A method for preparing all-solid-state photonic crystal fiber preform by extrusion by aligning the center of the first jacking end of the first jacking rod with the center of the core outlet mold. The adverse effect on this part of extruded core glass by oxygen or other impurities in air during the extrusion out of the core outlets can be avoided. The defects on the core glass surface and the cladding glass surface can be effectively removed, and the purity and quality of the core component in the obtained fiber preform can be improved.

Systems and methods according to one or more embodiments are provided for annealing a chalcogenide lens at an elevated temperature to accelerate release of internal stress within the chalcogenide lens caused during a molding process that formed the chalcogenide lens. In particular, the annealing process includes gradually heating the chalcogenide lens to a dwell temperature, maintaining the chalcogenide lens at the dwell temperature for a predetermined period of time, and gradually cooling the chalcogenide lens from the dwell temperature. The annealing process stabilizes the shape, the effective focal length, and/or the modulation transfer function of the chalcogenide lens. Associated optical assemblies and infrared imaging devices are also described.

A method of fabricating a shaped optical element for refracting infrared light. The method can include providing a chalcogenide glass mass within a precision mold, the chalcogenide glass mass having a starting volume that is equal to or less than about 105% of the volume of the shaped optical element, precision molding the chalcogenide glass mass by providing heat and pressure to form the chalcogenide glass mass into a near-net shaped optical element, removing the near-net shaped optical element from the precision mold, and refining the near-net shaped optical element to generate the shaped optical element, the outside diameter of the near-net shaped optical element being less than or equal to 25 μm larger than an outside diameter of the shaped optical element. The near-net shaped optical element can have an outside diameter less than 20 μm greater than the outside diameter of the shaped optical element.

A method for producing a solid electrolyte, including: stirring a slurry including lithium sulfide and phosphorus sulfide in a hydrocarbon solvent in a reaction vessel, and circulating the slurry through a connecting pipe by a pump. The method is carried out in an apparatus including the reaction vessel and the connecting pipe connected to the pump and the reaction vessel.

Molding a Li ion conductive sulfide glass construct into a flat preform shape using a mold having a molding surface of a material that is chemically inert in direct contact with a glass blank when heated can improve molding performance.

Li ion conductive sulfide glass, can be made by providing a pre-mix of precursor materials for making the Li ion conductive sulfide glass, providing a melting tank for processing the pre-mix to a molten state, and heating the melting tank to a temperature that is sufficient to melt form the Li ion conductive sulfide glass, wherein the melting tank is a metal vessel having inner wall surfaces that are coated with a corrosion resistant metal oxide layer.

The present invention provides for synthesizing high optical quality multicomponent chalcogenide glasses without refractive index perturbations due to striae, phase separation or crystal formation using a two-zone furnace and multiple fining steps. The top and bottom zones are initially heated to the same temperature, and then a temperature gradient is created between the top zone and the bottom zone. The fining and cooling phase is divided into multiple steps with multiple temperature holds.

Provided is a small-diameter chalcogenide glass material having excellent weather resistance and mechanical strength and being suitable as an optical element for an infrared sensor. The chalcogenide glass material has an unpolished side surface, a pillar shape with a diameter of 15 mm or less, and a composition of, in terms of % by mole, 40 to 90% S+Se+Te and an inside of the glass material is free of stria with a length of 500 μm or more.

Manufacturing methods for making a substantially rectangular and flat glass preform for manufacturing a Li ion conducting glass separator can involve drawing the preform to a thin sheet and may involve one or more of slumping, rolling or casting the glass within a frame that defines a space filling region and therewith the shape and size of the preform. The thickness of the rectangular flat preform so formed may be about 2 mm or less. The frame may be slotted having a back surface and widthwise wall portion that define the height and width of the space filling region. The flat backing surface and surfaces of the widthwise wall portions are defined may be coated by a material that is inert in direct contact with the heated glass material, such as gold.

Provided is a glass manufacturing method in which temperature can be easily increased and decreased at a high speed and in which the productivity can be improved. A glass manufacturing method according to an embodiment of the present invention includes the steps of: making a melt 11 by melting a raw material disposed in a container 1; obtaining a glass by cooling the melt 11, in which the raw material contains a metal, and in the step of making the melt 11 from the raw material, the raw material is induction-heated.