The invention discloses a lubricating grease with thixotropy and a preparation method thereof. The lubricating grease comprises a polyurea/high base number calcium sulfonate composite thickener, colloidally dispersed calcium carbonate solid particles in the form of calcite, a calcium borate or calcium borate composite, and a calcium soap of fatty acid having 12 to 24 carbon atoms. The above components are uniformly dispersed in an oil phase medium. The content of high base number calcium sulfonate in the lubricating grease is less than 22 wt %.

The invention discloses a lubricating grease with thixotropy and a preparation method thereof. The lubricating grease comprises a polyurea/high base number calcium sulfonate composite thickener, colloidally dispersed calcium carbonate solid particles in the form of calcite, a calcium borate or calcium borate composite, and a calcium soap of fatty acid having 12 to 24 carbon atoms. The above components are uniformly dispersed in an oil phase medium. The content of high base number calcium sulfonate in the lubricating grease is less than 22 wt %.

An extremely rheopectic sulfonate-based grease composition and method comprising adding overbased calcium sulfonate, overbased magnesium sulfonate, and a facilitating acid, using a particular type of overbased calcium sulfonate and/or methods for adding overbased calcium sulfonate relative to the magnesium sulfonate and facilitating acid to favor the reaction between the magnesium sulfonate and facilitating acid. A preferred overbased calcium sulfonate comprises benzene rings having multiple alkyl groups. Preferred methods comprise (1) adding all calcium sulfonate after adding the magnesium sulfonate and facilitating acid, (2) adding a first portion of calcium sulfonate with the magnesium sulfonate before adding the facilitating acid and a second portion of calcium sulfonate after the facilitating acid, and/or (3) one or more calcium sulfonate delay periods relative to adding the facilitating acid. The extremely rheopectic grease is fluid and pourable and only takes on a grease structure after milling or shearing.

A method of making an overbased calcium sulfonate or calcium magnesium sulfonate grease using one or more delay periods between the addition of at least a portion of a facilitating acid, such as DDBSA, and at least a portion of the next subsequently added ingredient. The delay period may be a temperature adjustment delay or a holding delay period. An overbased calcium sulfonate or calcium magnesium sulfonate grease composition comprises 0.5%-5% of a facilitating acid, allows for a reduced amount of overbased calcium sulfonate below 22%, and allows for a reduced amount of calcium hydroxyapatite to provide 10-25% of hydroxide equivalent basicity of the total hydroxide equivalent basicity due to calcium hydroxyapatite and added calcium hydroxide, while maintaining a high dropping point.

An overbased calcium magnesium sulfonate grease composition and method of making such grease without using any conventional non-aqueous converting agents, such as hexylene glycol, as a pre-conversion ingredient. The addition of magnesium sulfonate as an ingredient prior to conversion appears to act as a new, non-conventional converting agent, resulting in greases with improved thickener yield and excellent dropping point.

A bearing flushing composition includes a grease component and a solvent component. The grease component may include a grease thickener component, a base oil component, and, optionally, a performance additive component. The solvent component may include one or more solvent agents blended with the grease component.

A bearing flushing composition includes a grease component and a solvent component. The grease component may include a grease thickener component, a base oil component, and, optionally, a performance additive component. The solvent component may include one or more solvent agents blended with the grease component.

This invention relates to overbased calcium sulfonate complex grease compositions prepared without boric acid and alcohol promotors containing anti-wear, anti-friction, thermal & oxidation stability additives.

This invention relates to overbased calcium sulfonate complex grease compositions prepared without boric acid and alcohol promotors containing anti-wear, anti-friction, thermal & oxidation stability additives.

The invention discloses a lubricating grease with thixotropy and a preparation method thereof. The lubricating grease comprises a polyurea/high base number calcium sulfonate composite thickener, colloidally dispersed calcium carbonate solid particles in the form of calcite, a calcium borate or calcium borate composite, and a calcium soap of fatty acid having 12 to 24 carbon atoms. The above components are uniformly dispersed in an oil phase medium. The content of high base number calcium sulfonate in the lubricating grease is less than 22 wt %, and the lubricating grease has a worked cone penetration of 295 or less.