A method of producing microparticles by spray drying comprises the steps of providing a spray-drying feedstock solution comprising water, a volatile divalent metal salt, weak acid, 5-15% dairy or vegetable protein (w/v) and 1-20% active agent (w/v). The feedstock solution is adjusted to have a pH at which the volatile divalent metal salt is substantially insoluble. The feedstock solution is then spray-dried at an elevated temperature to provide atomised droplets, whereby the volatile divalent metal salt disassociates at the elevated temperature to release divalent metal ions which crosslink and aggregate the protein in the atomised droplets to produce microparticles having a crosslinked aggregated protein matrix and active agent dispersed throughout the matrix.

A method for continuously preparing graphene powder directly dispersed in an organic system, including: mixing an aqueous graphene oxide dispersion, an emulsifier and an oil-soluble monomer followed by pH adjustment and dispersing to obtain a pre-emulsified dispersion; subjecting the pre-emulsified dispersion to an emulsion polymerization reaction in the presence of an initiator; introducing a reducing agent to reduce graphene oxide; and subjecting the reaction mixture after emulsion polymerization to spray drying to obtain the graphene powder. Equipment used in the preparation method is also provided herein.

Embodiments of a spray-drying process for producing low aspect ratio particles of poly[(methyl methacrylate)-co-(methacrylic acid)] (PMMAMA) are disclosed. In some examples, at least 95% of PMMAMA-containing particles made by the process have an aspect ratio <10. The particles may further include an active ingredient and/or an excipient.

[Object]

The purpose of the present invention is to provide a layered composite that is high in both flexural modulus and moldability.

[Solving Means]

Provided is a layered composite including a carbon-fiber-reinforced resin in which a chopped strand prepreg obtained by impregnating fiber in resin is oriented in such a manner as to exhibit pseudo-isotropic properties, and a steel plate that is layered on at least one surface of the carbon-fiber-reinforced resin and has a tensile breakage elongation ϕ of equal to or more than 20%, the flexural modulus in a flat plate state obtained in compliance with ASTM D-790 being equal to or more than 30 GPa.

Protein-based nanoparticles and methods of forming such protein-based nanoparticles via electrohydrodynamic jetting methods are provided. The nanoparticle may comprise a water-soluble protein having an average molecular weight of ≥ about 8 kDa and < about 700 kDa. In certain variations, the water-soluble protein is cross-linked (e.g., with an optional crosslinking agent) and defines a mesh structure having an average linear mesh size of ≥ about 1 nm to ≤ about 4 nm. Methods of making such nanoparticles may include jetting a liquid comprising the water-soluble protein through a nozzle, followed by exposing the liquid to an electric field sufficient to solidify the liquid and form the protein-based nanoparticles described above.

C

Provided is a method of making a polymeric composition comprising (a) providing a dispersion of initial polyolefin particles in an aqueous medium, wherein the initial polyolefin particles comprise (i) one or more hydrocarbon polyolefin, (ii) one or more non-hydrocarbon polyolefin, and (iii) one or more crosslinking agent; (b) contacting the initial polyolefin particles with a peroxide initiator to form crosslinked polyolefin particles.

A method of preparing a superabsorbent polymer, which enables the preparation of the superabsorbent polymer exhibiting an improved absorption rate while maintaining excellent absorption performances is provided. The method of preparing the superabsorbent polymer includes carrying out a crosslinking polymerization of a water-soluble ethylene-based unsaturated monomer having acidic groups which are at least partially neutralized, in the presence of an internal crosslinking agent having a predetermined chemical structure to form a water-containing gel polymer, gel-pulverizing the water-containing gel polymer, drying, pulverizing, and size-sorting the gel-pulverized water-containing gel polymer to form a base polymer powder, and carrying out a surface crosslinking of the base polymer powder by a heat treatment in the presence of a surface crosslinking agent, wherein the gel-pulverizing is carried out by extruding the water-containing gel polymer through a porous plate having a plurality of holes using a screw extruder mounted inside a cylindrical pulverizer under a condition that a chopping index is 28 (/s) or more.

Superabsorbent mixtures M comprising at least 70% by weight of superabsorbent A having a liquid absorption of 20 g/g (T20) of less than 300 s and/or a volumetric liquid absorption under pressure 0.3 psi (2.07 kPa) (VAUL) with a τ value of less than 400 s, and at least 5% by weight of superabsorbent B having a centrifuge retention capacity (CRC) of at least 30 g/g.

The present invention provides a post-treatment method of a vinyl chloride-based polymer including: (a) preparing a stream containing vinyl chloride-based polymer powder and unreacted vinyl chloride-based monomers by drying a vinyl chloride-based polymer latex in a drying unit; (b) filtering the stream containing the vinyl chloride-based polymer powder and the unreacted vinyl chloride-based monomers in a filtering unit; and (c) recirculating a gas containing the unreacted vinyl chloride-based monomers discharged from the filtering unit to a latex storage unit.

The present invention relates to a method for preparing thermoplastic polymer particles, the method comprising the steps of: (1) extruding a thermoplastic polymer resin by means of an extruder; (2) granulating the extruded polymer resin by using an inert gas; and (3) cooling the granulated thermoplastic polymer resin, and thermoplastic polymer particles prepared thereby.