Patent classifications
C07C50/18
ELECTROACTIVE SPECIES AND METHOD FOR ELECTROCHEMICAL GAS SEPARATION
An electroactive species includes a quinone core structure and at least one stabilizing group covalently bound thereto. The stabilizing group includes a cationic group, a hydrogen bond donor, or a combination thereof. The electroactive species has an oxidized state and at least one reduced state capable of bonding with a Lewis acid gas to form an anion adduct. Methods for separating a Lewis acid gas from a fluid mixture, electrochemical cells, and gas separation systems are also provided.
ELECTROACTIVE SPECIES AND METHOD FOR ELECTROCHEMICAL GAS SEPARATION
An electroactive species includes a quinone core structure and at least one stabilizing group covalently bound thereto. The stabilizing group includes a cationic group, a hydrogen bond donor, or a combination thereof. The electroactive species has an oxidized state and at least one reduced state capable of bonding with a Lewis acid gas to form an anion adduct. Methods for separating a Lewis acid gas from a fluid mixture, electrochemical cells, and gas separation systems are also provided.
SENNA OBTUSIFOLIA SEED EXTRACT AND A METHOD FOR COMPREHENSIVE DEVELOPMENT AND UTILIZATION OF SENNA OBTUSIFOLIA SEEDS
A method of preparing a Senna obtusifolia seed extract rich in anthraquinones and a galactomannan extract includes the following steps: (1) crushing Senna obtusifolia seeds into a Senna obtusifolia seed powder; (2) extracting the Senna obtusifolia seed powder with 40-85% ethanol, filtering to obtain an extract solution and a residue; (3) concentrating the extract solution under vacuum to obtain a concentrated extract solution, spray-drying the concentrated extract solution to obtain the Senna obtusifolia seed extract; (4) extracting the residue with membrane filtered water, conducting a centrifugation to obtain a supernatant; (5) adding ammonium sulfate and ethanol to the supernatant to form a two-phase aqueous system, collecting a bottom layer of the two-phase aqueous system; and (6) conducting an ultrafiltration of the bottom layer with a cut-off molecular weight of 50 k-200 k to obtain a galactomannan extract solution, drying the galactomannan extract solution under vacuum to obtain the galactomannan extract.
SENNA OBTUSIFOLIA SEED EXTRACT AND A METHOD FOR COMPREHENSIVE DEVELOPMENT AND UTILIZATION OF SENNA OBTUSIFOLIA SEEDS
A method of preparing a Senna obtusifolia seed extract rich in anthraquinones and a galactomannan extract includes the following steps: (1) crushing Senna obtusifolia seeds into a Senna obtusifolia seed powder; (2) extracting the Senna obtusifolia seed powder with 40-85% ethanol, filtering to obtain an extract solution and a residue; (3) concentrating the extract solution under vacuum to obtain a concentrated extract solution, spray-drying the concentrated extract solution to obtain the Senna obtusifolia seed extract; (4) extracting the residue with membrane filtered water, conducting a centrifugation to obtain a supernatant; (5) adding ammonium sulfate and ethanol to the supernatant to form a two-phase aqueous system, collecting a bottom layer of the two-phase aqueous system; and (6) conducting an ultrafiltration of the bottom layer with a cut-off molecular weight of 50 k-200 k to obtain a galactomannan extract solution, drying the galactomannan extract solution under vacuum to obtain the galactomannan extract.
Method for separating 2-alkylanthracenes and use thereof for producing hydrogen peroxide
A method for preparing 2-alkylanthracene includes the step of separating 2-alkylanthracene from a reaction product of anthracene alkylation reaction. The anthracene alkylation reaction is a reaction of anthracene and an alkylation reagent under an alkylation condition and in the presence of an alkylation reaction solvent and a catalyst. The reaction product of the anthracene alkylation reaction contains anthracene and the product of a series of alkylanthracenes containing 2-alkylanthracene.
Method for separating 2-alkylanthracenes and use thereof for producing hydrogen peroxide
A method for preparing 2-alkylanthracene includes the step of separating 2-alkylanthracene from a reaction product of anthracene alkylation reaction. The anthracene alkylation reaction is a reaction of anthracene and an alkylation reagent under an alkylation condition and in the presence of an alkylation reaction solvent and a catalyst. The reaction product of the anthracene alkylation reaction contains anthracene and the product of a series of alkylanthracenes containing 2-alkylanthracene.
<i>Senna obtusifolia </i>seed extract and a method for comprehensive development and utilization of <i>Senna obtusifolia </i>seeds
A method of preparing a Senna obtusifolia seed extract rich in anthraquinones and a galactomannan extract includes the following steps: (1) crushing Senna obtusifolia seeds into a Senna obtusifolia seed powder; (2) extracting the Senna obtusifolia seed powder with 40-85% ethanol, filtering to obtain an extract solution and a residue; (3) concentrating the extract solution under vacuum to obtain a concentrated extract solution, spray-drying the concentrated extract solution to obtain the Senna obtusifolia seed extract; (4) extracting the residue with membrane filtered water, conducting a centrifugation to obtain a supernatant; (5) adding ammonium sulfate and ethanol to the supernatant to form a two-phase aqueous system, collecting a bottom layer of the two-phase aqueous system; and (6) conducting an ultrafiltration of the bottom layer with a cut-off molecular weight of 50 k-200 k to obtain a galactomannan extract solution, drying the galactomannan extract solution under vacuum to obtain the galactomannan extract.
<i>Senna obtusifolia </i>seed extract and a method for comprehensive development and utilization of <i>Senna obtusifolia </i>seeds
A method of preparing a Senna obtusifolia seed extract rich in anthraquinones and a galactomannan extract includes the following steps: (1) crushing Senna obtusifolia seeds into a Senna obtusifolia seed powder; (2) extracting the Senna obtusifolia seed powder with 40-85% ethanol, filtering to obtain an extract solution and a residue; (3) concentrating the extract solution under vacuum to obtain a concentrated extract solution, spray-drying the concentrated extract solution to obtain the Senna obtusifolia seed extract; (4) extracting the residue with membrane filtered water, conducting a centrifugation to obtain a supernatant; (5) adding ammonium sulfate and ethanol to the supernatant to form a two-phase aqueous system, collecting a bottom layer of the two-phase aqueous system; and (6) conducting an ultrafiltration of the bottom layer with a cut-off molecular weight of 50 k-200 k to obtain a galactomannan extract solution, drying the galactomannan extract solution under vacuum to obtain the galactomannan extract.
<i>Senna obtusifolia </i>seed extract and a method for comprehensive development and utilization of <i>Senna obtusifolia </i>seeds
A method of preparing a Senna obtusifolia seed extract rich in anthraquinones and a galactomannan extract includes the following steps: (1) crushing Senna obtusifolia seeds into a Senna obtusifolia seed powder; (2) extracting the Senna obtusifolia seed powder with 40-85% ethanol, filtering to obtain an extract solution and a residue; (3) concentrating the extract solution under vacuum to obtain a concentrated extract solution, spray-drying the concentrated extract solution to obtain the Senna obtusifolia seed extract; (4) extracting the residue with membrane filtered water, conducting a centrifugation to obtain a supernatant; (5) adding ammonium sulfate and ethanol to the supernatant to form a two-phase aqueous system, collecting a bottom layer of the two-phase aqueous system; and (6) conducting an ultrafiltration of the bottom layer with a cut-off molecular weight of 50 k-200 k to obtain a galactomannan extract solution, drying the galactomannan extract solution under vacuum to obtain the galactomannan extract.
Conductive surface coating based on modified and unmodified particles and method of preparation thereof
Conductive coating compositions and methods of preparation and application thereof are provided, whereby a mixture of conductive polymer encapsulated particles and non-encapsulated particles are employed to provide a conductive surface coating with controllable viscosity and conductivity. The particles may be filler and/or pigment particles such as calcium carbonate or clay, a portion of which are coated with a conductive polymer such as polypyrrole. Encapsulated particles are prepared and filtered, mixed with non-encapsulated particles, and subsequently combined with a binder for application to a surface or substrate such as paper. A dispersant may be included to obtain a suitable viscosity of the mixture prior to application. The relative concentrations of the encapsulated and non-encapsulated particles may be selected to tailor the resulting conductivity of the coating.