Provided is a method capable of manufacturing high-purity 1,3-butylene glycol having a high potassium permanganate test value, a very low content of low boiling point components, and a high initial boiling point with a high recovery rate.

A method for manufa.cturing 1,3-butylene glycol is a method for obtaining purified 1,3-butylene glycol from a crude reaction liquid containing 1,3-butylene glycol. In a dehydration column used in the dehydration step, a liquid feed containing 1,3-butylene glycol and water with an acetaldehyde content of 1000 ppm or lower and a crotonaldehyde content of 400 ppm or lower is distilled, and a liquid concentrated with a low boiling point component containing water is distilled off from above a feed plate; and in a product column used in the product distillation step, a 1,3-butylene glycol liquid feed having an acetaldehyde content of 500 ppm or lower and a crotonaldehyde content of 200 ppm or lower is distilled under a condition of a reflux ratio of higher than 0.1.

Provided is a method capable of manufacturing high-purity 1,3-butylene glycol having a high potassium permanganate test value, a very low content of low boiling point components, and a high initial boiling point with a high recovery rate.

A method for manufa.cturing 1,3-butylene glycol is a method for obtaining purified 1,3-butylene glycol from a crude reaction liquid containing 1,3-butylene glycol. In a dehydration column used in the dehydration step, a liquid feed containing 1,3-butylene glycol and water with an acetaldehyde content of 1000 ppm or lower and a crotonaldehyde content of 400 ppm or lower is distilled, and a liquid concentrated with a low boiling point component containing water is distilled off from above a feed plate; and in a product column used in the product distillation step, a 1,3-butylene glycol liquid feed having an acetaldehyde content of 500 ppm or lower and a crotonaldehyde content of 200 ppm or lower is distilled under a condition of a reflux ratio of higher than 0.1.

The present disclosure provides for organic solvent production via distillation and dehydration by: directing portions of a feed stream to a first and second distillation columns operating at a different pressures from each other, wherein the organic solvent is preferably an alcohol and more preferably ethanol; generating, in the first distillation column, a vaporous first overhead stream; directing the vaporous first overhead stream directly to a rectification system; generating, in the second distillation column, a vaporous second overhead stream; forming a condensed second overhead stream from the vaporous second overhead stream; directing, at least a portion of the condensed second overhead stream to the rectification system; generating, via the rectification system, a third overhead stream; directing at least a portion of the third overhead stream to a separation system; and generating, in the separation system, an enriched solvent stream.

The present disclosure provides for organic solvent production via distillation and dehydration by: directing portions of a feed stream to a first and second distillation columns operating at a different pressures from each other, wherein the organic solvent is preferably an alcohol and more preferably ethanol; generating, in the first distillation column, a vaporous first overhead stream; directing the vaporous first overhead stream directly to a rectification system; generating, in the second distillation column, a vaporous second overhead stream; forming a condensed second overhead stream from the vaporous second overhead stream; directing, at least a portion of the condensed second overhead stream to the rectification system; generating, via the rectification system, a third overhead stream; directing at least a portion of the third overhead stream to a separation system; and generating, in the separation system, an enriched solvent stream.

The present invention relates to a plant for removing C.sub.6-C.sub.11 hydrocarbons from methanol, comprising at least one reactor for the conversion of carbon monoxide and hydrogen to a crude methanol containing hydrocarbons, a distillation column with a head and a sump for the purification of the methanol, and at least one conduit for guiding the crude methanol from the at least one reactor into the distillation column. At its head, the distillation column includes a feed conduit for feeding in water.

The present invention relates to a plant for removing C.sub.6-C.sub.11 hydrocarbons from methanol, comprising at least one reactor for the conversion of carbon monoxide and hydrogen to a crude methanol containing hydrocarbons, a distillation column with a head and a sump for the purification of the methanol, and at least one conduit for guiding the crude methanol from the at least one reactor into the distillation column. At its head, the distillation column includes a feed conduit for feeding in water.

The present invention relates to a plant for removing C.sub.6-C.sub.11 hydrocarbons from methanol, comprising at least one reactor for the conversion of carbon monoxide and hydrogen to a crude methanol containing hydrocarbons, a distillation column with a head and a sump for the purification of the methanol, and at least one conduit for guiding the crude methanol from the at least one reactor into the distillation column. At its head, the distillation column includes a feed conduit for feeding in water.

The separation method separates a polyalcohol compound from water, so as to obtain a purified product stream comprising the polyalcohol compound in an output concentration of at least 90 wt %. Thereto, a mixture of the polyalcohol compound and water is provided, said mixture having a polyalcohol concentration. The polyalcohol concentration of the mixture is increased in an evaporation stage. Subsequently, the mixture is treated in a distillation stage to deliver the purified product stream comprising the polyalcohol compound in the output concentration of at least 90 wt %. Herein, the distillation stage is operated to produce steam output, that is optionally compressed to a steam pressure, and is coupled to the evaporation stage. The maximum distillation pressure and/or said compressed steam pressure is not less than the maximum evaporation pressure. The reactor system is configured for performing the separation method.

The separation method separates a polyalcohol compound from water, so as to obtain a purified product stream comprising the polyalcohol compound in an output concentration of at least 90 wt %. Thereto, a mixture of the polyalcohol compound and water is provided, said mixture having a polyalcohol concentration. The polyalcohol concentration of the mixture is increased in an evaporation stage. Subsequently, the mixture is treated in a distillation stage to deliver the purified product stream comprising the polyalcohol compound in the output concentration of at least 90 wt %. Herein, the distillation stage is operated to produce steam output, that is optionally compressed to a steam pressure, and is coupled to the evaporation stage. The maximum distillation pressure and/or said compressed steam pressure is not less than the maximum evaporation pressure. The reactor system is configured for performing the separation method.

A method is described herein, comprising vaporizing a glycol material by thermal contact with a heating medium to form a vaporized glycol stream, increasing a pressure of the vaporized glycol stream to form a pressurized glycol stream, and increasing a temperature of the heating medium by thermally contacting the heating medium with the pressurized glycol stream.