C07C37/70

SYSTEMS AND METHODS FOR REFINING CANNABIDIOL

A method of making CBD concentrate or CBD Isolate comprises (a) milling a raw material; (b) contacting the milled raw material with an extraction solvent and separating a solid waste material to form a filtered extract; (c) concentrating the filtered extract; (d) washing the concentrated extract to form an organic phase and an aqueous phase; (e) separating the aqueous phase from the organic phase to form a washed extract; (f) removing an organic solvent from the washed extract to form a concentrated washed extract; (g) decarboxylating the concentrated washed extract; (h) vacuum distilling the decarboxylated extract to form a distillate; (i) dewaxing the distillate to form a post-dewax filtrate; (j) applying a vacuum to the post-dewax filtrate to form a post-dewax concentrate; (k) degassing the post-dewax concentrate; and (l) vacuum distilling the degassed concentrate to form a CBD concentrate.

SYSTEMS AND METHODS FOR REFINING CANNABIDIOL

A method of making CBD concentrate or CBD Isolate comprises (a) milling a raw material; (b) contacting the milled raw material with an extraction solvent and separating a solid waste material to form a filtered extract; (c) concentrating the filtered extract; (d) washing the concentrated extract to form an organic phase and an aqueous phase; (e) separating the aqueous phase from the organic phase to form a washed extract; (f) removing an organic solvent from the washed extract to form a concentrated washed extract; (g) decarboxylating the concentrated washed extract; (h) vacuum distilling the decarboxylated extract to form a distillate; (i) dewaxing the distillate to form a post-dewax filtrate; (j) applying a vacuum to the post-dewax filtrate to form a post-dewax concentrate; (k) degassing the post-dewax concentrate; and (l) vacuum distilling the degassed concentrate to form a CBD concentrate.

SYSTEMS AND METHODS FOR CANNABIS CBD EXTRACTION
20230034720 · 2023-02-02 ·

Systems and methods for extracting a compound of interest from plant material, such as a cannabidiol (CBD) from cannabis, are provided. Particularly, the disclosed systems and methods utilize a crude oil to separate water and impurities including fats, sugars, resin glues, chlorophyll, and proteins prior to preparation of a CBD distillate. The systems and methods are operable to remove the impurities from the crude oil with a brine solution and at least one acid prior to distillation. The systems and methods are operable with conventional solvents containing between about 5 wt % and about 8 wt % water.

METHOD FOR PREPARING A SOLID FORM OF BISPHENOL F

A method for preparing a solid form of Bisphenol F is disclosed. The method comprises feeding Bisphenol F at a temperature in the range of 130-170° C. into an extruder; processing the fed Bisphenol F in a first mixing zone of the extruder, the first mixing zone maintained at a temperature in the range of 110-130° C., and then in a second mixing zone of the extruder, the second mixing zone maintained at a temperature in the range of 100-110° C.; conveying the processed Bisphenol F to a discharge zone of the extruder, the discharge zone maintained at a temperature in the range of 75-100° C.; discharging the processed Bisphenol F; and obtaining Bisphenol F in the solid form.

METHOD FOR PREPARING A SOLID FORM OF BISPHENOL F

A method for preparing a solid form of Bisphenol F is disclosed. The method comprises feeding Bisphenol F at a temperature in the range of 130-170° C. into an extruder; processing the fed Bisphenol F in a first mixing zone of the extruder, the first mixing zone maintained at a temperature in the range of 110-130° C., and then in a second mixing zone of the extruder, the second mixing zone maintained at a temperature in the range of 100-110° C.; conveying the processed Bisphenol F to a discharge zone of the extruder, the discharge zone maintained at a temperature in the range of 75-100° C.; discharging the processed Bisphenol F; and obtaining Bisphenol F in the solid form.

Processes for recovering valuable components from a catalytic fast pyrolysis process

Methods of separating products from the catalytic fast pyrolysis of biomass are described. In a preferred method, a portion of the products from a pyrolysis reactor are recovered and separated using a quench system and solvent contacting system that employs materials produced in the pyrolysis process.

Processes for recovering valuable components from a catalytic fast pyrolysis process

Methods of separating products from the catalytic fast pyrolysis of biomass are described. In a preferred method, a portion of the products from a pyrolysis reactor are recovered and separated using a quench system and solvent contacting system that employs materials produced in the pyrolysis process.

PROCESS FOR GENERATING HEMP OIL WITH A HIGH CANNABIDIOL (CBD) CONTENT
20210395176 · 2021-12-23 ·

A method for producing hemp oil, comprising decarboxylation of CBDA in hemp oil; short-path evaporation of CBD from the decarboxylated hemp oil to produce CBD oil; selective THC to CBN conversion performed on the decarboxylated hemp oil.

PROCESS FOR GENERATING HEMP OIL WITH A HIGH CANNABIDIOL (CBD) CONTENT
20210395176 · 2021-12-23 ·

A method for producing hemp oil, comprising decarboxylation of CBDA in hemp oil; short-path evaporation of CBD from the decarboxylated hemp oil to produce CBD oil; selective THC to CBN conversion performed on the decarboxylated hemp oil.

POWDERED BOTANICAL EXTRACT PREPARATIONS AND FORMULATIONS THEREOF
20210393719 · 2021-12-23 ·

The present invention provides a powdered botanical extract preparation comprising an evenly distributed dispersion of a botanical extract in a methylsulfonylmethane matrix, processes for preparing the preparations, and dosage forms comprising the preparations.