The solution provides a method for separating a Chinese traditional medicine composition. To explain a pharmacological effect mechanism of a medicine made of two or more components and scientific content in rules of compatibility among components of a compound medicine, systematic researches on the material basis is very necessary. Accordingly, deep researches are done on chemical components of the pharmaceutical composition in the solution, and eight compounds are separated, which are 10-O-(p-hydroxycinnamoyl)-adoxosidic acid, aloe-emodin-8-O-β-D-glucopyranoside, quercitrin, matairesinol-4′-O-glucoside, liquiritin apioside, epi-vogeloside, vogeloside and ethyl caffeate, which provides a new quality control method for the composition in the solution.

The present invention relates to a process for depolymerizing a polyester feedstock comprising opaque PET, which comprises: a) a conditioning step; b) a step of glycolysis, operated at between 180 and 400° C., a residence time of from 0.1 to 10 h in the presence of diol; c) a diol separation step, at a temperature of between 100 and 250° C., a pressure lower than that of step b) and producing a diol effluent and an effluent rich in monomers; d) a step of separating into a heavy impurities effluent and a prepurified monomers effluent, at a temperature of less than 250° C. and a pressure of less than 0.001 MPa and a residence time of less than 10 min; e) a step of decolourizing the prepurified monomers effluent, by adsorption of a mixture comprising between 20% and 90% by weight of the prepurified monomers effluent and a solvent, at a temperature of between 100 and 200° C., a pressure of between 0.1 and 1.0 MPa and in the presence of at least one adsorbent.

The present invention relates to a process for depolymerizing a polyester feedstock comprising opaque PET, which comprises: a) a conditioning step; b) a step of glycolysis, operated at between 180 and 400° C., a residence time of from 0.1 to 10 h in the presence of diol; c) a diol separation step, at a temperature of between 100 and 250° C., a pressure lower than that of step b) and producing a diol effluent and an effluent rich in monomers; d) a step of separating into a heavy impurities effluent and a prepurified monomers effluent, at a temperature of less than 250° C. and a pressure of less than 0.001 MPa and a residence time of less than 10 min; e) a step of decolourizing the prepurified monomers effluent, by adsorption of a mixture comprising between 20% and 90% by weight of the prepurified monomers effluent and a solvent, at a temperature of between 100 and 200° C., a pressure of between 0.1 and 1.0 MPa and in the presence of at least one adsorbent.

A gas separation method includes supplying a mixed gas to a zeolite membrane complex and permeating a high permeability gas through the zeolite membrane complex to separate the high permeability gas from other gases. The mixed gas includes a high permeability gas and a trace gas that is lower in concentration than the high permeability gas. The molar concentration of a first gas included in the trace gas in the mixed gas is higher than the molar concentration of a second gas included in the trace gas in the mixed gas. The adsorption equilibrium constant of the first gas on the zeolite membrane is less than 60 times that of the high permeability gas. The adsorption equilibrium constant of the second gas on the zeolite membrane is 400 times or more that of the high permeability gas.

A gas separation method includes supplying a mixed gas to a zeolite membrane complex and permeating a high permeability gas through the zeolite membrane complex to separate the high permeability gas from other gases. The mixed gas includes a high permeability gas and a trace gas that is lower in concentration than the high permeability gas. The molar concentration of a first gas included in the trace gas in the mixed gas is higher than the molar concentration of a second gas included in the trace gas in the mixed gas. The adsorption equilibrium constant of the first gas on the zeolite membrane is less than 60 times that of the high permeability gas. The adsorption equilibrium constant of the second gas on the zeolite membrane is 400 times or more that of the high permeability gas.

A preparation method of eicosapentaenoic acid (EPA) ethyl ester is provided and relates to the field of EPA ethyl ester processing technologies. The preparation method includes: performing degumming and deacidification on a sardine crude oil to obtain a semi-refined sardine oil, performing esterification on the semi-refined sardine oil to obtain an esterified sardine oil and then performing winterization on the esterified sardine oil to thereby obtain an semi-refined esterified sardine oil, performing bleaching and deodorization on the semi-refined esterified sardine oil, and performing multi-stage distillation treatment. Finally, the sardine oil is purified by liquid chromatography to obtain the high purity EPA ethyl ester. The preparation method can improve a utilization rate of the sardine oil and obtain the high-purity EPA ethyl ester.

A preparation method of eicosapentaenoic acid (EPA) ethyl ester is provided and relates to the field of EPA ethyl ester processing technologies. The preparation method includes: performing degumming and deacidification on a sardine crude oil to obtain a semi-refined sardine oil, performing esterification on the semi-refined sardine oil to obtain an esterified sardine oil and then performing winterization on the esterified sardine oil to thereby obtain an semi-refined esterified sardine oil, performing bleaching and deodorization on the semi-refined esterified sardine oil, and performing multi-stage distillation treatment. Finally, the sardine oil is purified by liquid chromatography to obtain the high purity EPA ethyl ester. The preparation method can improve a utilization rate of the sardine oil and obtain the high-purity EPA ethyl ester.

A preparation method of eicosapentaenoic acid (EPA) ethyl ester is provided and relates to the field of EPA ethyl ester processing technologies. The preparation method includes: performing degumming and deacidification on a sardine crude oil to obtain a semi-refined sardine oil, performing esterification on the semi-refined sardine oil to obtain an esterified sardine oil and then performing winterization on the esterified sardine oil to thereby obtain an semi-refined esterified sardine oil, performing bleaching and deodorization on the semi-refined esterified sardine oil, and performing multi-stage distillation treatment. Finally, the sardine oil is purified by liquid chromatography to obtain the high purity EPA ethyl ester. The preparation method can improve a utilization rate of the sardine oil and obtain the high-purity EPA ethyl ester.

This invention relates to a process for hydrogenation of a phthalate based compound. According to the invention, generation of by-products is inhibited during hydrogenation, and thus, catalytic activity is improved and life is prolonged, thereby increasing efficiency and economical feasibility of the industrial process. And, since the hydrogenation product prepared according to the invention has high purity and low acid value, it has excellent qualities as a plasticizer, and thus, can be used for various products.

This invention relates to a process for hydrogenation of a phthalate based compound. According to the invention, generation of by-products is inhibited during hydrogenation, and thus, catalytic activity is improved and life is prolonged, thereby increasing efficiency and economical feasibility of the industrial process. And, since the hydrogenation product prepared according to the invention has high purity and low acid value, it has excellent qualities as a plasticizer, and thus, can be used for various products.