Embodiments of the invention relate to concrete admixtures, provide a phosphonato block polymer, a preparation method and an application. The method includes: the phosphonato block polymer prepared by copolycondensating an ether-type segment A, a phosphonato segment B, and a third part of aldehyde C. The ether-type segment A is obtained by polycondensating a polyether monomer and a first part of aldehyde C. The phosphonato segment B is obtained by polycondensating a monomer b containing phosphonato, a monomer c, and a second part of aldehyde C in an aprotic weak polar solvent E. By preparing a block polymer using arylalkane as a main chain and using a phosphonic acid or phosphinic acid functional group as an adsorption group, the invention improves the resistance of the block polymer to sulfate and clay interference, and can achieve initial high dispersion of concrete with a low water-cement ratio and decreasing of the system viscosity.

Embodiments of the invention relate to concrete admixtures, provide a phosphonato block polymer, a preparation method and an application. The method includes: the phosphonato block polymer prepared by copolycondensating an ether-type segment A, a phosphonato segment B, and a third part of aldehyde C. The ether-type segment A is obtained by polycondensating a polyether monomer and a first part of aldehyde C. The phosphonato segment B is obtained by polycondensating a monomer b containing phosphonato, a monomer c, and a second part of aldehyde C in an aprotic weak polar solvent E. By preparing a block polymer using arylalkane as a main chain and using a phosphonic acid or phosphinic acid functional group as an adsorption group, the invention improves the resistance of the block polymer to sulfate and clay interference, and can achieve initial high dispersion of concrete with a low water-cement ratio and decreasing of the system viscosity.

The present invention relates to a process for lignin dissolution in which partial methylolation of lignin is carried out during the step of preparing a solution of lignin in an aqueous medium comprising alkali and phenol. The lignin prepared according to the process of the present invention can be used to manufacture lignin-based phenolic resins, which are particularly useful in the manufacture of laminates.

The present invention relates to a process for lignin dissolution in which partial methylolation of lignin is carried out during the step of preparing a solution of lignin in an aqueous medium comprising alkali and phenol. The lignin prepared according to the process of the present invention can be used to manufacture lignin-based phenolic resins, which are particularly useful in the manufacture of laminates.

Methods of preparing phthalonitrile coating compositions are provided, including phthalonitrile sprays, phthalonitrile pastes, and phthalonitrile composite films. In embodiments, such a method comprises, heating a phthalonitrile precursor composition comprising a bisphthalonitrile compound to a temperature and for a period of time to form a phthalonitrile prepolymer composition comprising a bisphthalonitrile prepolymer; cooling the phthalonitrile prepolymer composition to ambient temperature and pulverizing the phthalonitrile prepolymer composition to form particles; combining the particles with a liquid medium to form a phthalonitrile solution; optionally, adding an additive to the phthalonitrile solution; and mixing the phthalonitrile solution to form a phthalonitrile coating composition.

Methods of preparing phthalonitrile coating compositions are provided, including phthalonitrile sprays, phthalonitrile pastes, and phthalonitrile composite films. In embodiments, such a method comprises, heating a phthalonitrile precursor composition comprising a bisphthalonitrile compound to a temperature and for a period of time to form a phthalonitrile prepolymer composition comprising a bisphthalonitrile prepolymer; cooling the phthalonitrile prepolymer composition to ambient temperature and pulverizing the phthalonitrile prepolymer composition to form particles; combining the particles with a liquid medium to form a phthalonitrile solution; optionally, adding an additive to the phthalonitrile solution; and mixing the phthalonitrile solution to form a phthalonitrile coating composition.

Embodiments of the invention relate to concrete admixtures, provide a phosphonato block polymer, a preparation method and an application. The method includes: the phosphonato block polymer prepared by copolycondensating an ether-type segment A, a phosphonato segment B, and a third part of aldehyde C. The ether-type segment A is obtained by polycondensating a polyether monomer and a first part of aldehyde C. The phosphonato segment B is obtained by polycondensating a monomer b containing phosphonato, a monomer c, and a second part of aldehyde C in an aprotic weak polar solvent E. By preparing a block polymer using arylalkane as a main chain and using a phosphonic acid or phosphinic acid functional group as an adsorption group, the invention improves the resistance of the block polymer to sulfate and clay interference, and can achieve initial high dispersion of concrete with a low water-cement ratio and decreasing of the system viscosity.

Embodiments of the invention relate to concrete admixtures, provide a phosphonato block polymer, a preparation method and an application. The method includes: the phosphonato block polymer prepared by copolycondensating an ether-type segment A, a phosphonato segment B, and a third part of aldehyde C. The ether-type segment A is obtained by polycondensating a polyether monomer and a first part of aldehyde C. The phosphonato segment B is obtained by polycondensating a monomer b containing phosphonato, a monomer c, and a second part of aldehyde C in an aprotic weak polar solvent E. By preparing a block polymer using arylalkane as a main chain and using a phosphonic acid or phosphinic acid functional group as an adsorption group, the invention improves the resistance of the block polymer to sulfate and clay interference, and can achieve initial high dispersion of concrete with a low water-cement ratio and decreasing of the system viscosity.

Methods of preparing phthalonitrile coating compositions are provided, including phthalonitrile sprays, phthalonitrile pastes, and phthalonitrile composite films. In embodiments, such a method comprises, heating a phthalonitrile precursor composition comprising a bisphthalonitrile compound to a temperature and for a period of time to form a phthalonitrile prepolymer composition comprising a bisphthalonitrile prepolymer; cooling the phthalonitrile prepolymer composition to ambient temperature and pulverizing the phthalonitrile prepolymer composition to form particles; combining the particles with a liquid medium to form a phthalonitrile solution; optionally, adding an additive to the phthalonitrile solution; and mixing the phthalonitrile solution to form a phthalonitrile coating composition.

Methods of preparing phthalonitrile coating compositions are provided, including phthalonitrile sprays, phthalonitrile pastes, and phthalonitrile composite films. In embodiments, such a method comprises, heating a phthalonitrile precursor composition comprising a bisphthalonitrile compound to a temperature and for a period of time to form a phthalonitrile prepolymer composition comprising a bisphthalonitrile prepolymer; cooling the phthalonitrile prepolymer composition to ambient temperature and pulverizing the phthalonitrile prepolymer composition to form particles; combining the particles with a liquid medium to form a phthalonitrile solution; optionally, adding an additive to the phthalonitrile solution; and mixing the phthalonitrile solution to form a phthalonitrile coating composition.