C01F7/785

Microparticulate hydrotalcite, method for producing same, resin composition of same, and suspension of same
11591234 · 2023-02-28 · ·

A hydrotalcite is represented by formula (1):
(M.sup.2+).sub.1-X(M.sup.3+).sub.X(OH).sub.2(A.sup.n−).sub.X/n.Math.mH.sub.2O  (1), wherein M.sup.2+ indicates a divalent metal, M.sup.3+ indicates a trivalent metal, A.sup.n− indicates an n-valent anion, n indicates an integer of 1 to 6, 0.17≤x≤0.36, and 0≤m≤10. The hydrotalcite has (A) a lattice strain in the <003> direction is 3×10.sup.−3 or less as measured using an X-ray diffraction method; (B) primary particles with an average width between 5 nm and 200 nm inclusive per a SEM method; and (C) a degree of monodispersity of 50% or greater (degree of monodispersity (%)=(average width of primary particles as measured using the SEM method/average width of secondary particles as measured using a dynamic light scattering method)×100). A resin containing the hydrotalcite, a suspension containing the hydrotalcite and a method for producing the hydrotalcite are disclosed.

Microparticulate hydrotalcite, method for producing same, resin composition of same, and suspension of same
11591234 · 2023-02-28 · ·

A hydrotalcite is represented by formula (1):
(M.sup.2+).sub.1-X(M.sup.3+).sub.X(OH).sub.2(A.sup.n−).sub.X/n.Math.mH.sub.2O  (1), wherein M.sup.2+ indicates a divalent metal, M.sup.3+ indicates a trivalent metal, A.sup.n− indicates an n-valent anion, n indicates an integer of 1 to 6, 0.17≤x≤0.36, and 0≤m≤10. The hydrotalcite has (A) a lattice strain in the <003> direction is 3×10.sup.−3 or less as measured using an X-ray diffraction method; (B) primary particles with an average width between 5 nm and 200 nm inclusive per a SEM method; and (C) a degree of monodispersity of 50% or greater (degree of monodispersity (%)=(average width of primary particles as measured using the SEM method/average width of secondary particles as measured using a dynamic light scattering method)×100). A resin containing the hydrotalcite, a suspension containing the hydrotalcite and a method for producing the hydrotalcite are disclosed.

SiO2-layered double hydroxide microspheres and methods of making them
11643331 · 2023-05-09 · ·

Porous particles comprising an active ingredient and a coating exhibiting greater dissolution rate in aqueous media than in alcoholic media are disclosed. A process for the manufacture of the particles is also disclosed, as well as tamper-proof particles and solid dosage forms comprising the coated particles. The differential solubility characteristics of the particle coating allow the particles to be incorporated into abuse-deterrent medicaments.

SiO2-layered double hydroxide microspheres and methods of making them
11643331 · 2023-05-09 · ·

Porous particles comprising an active ingredient and a coating exhibiting greater dissolution rate in aqueous media than in alcoholic media are disclosed. A process for the manufacture of the particles is also disclosed, as well as tamper-proof particles and solid dosage forms comprising the coated particles. The differential solubility characteristics of the particle coating allow the particles to be incorporated into abuse-deterrent medicaments.

Surface modified layered double hydroxide

Surface-modified layered double hydroxides (LDHs) are disclosed, as well as processes by which they are made, and uses of the LDHs in composite materials. The surface-modified LDHs of the invention are more organophilic than their unmodified analogues, which allows the LDHs to be incorporated in a wide variety of materials, wherein the interesting functionality of LDHs may be exploited.

Hydrotalcite-like particulate material and method for production thereof

A hydrotalcite-like granular material having a grain size of 0.24 mm or larger is produced by drying a material that contains at least a hydrotalcite-like substance and that has a water content of 70% or lower at equal to or lower than a temperature at which the hydrotalcite-like substance is dehydrated of crystal water contained therein, preferably at 90° C. or higher and 110° C. or lower, such that the resulting hydrotalcite-like granular material has a water content of 10% or higher. In this manner, a hydrotalcite-like granular material that has a stable morphology and a high anion exchange performance and that can be produced at a low cost can be produced.

Application of lactam as solvent in nanomaterial preparation

The present invention disclosed use of lactam as a solvent in the preparation of nanomaterials by precipitation method, sol-gel method or high temperature pyrolysis. These methods are able to recycle lactam solvent, which meet requirements of environmental protection.

LAYERED DOUBLE HYDROXIDE FILM AND COMPOSITE MATERIAL CONTAINING LAYERED DOUBLE HYDROXIDE

Provided is a layered double hydroxide membrane containing a layered double hydroxide represented by the formula: M.sup.2+.sub.1−xM.sup.3+.sub.x(OH).sub.2A.sup.n−.sub.x/n.mH.sub.2O (where M.sup.2+ represents a divalent cation, M.sup.3+ represents a trivalent cation, A.sup.n− represents an n-valent anion, n is an integer of 1 or more, and x is 0.1 to 0.4), the layered double hydroxide membrane having water impermeability. The layered double hydroxide membrane includes a dense layer having water impermeability, and a non-flat surface structure that is rich in voids and/or protrusions and disposed on at least one side of the dense layer. The present invention provides an LDH membrane suitable for use as a solid electrolyte separator for a battery, the LDH membrane including a dense layer having water impermeability, and a specific structure disposed on at least one side of the dense layer and suitable for reducing the interfacial resistance between the LDH membrane and an electrolytic solution.

PREPARATION METHOD OF LITHIUM HYDROXIDE

A preparation method of lithium hydroxide includes the following steps: A. coprecipitating a lithium extraction mother solution of salt lake brine with an aluminum salt solution and a sodium hydroxide solution, aging and then performing solid-liquid separation, washing and drying to obtain lithium aluminum hydrotalcite; B. acidifying the lithium aluminum hydrotalcite to obtain a lithium aluminate solution; C. performing nanofiltration on the lithium aluminate solution for lithium-aluminum separation, and sequentially performing primary concentration by reverse osmosis to obtain a primary concentrated lithium-rich solution; D. deeply removing aluminum from the lithium-rich solution to obtain an aluminum-removed lithium-rich solution; E. performing bipolar membrane electrodialysis on the aluminum-removed lithium-rich solution to obtain a secondary concentrated lithium-rich solution; F. evaporating the secondary concentrated lithium-rich solution for concentration to obtain lithium hydroxide.

MAGNESIUM-ALUMINUM HYDROTALCITE-LOADED NANO ZERO-VALENT IRON COMPOSITE MATERIAL, METHOD FOR PREPARING SAME AND USE THEREOF

It discloses a method for preparing a magnesium-aluminum hydrotalcite-loaded nano zero-valent iron material for specifically removing perfluorooctanoic acid in a water environment and an optimized process for removing perfluorooctanoic acid thereby, and relates to the technical field of removing persistent organic pollutants in water using adsorption method and oxidation-reduction method and, in particular, to a composite material prepared by loading a nano zero-valent iron on magnesium-aluminum hydrotalcite using liquid phase reduction method.