Provided herein are methods for making a freeze-cast material having a internal structure, the methods comprising steps of: determining the internal structure of the material, the internal structure having a plurality of pores, wherein: each of the plurality of pores has directionality; and the step of determining comprises: selecting a temperature gradient and a freezing front velocity to obtain the determined internal structure based on the selected temperature gradient and the selected freezing front velocity; directionally freezing a liquid formulation to form a frozen solid, the step of directionally freezing comprising: controlling the temperature gradient and the freezing front velocity to match the selected temperature gradient and the selected freezing front velocity during directionally freezing; wherein the liquid formulation comprises at least one solvent and at least one dispersed species; and subliming the at least one solvent out of the frozen solid to form the material.

A container, that includes a transparent portion, which reveals an interior portion of the container, an access aperture communicating with the interior portion of the container, and a lid adjacent the access aperture. A first liquid component is placed into the interior portion. A second liquid component is poured into the interior portion. The lid of the container is closed to fully enclose the first and second liquid components. The components are agitated until the first and second liquid components are a mixture of uniform color, without an appearance of marbling and swirling, when viewed through the transparent portion of the container. The lid is opened to expose the mixture of uniform color. The mixture of uniform color is poured from the container into a receiving structure. The mixture of uniform color is transformed into a closed-cell polyurethane structure within the receiving structure.

Provided herein are methods for making a freeze-cast material having a internal structure, the methods comprising steps of: determining the internal structure of the material, the internal structure having a plurality of pores, wherein: each of the plurality of pores has directionality; and the step of determining comprises: selecting a temperature gradient and a freezing front velocity to obtain the determined internal structure based on the selected temperature gradient and the selected freezing front velocity; directionally freezing a liquid formulation to form a frozen solid, the step of directionally freezing comprising: controlling the temperature gradient and the freezing front velocity to match the selected temperature gradient and the selected freezing front velocity during directionally freezing; wherein the liquid formulation comprises at least one solvent and at least one dispersed species; and subliming the at least one solvent out of the frozen solid to form the material.

A superhydrophobic coating is provided and contains organosilane, an inorganic nanomaterial, and an emulsifying agent. A mass proportion of the components is controlled, so that the superhydrophobic coating can form a micro-nano mixed microstructure inside foam concrete. The organosilane first forms dense hydrophobic surface layers on the surface and in inner pores of the foam concrete, and the nanomaterial forms uniformly distributed nano-bulges on the hydrophobic surface layers formed by the silane. The superhydrophobic performance of the foam concrete can be effectively improved by combining the two microstructures. The foam concrete exhibits excellent superhydrophobic performance.

Provided herein are methods for making a freeze-cast material having a internal structure, the methods comprising steps of: determining the internal structure of the material, the internal structure having a plurality of pores, wherein: each of the plurality of pores has directionality; and the step of determining comprises: selecting a temperature gradient and a freezing front velocity to obtain the determined internal structure based on the selected temperature gradient and the selected freezing front velocity; directionally freezing a liquid formulation to form a frozen solid, the step of directionally freezing comprising: controlling the temperature gradient and the freezing front velocity to match the selected temperature gradient and the selected freezing front velocity during directionally freezing; wherein the liquid formulation comprises at least one solvent and at least one dispersed species; and subliming the at least one solvent out of the frozen solid to form the material.

A combustion assembly for a gas turbine engine may be provided. The combustion assembly may include a ceramic matrix composite combustor shell, which may include a chamber defined by a wall of the ceramic matrix composite combustor shell, and the ceramic matrix composite combustor shell may include a ceramic matrix composite chute integral with the ceramic matrix composite combustor shell. The ceramic matrix composite chute may extend towards a midline of the chamber. A method for fabricating a ceramic matrix composite chute may be provided. At least one chute may be woven in three dimensions into a ceramic preform. A layup tool may be inserted into the chute. The chute may be enlarged with the layup tool. The ceramic preform may be formed into a ceramic matrix composite body, which includes a combustor shell and the chute.

A method for producing a bulk material consisting substantially of foamed or blown mineral or oxide particles by thermal treatment of a bulk material of basic particles, characterized in that the thermal treatment includes transport of a transversely conveyed or horizontal layer or of a free flow of the bulk material through a radiation field, the substantial active component of which lies in the near infrared range (NIR), and which has a power density of at least 50 kW/m2.

A superhydrophobic coating is provided and contains organosilane, an inorganic nanomaterial, and an emulsifying agent. A mass proportion of the components is controlled, so that the superhydrophobic coating can form a micro-nano mixed microstructure inside foam concrete. The organosilane first forms dense hydrophobic surface layers on the surface and in inner pores of the foam concrete, and the nanomaterial forms uniformly distributed nano-bulges on the hydrophobic surface layers formed by the silane. The superhydrophobic performance of the foam concrete can be effectively improved by combining the two microstructures. The foam concrete exhibits excellent superhydrophobic performance.

A method for producing a bulk material consisting substantially of foamed or blown mineral or oxide particles by thermal treatment of a bulk material of basic particles, characterized in that the thermal treatment includes transport of a transversely conveyed or horizontal layer or of a free flow of the bulk material through a radiation field, the substantial active component of which lies in the near infrared range (NIR), and which has a power density of at least 50 kW/m2.

Provided herein are methods for making a freeze-cast material having a internal structure, the methods comprising steps of: determining the internal structure of the material, the internal structure having a plurality of pores, wherein: each of the plurality of pores has directionality; and the step of determining comprises: selecting a temperature gradient and a freezing front velocity to obtain the determined internal structure based on the selected temperature gradient and the selected freezing front velocity; directionally freezing a liquid formulation to form a frozen solid, the step of directionally freezing comprising: controlling the temperature gradient and the freezing front velocity to match the selected temperature gradient and the selected freezing front velocity during directionally freezing; wherein the liquid formulation comprises at least one solvent and at least one dispersed species; and subliming the at least one solvent out of the frozen solid to form the material.