C08B1/10

System for the production of a spinning dope composition

The present invention describes a method for the production of a spinning dope composition, said method comprising a homogenization involving vigorous mixing of a cellulosic pulp material in alkali solution, vigorous mixing implying supplying a power density to agitators used in the homogenization step of at least 150 kW/m.sup.3 (kW supplied to agitators per mixed unit of liquid volume), and thereafter a dissolution involving mixing of the cellulosic pulp material in the alkali solution to obtain a spinning dope composition, wherein the power density supplied to agitators used in the dissolution step is maximum 75 kW/m.sup.3 (kW supplied to agitators per mixed unit of liquid volume); and wherein the cellulosic pulp material in alkali solution is kept at a temperature of less than 0° C. during the homogenization and during at least part of the dissolution. The present invention is also directed to a system intended for the production of a spinning dope composition.

DEVICE FOR PRETREATING REFINED COTTON AND METHOD OF USE OF SAME

A device for pretreating refined cotton and a method of use thereof are provided. The device includes a body frame including a lower baseplate, four columns mounted on the upper surface of the lower baseplate, and an upper baseplate mounted at the top of the four columns, a first rotation shafts are fixed on the front and rear sides of a pretreatment drum, a lateral support is rotationally installed on the outer surface of the first rotation shaft; a power drive mechanism, a material-allocating mechanism and a reciprocating swing mechanism cooperate with a spraying mechanism, the stroke switch of the material-allocating mechanism cooperates with the power drive mechanism to achieve the forward and backward movement of the power drive mechanism, cooperates with the reciprocating swing mechanism to achieve the repeated swinging of the pretreatment drum, cooperates with the material-allocating mechanism to achieve the repeated fluctuation of the material.

DEVICE FOR PRETREATING REFINED COTTON AND METHOD OF USE OF SAME

A device for pretreating refined cotton and a method of use thereof are provided. The device includes a body frame including a lower baseplate, four columns mounted on the upper surface of the lower baseplate, and an upper baseplate mounted at the top of the four columns, a first rotation shafts are fixed on the front and rear sides of a pretreatment drum, a lateral support is rotationally installed on the outer surface of the first rotation shaft; a power drive mechanism, a material-allocating mechanism and a reciprocating swing mechanism cooperate with a spraying mechanism, the stroke switch of the material-allocating mechanism cooperates with the power drive mechanism to achieve the forward and backward movement of the power drive mechanism, cooperates with the reciprocating swing mechanism to achieve the repeated swinging of the pretreatment drum, cooperates with the material-allocating mechanism to achieve the repeated fluctuation of the material.

Methods for preparing alkali cellulose and cellulose ether

The invention is a method for efficiently preparing alkali cellulose having a uniform alkali distribution therein. More specifically, the invention is a method for preparing alkali cellulose comprising steps of bringing pulp into continuous contact with an alkali metal hydroxide solution in a bucket conveyor type contactor to generate a contact mixture, and draining the contact mixture; a method for preparing a cellulose ether comprising use of the alkali cellulose thus prepared; and an apparatus for preparing alkali cellulose comprising a bucket conveyor contactor comprising at least one inlet port for introducing pulp and an alkali metal hydroxide solution at one end and at least one outlet port for discharging a contact mixture wherein the pulp and the alkali metal hydroxide solution can be moved from one end to the other end while bringing them into contact with each other to generate the contact mixture; and a drainer for separating a cake from the contact mixture discharged from the outlet port.

Methods for preparing alkali cellulose and cellulose ether

The invention is a method for efficiently preparing alkali cellulose having a uniform alkali distribution therein. More specifically, the invention is a method for preparing alkali cellulose comprising steps of bringing pulp into continuous contact with an alkali metal hydroxide solution in a bucket conveyor type contactor to generate a contact mixture, and draining the contact mixture; a method for preparing a cellulose ether comprising use of the alkali cellulose thus prepared; and an apparatus for preparing alkali cellulose comprising a bucket conveyor contactor comprising at least one inlet port for introducing pulp and an alkali metal hydroxide solution at one end and at least one outlet port for discharging a contact mixture wherein the pulp and the alkali metal hydroxide solution can be moved from one end to the other end while bringing them into contact with each other to generate the contact mixture; and a drainer for separating a cake from the contact mixture discharged from the outlet port.

Methods for preparing alkali cellulose and cellulose ether

The invention is a method for efficiently preparing alkali cellulose having a uniform alkali distribution therein. More specifically, pulp and an excess alkali metal hydroxide solution are introduced continuously in a screw conveyor type contactor and brought into contact with each other in the screw conveyor type reactor. By changing at least one factor selected from the group consisting of a rotation speed of the screw conveyor, a screw pitch and a length of immersion zone, a ratio of an alkali to cellulose in the alkali cellulose obtained by draining is controlled. The alkali cellulose thus obtained is etherified into the corresponding cellulose ether.

Methods for preparing alkali cellulose and cellulose ether

The invention is a method for efficiently preparing alkali cellulose having a uniform alkali distribution therein. More specifically, pulp and an excess alkali metal hydroxide solution are introduced continuously in a screw conveyor type contactor and brought into contact with each other in the screw conveyor type reactor. By changing at least one factor selected from the group consisting of a rotation speed of the screw conveyor, a screw pitch and a length of immersion zone, a ratio of an alkali to cellulose in the alkali cellulose obtained by draining is controlled. The alkali cellulose thus obtained is etherified into the corresponding cellulose ether.

Methods for preparing alkali cellulose and cellulose ether

The invention is an efficient method for preparing alkali cellulose having the low water content and a uniform alkali distribution therein. More specifically, the invention is a method for continuously preparing alkali cellulose comprising steps of bringing pulp into continuous contact with an alkali metal hydroxide solution to generate a contact mixture and then draining the contact mixture by a centrifugal separator. The invention also includes a method for preparing cellulose ether comprising a step of etherifying the alkali cellulose.

Methods for preparing alkali cellulose and cellulose ether

The invention is an efficient method for preparing alkali cellulose having the low water content and a uniform alkali distribution therein. More specifically, the invention is a method for continuously preparing alkali cellulose comprising steps of bringing pulp into continuous contact with an alkali metal hydroxide solution to generate a contact mixture and then draining the contact mixture by a centrifugal separator. The invention also includes a method for preparing cellulose ether comprising a step of etherifying the alkali cellulose.