An iron-based oxide magnetic particle powder has a narrow particle size distribution a small content of fine particles that do not contribute to magnetic recording characteristics, and a narrow coercive force distribution, to enhance magnetic recording medium density. Neutralizing an aqueous solution containing a trivalent iron ion and an ion of the metal substituting a part of the Fe sites by adding an alkali to make pH of 1.5 or more and 2.5 or less, adding a hydroxycarboxylic acid, and further neutralizing by adding an alkali to make pH of 8.0 or more and 9.0 or less are performed at 5° C. or more and 25° C. or less. A formed iron oxyhydroxide precipitate containing the substituting metal element is rinsed with water, then coated with silicon oxide, and then heated thereby providing e-type iron-based oxide magnetic particle powder. The rinsed precipitate may be subjected to a hydrothermal treatment.

An iron-based oxide magnetic particle powder has a narrow particle size distribution a small content of fine particles that do not contribute to magnetic recording characteristics, and a narrow coercive force distribution, to enhance magnetic recording medium density. Neutralizing an aqueous solution containing a trivalent iron ion and an ion of the metal substituting a part of the Fe sites by adding an alkali to make pH of 1.5 or more and 2.5 or less, adding a hydroxycarboxylic acid, and further neutralizing by adding an alkali to make pH of 8.0 or more and 9.0 or less are performed at 5° C. or more and 25° C. or less. A formed iron oxyhydroxide precipitate containing the substituting metal element is rinsed with water, then coated with silicon oxide, and then heated thereby providing e-type iron-based oxide magnetic particle powder. The rinsed precipitate may be subjected to a hydrothermal treatment.

A core-shell particle includes: a core including an iron oxyhydroxide compound represented by Formula A.sup.3.sub.a3Fe.sub.1−a3OOH (in which A.sup.3 represents at least one metal element other than Fe, and a3 satisfies 0<a3<1) or at least one iron oxide compound selected from the group consisting of Fe.sub.2O.sub.3, a compound represented by Formula A.sup.1.sub.a1Fe.sub.2−a1O.sub.3 (in which A.sup.1 represents at least one metal element other than Fe, and a1 satisfies 0<a1<2), Fe.sub.3O.sub.4, and a compound represented by Formula A.sup.2.sub.a2Fe.sub.3−a2O.sub.4 (in which A.sup.2 represents at least one metal element other than Fe, and a2 satisfies 0<a2<2); and a shell which covers the core and includes a polycondensate of a metal alkoxide.

A core-shell particle includes: a core including an iron oxyhydroxide compound represented by Formula A.sup.3.sub.a3Fe.sub.1−a3OOH (in which A.sup.3 represents at least one metal element other than Fe, and a3 satisfies 0<a3<1) or at least one iron oxide compound selected from the group consisting of Fe.sub.2O.sub.3, a compound represented by Formula A.sup.1.sub.a1Fe.sub.2−a1O.sub.3 (in which A.sup.1 represents at least one metal element other than Fe, and a1 satisfies 0<a1<2), Fe.sub.3O.sub.4, and a compound represented by Formula A.sup.2.sub.a2Fe.sub.3−a2O.sub.4 (in which A.sup.2 represents at least one metal element other than Fe, and a2 satisfies 0<a2<2); and a shell which covers the core and includes a polycondensate of a metal alkoxide.

The invention provides for the orchestrated treatment of disparate fractions of a shale deposit to recover vanadium values, with distinct steps of beneficiation that together provide a combined vanadium-enriched concentrate amenable to subsequent combined steps of hydrometallurgical vanadium extraction.

The present disclosure provides a method for separating iron element in brine and application thereof. The method for separating iron element in brine comprises: adding a pH adjusting agent to brine, to adjust pH of the brine to 6.0-7.0, and controlling the temperature of the brine to 75° C.-90° C.; introducing an oxygen-containing gas into the brine, to covert the iron element in the brine into magnetic iron oxide; and separating the magnetic iron oxide from the brine by magnetic adsorption to obtain an iron-removed brine.

This invention relates to a process for treating acid mine drainage (AMD). The process includes the steps of adjusting the pH of the AMD to be in the range of 3 to 5; adding maghemite nanoparticles to form a slurry; and a) aerating the slurry obtained in step 3), or b) simultaneously heating and mixing the slurry obtained in step 3). Thereafter maghemite nanoparticles loaded with one or more metals and sulphate and precipitated metals is separated from the slurry.

This invention relates to a process for treating acid mine drainage (AMD). The process includes the steps of adjusting the pH of the AMD to be in the range of 3 to 5; adding maghemite nanoparticles to form a slurry; and a) aerating the slurry obtained in step 3), or b) simultaneously heating and mixing the slurry obtained in step 3). Thereafter maghemite nanoparticles loaded with one or more metals and sulphate and precipitated metals is separated from the slurry.

A method of preparing iron oxide nanoparticles using an herbal mixture comprising Capparis spinosa, Cichorium intybus, Solanum nigrum, Cassia occidentalis, Terminalia arjuna, Achillea millefolium, and Tamarix gallica. The method produces crystalline γ-Fe.sub.2O.sub.3 nanoparticles which are superparamagnetic. The iron oxide nanoparticles are used in a method of killing or inhibiting the growth of a bacteria and/or fungus, particularly in the form of a biofilm. The nanoparticles are also used in a method of treating colon cancer.

A method of preparing iron oxide nanoparticles using an herbal mixture comprising Capparis spinosa, Cichorium intybus, Solanum nigrum, Cassia occidentalis, Terminalia arjuna, Achillea millefolium, and Tamarix gallica. The method produces crystalline γ-Fe.sub.2O.sub.3 nanoparticles which are superparamagnetic. The iron oxide nanoparticles are used in a method of killing or inhibiting the growth of a bacteria and/or fungus, particularly in the form of a biofilm. The nanoparticles are also used in a method of treating colon cancer.