resistance of the material, and improving the accuracy of the chemical composition of the yielded product.

The present invention relates to a device for efficiently preparing magnesium hydroxide, comprising a material mixing tank, a coordinated pressure control unit I, a reactor, a coordinated pressure control unit II, a condenser, a three-way valve, a material storage tank, a coordinated pressure control unit III and a steam generator. A outlet of the material mixing tank is connected with one end of the coordinated pressure control unit I by a pump; the other end of the coordinated pressure control unit I is connected with an inlet of the reactor; the outlet of the reactor is connected with one end of the coordinated pressure control unit II; the other end of the coordinated pressure control unit II is connected with one end of the condenser; the other end of the condenser is connected with a first port of the three-way valve; a second port of the three-way valve is connected with a material inlet of the material mixing tank; a third port of the three-way valve is connected with the material storage tank; a steam inlet of the reactor is connected with one end of the coordinated pressure control unit III; and the other end of the coordinated pressure control unit III is connected with the steam generator.

The present invention relates to a device for efficiently preparing magnesium hydroxide, comprising a material mixing tank, a coordinated pressure control unit I, a reactor, a coordinated pressure control unit II, a condenser, a three-way valve, a material storage tank, a coordinated pressure control unit III and a steam generator. A outlet of the material mixing tank is connected with one end of the coordinated pressure control unit I by a pump; the other end of the coordinated pressure control unit I is connected with an inlet of the reactor; the outlet of the reactor is connected with one end of the coordinated pressure control unit II; the other end of the coordinated pressure control unit II is connected with one end of the condenser; the other end of the condenser is connected with a first port of the three-way valve; a second port of the three-way valve is connected with a material inlet of the material mixing tank; a third port of the three-way valve is connected with the material storage tank; a steam inlet of the reactor is connected with one end of the coordinated pressure control unit III; and the other end of the coordinated pressure control unit III is connected with the steam generator.

A method is shown for the slaking of calcium oxides and magnesium from calcomagnesian compound containing at least 10 wt. % of MgO in relation to the total weight of said calcomagnesian compound, in which a slaking aqueous phase is supplied to a slaking device, and slaking the compound containing anhydrous dolomite delivered to the slaking device, by means of the slaking aqueous phase, forming hydrated solid particles of Mg(OH).sub.2, in the presence of an additive.

A method is shown for the slaking of calcium oxides and magnesium from calcomagnesian compound containing at least 10 wt. % of MgO in relation to the total weight of said calcomagnesian compound, in which a slaking aqueous phase is supplied to a slaking device, and slaking the compound containing anhydrous dolomite delivered to the slaking device, by means of the slaking aqueous phase, forming hydrated solid particles of Mg(OH).sub.2, in the presence of an additive.

The invention relates to a method for the dry slaking of calcium oxides and magnesium from calcomagnesian compound containing preferably at least 10 wt. % of MgO in relation to the total weight of said calcomagnesian compound, in which calcomagnesian compound is supplied to a slaking vessel, a slaking aqueous phase is supplied to the slaking vessel, followed by slaking the calcomagnesian compound delivered to the slaking vessel, by means of the slaking aqueous phase, and forming hydrated solid particles of calcium hydroxides and magnesium, in the presence of an additive. The invention also relates to the compound produced in this way.

The invention relates to a method for the dry slaking of calcium oxides and magnesium from calcomagnesian compound containing preferably at least 10 wt. % of MgO in relation to the total weight of said calcomagnesian compound, in which calcomagnesian compound is supplied to a slaking vessel, a slaking aqueous phase is supplied to the slaking vessel, followed by slaking the calcomagnesian compound delivered to the slaking vessel, by means of the slaking aqueous phase, and forming hydrated solid particles of calcium hydroxides and magnesium, in the presence of an additive. The invention also relates to the compound produced in this way.

A method of manufacture of high-solids hydroxide slurries from caustic calcined carbonate powder is described, whereby the properties of the slurry are its low resistance to shear thinning to facilitate transport, a high stability for transport and storage, ease of reconstitution after long periods of storage, and, as required, a high concentration of chemically reactive species at the particle surface. The method achieves these specifications by mixing caustic calcined carbonate or hydroxide powder with water in an insulated reactor vessel, and agitating the slurry sufficiently such that the hydration reaction causes the water to spontaneously boil, such that the remaining hydration proceeds spontaneously under the fixed conditions of boiling through the water loss. The mixing process is preferably carried out by a shear pump. A viscosity modifier, such as acetic acid, is used to thin the slurry to enable the mixing system to maintain uniform mixing. The reaction is terminated when the boiling has spontaneously ceased and the temperature has spontaneously dropped to a set point though the reactor heat losses, where the processing time is sufficiently long that the slurry meets the desired specifications.

A method of manufacture of high-solids hydroxide slurries from caustic calcined carbonate powder is described, whereby the properties of the slurry are its low resistance to shear thinning to facilitate transport, a high stability for transport and storage, ease of reconstitution after long periods of storage, and, as required, a high concentration of chemically reactive species at the particle surface. The method achieves these specifications by mixing caustic calcined carbonate or hydroxide powder with water in an insulated reactor vessel, and agitating the slurry sufficiently such that the hydration reaction causes the water to spontaneously boil, such that the remaining hydration proceeds spontaneously under the fixed conditions of boiling through the water loss. The mixing process is preferably carried out by a shear pump. A viscosity modifier, such as acetic acid, is used to thin the slurry to enable the mixing system to maintain uniform mixing. The reaction is terminated when the boiling has spontaneously ceased and the temperature has spontaneously dropped to a set point though the reactor heat losses, where the processing time is sufficiently long that the slurry meets the desired specifications.