C09D101/26

Oxidation-resistant conductive copper paste, method for preparation thereof and method for manufacturing conductive film

The present invention discloses an oxidation-resistant conductive copper past, a manufacturing method and a use thereof. The oxidation-resistant conductive copper paste comprises 70 wt % to 90 wt % of copper particles, a binder, a thixotropic agent and a solvent. The manufacturing method comprises the steps of mixing the binder, the thixotropic agent and ethanol thoroughly to obtain a first mixture; mixing the solvent with the first mixture thoroughly to obtain a second mixture; mixing the copper particles with the second mixture to obtain a conductive copper paste precursor; and removing the ethanol from the conductive copper paste precursor to obtain the oxidation-resistant conductive copper paste. The oxidation-resistant conductive copper paste can be used for manufacturing a conductive film of a circuit board or an electrode of a solar battery by a printing process.

Oxidation-resistant conductive copper paste, method for preparation thereof and method for manufacturing conductive film

The present invention discloses an oxidation-resistant conductive copper past, a manufacturing method and a use thereof. The oxidation-resistant conductive copper paste comprises 70 wt % to 90 wt % of copper particles, a binder, a thixotropic agent and a solvent. The manufacturing method comprises the steps of mixing the binder, the thixotropic agent and ethanol thoroughly to obtain a first mixture; mixing the solvent with the first mixture thoroughly to obtain a second mixture; mixing the copper particles with the second mixture to obtain a conductive copper paste precursor; and removing the ethanol from the conductive copper paste precursor to obtain the oxidation-resistant conductive copper paste. The oxidation-resistant conductive copper paste can be used for manufacturing a conductive film of a circuit board or an electrode of a solar battery by a printing process.

ETHYLCELLULOSE DISPERSION AND POWDER

Provided is an aqueous composition having pH of 8 or higher and comprising (i) a solid phase comprising dispersed particles that comprise ethylcellulose polymer, (ii) fatty acid, wherein 25 mole % to 100 mole % of said fatty acid is in ionic form, (iii) 0% to 0.1% colloid stabilizer, by weight based on the dry weight of said ethylcellulose polymer, (iv) 0% to 7% plasticizer, by weight based on the dry weight of said ethylcellulose polymer, and (v) one or more cations of an alkali metal or an alkaline earth, wherein the equivalent ratio of said cations to said fatty acid is 0.1:1 to 2:1. Also provided are a method of spray drying an aqueous composition and a powder composition.

ETHYLCELLULOSE DISPERSION AND POWDER

Provided is an aqueous composition having pH of 8 or higher and comprising (i) a solid phase comprising dispersed particles that comprise ethylcellulose polymer, (ii) fatty acid, wherein 25 mole % to 100 mole % of said fatty acid is in ionic form, (iii) 0% to 0.1% colloid stabilizer, by weight based on the dry weight of said ethylcellulose polymer, (iv) 0% to 7% plasticizer, by weight based on the dry weight of said ethylcellulose polymer, and (v) one or more cations of an alkali metal or an alkaline earth, wherein the equivalent ratio of said cations to said fatty acid is 0.1:1 to 2:1. Also provided are a method of spray drying an aqueous composition and a powder composition.

GLASS-CERAMIC THERMAL PAINT SYSTEM AND METHOD USING UV:VIS SPECTROSCOPY

Temperature measurements are critical in gas turbine engine design but difficult to obtain due to the extreme environment. Temperature indicating paints (thermal paints) have been used for decades to map maximum temperature fields on superalloy components but have numerous weaknesses. Disclosed herein are novel glass ceramic thermal paints that undergo viscous flow sintering to indicate temperatures up to 1000° C., with high resolution (±5° C.), by an optical transition. Disclosed paint formulations are designed to adhere to Nickel-based superalloys or SiC—SiC ceramic matrix composites (CMC) by closely matching coefficients of thermal expansion and may function for times above 60 hours. By utilizing automation and a UV:VIS spectrometer, quantitative temperature maps can be generated for easy comparison to theoretical models. A transient sintering energy model is disclosed to recover full thermal history information.

GLASS-CERAMIC THERMAL PAINT SYSTEM AND METHOD USING UV:VIS SPECTROSCOPY

Temperature measurements are critical in gas turbine engine design but difficult to obtain due to the extreme environment. Temperature indicating paints (thermal paints) have been used for decades to map maximum temperature fields on superalloy components but have numerous weaknesses. Disclosed herein are novel glass ceramic thermal paints that undergo viscous flow sintering to indicate temperatures up to 1000° C., with high resolution (±5° C.), by an optical transition. Disclosed paint formulations are designed to adhere to Nickel-based superalloys or SiC—SiC ceramic matrix composites (CMC) by closely matching coefficients of thermal expansion and may function for times above 60 hours. By utilizing automation and a UV:VIS spectrometer, quantitative temperature maps can be generated for easy comparison to theoretical models. A transient sintering energy model is disclosed to recover full thermal history information.

SELF-HEALING, OMNIPHOBIC COATINGS AND RELATED METHODS
20210261807 · 2021-08-26 ·

Self-healable, omniphobic coatings and related methods are provided. In embodiments, a self-healable, omniphobic coating comprises a matrix of crosslinked, entangled hydrogel polymers, the hydrogel polymers comprising hydroxyl (OH) groups, hydroxyl group precursors, or both, and nanoparticles distributed throughout the matrix; and fluorinated silane molecules covalently bound to the matrix.

OXIDATION-RESISTANT CONDUCTIVE COPPER PASTE, METHOD FOR PREPARATION THEREOF AND METHOD FOR MANUFACTURING CONDUCTIVE FILM
20200407569 · 2020-12-31 ·

The present invention discloses an oxidation-resistant conductive copper past, a manufacturing method and a use thereof. The oxidation-resistant conductive copper paste comprises 70 wt % to 90 wt % of copper particles, a binder, a thixotropic agent and a solvent. The manufacturing method comprises the steps of mixing the binder, the thixotropic agent and ethanol thoroughly to obtain a first mixture; mixing the solvent with the first mixture thoroughly to obtain a second mixture; mixing the copper particles with the second mixture to obtain a conductive copper paste precursor; and removing the ethanol from the conductive copper paste precursor to obtain the oxidation-resistant conductive copper paste. The oxidation-resistant conductive copper paste can be used for manufacturing a conductive film of a circuit board or an electrode of a solar battery by a printing process.

OXIDATION-RESISTANT CONDUCTIVE COPPER PASTE, METHOD FOR PREPARATION THEREOF AND METHOD FOR MANUFACTURING CONDUCTIVE FILM
20200407569 · 2020-12-31 ·

The present invention discloses an oxidation-resistant conductive copper past, a manufacturing method and a use thereof. The oxidation-resistant conductive copper paste comprises 70 wt % to 90 wt % of copper particles, a binder, a thixotropic agent and a solvent. The manufacturing method comprises the steps of mixing the binder, the thixotropic agent and ethanol thoroughly to obtain a first mixture; mixing the solvent with the first mixture thoroughly to obtain a second mixture; mixing the copper particles with the second mixture to obtain a conductive copper paste precursor; and removing the ethanol from the conductive copper paste precursor to obtain the oxidation-resistant conductive copper paste. The oxidation-resistant conductive copper paste can be used for manufacturing a conductive film of a circuit board or an electrode of a solar battery by a printing process.

Coating Composition for Applying Inkjet Printing Thereto to Form Marked Preparation, Preparation Marked with Aqueous Ink, and Method for Producing Marked Preparation

There are provided a coating composition for applying inkjet printing thereto to form a marked preparation, the composition providing good ink affinity, suppression of ink bleed, and excellent gloss; and others. More specifically, there are provided a composition for applying inkjet printing thereto to form a marked preparation, the composition including a water-soluble cellulose ether having a viscosity at 20 C. of from 2 to 50.0 mPa.Math.s, as determined in 2% by mass aqueous solution, polyvinyl alcohol, and a solvent, wherein a mass ratio of the water-soluble cellulose ether to the polyvinyl alcohol is from 99.0:1.0 to 55.0:45.0; a method for producing a preparation marked with aqueous ink, including a coating step of coating an object with the composition to form a coating layer, and a printing step of inkjet-printing on the coating layer with aqueous ink to obtain a preparation marked with aqueous ink; and others.